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Basic Information
CAS No.: 4651-67-6
Name: 3ALPHA-HYDROXY-7-OXO-5BETA-CHOLANIC ACID
Article Data: 70
Molecular Structure:
Molecular Structure of 4651-67-6 (3ALPHA-HYDROXY-7-OXO-5BETA-CHOLANIC ACID)
Formula: C24H38O4
Molecular Weight: 390.563
Synonyms: 3α-Hydroxy-7-keto-5β-cholanic Acid;3ALPHA-HYDROXY-7-OXO-5BETA-CHOLANIC ACID;3α-Hydroxy-7-oxo-5β-cholanic Acid;3a-Hydroxy-7-oxo-5b-cholanic acid;
Density: 1.124g/cm3
Melting Point: 205oC
Boiling Point: 545.9°C at 760 mmHg
Flash Point: 298°C
Solubility: 2.062mg/L at 25℃
PSA: 74.60000
LogP: 4.68610
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Synthetic route

3α-hydroxy-7-keto-5β-chol-11-en-24-oic acid

4651-67-6

7-Ketolithocholic acid

Conditions
ConditionsYield
With palladium on activated charcoal; hydrogen In methanol at 70℃; under 30003 Torr; for 12h;99%
With palladium on activated charcoal; hydrogen In tetrahydrofuran; methanol at 70℃; under 30003 Torr; for 8h;95%
With palladium on activated charcoal; hydrogen In tetrahydrofuran; methanol at 70℃; under 30003 Torr; for 8h;95%
474-25-9

chenodeoxycholic acid

4651-67-6

7-Ketolithocholic acid

Conditions
ConditionsYield
With dimethyl sulfoxide; triethylamine; trifluoroacetic anhydride In dichloromethane at -30℃; for 1.5h; Temperature; Swern Oxidation;98.6%
With sodium bromate; sulfuric acid; sodium bromide In dichloromethane at 20 - 30℃; for 6h;96.1%
With N-Bromosuccinimide In water; acetone at 20℃; for 2h; Darkness;94%
2646-38-0

sodium chenodeoxycholate

4651-67-6

7-Ketolithocholic acid

Conditions
ConditionsYield
With ethylenediaminetetraacetic acid; Acinetobacter calcoaceticus lwoffii 7α-hydroxysteroid dehydrogenase; sodium pyruvate; NAD; 2-hydroxyethanethiol; lactate dehydrogenase In aq. phosphate buffer at 22℃; pH=8.5; Enzymatic reaction;97%
With Xanthomonas maltophilia BS6 broth In water at 30℃; for 48h;99 % Chromat.

chenodeoxycholic acid

4651-67-6

7-Ketolithocholic acid

Conditions
ConditionsYield
Stage #1: chenodeoxycholic acid With tartaric acid In methanol for 0.5h;
Stage #2: With sodium hypochlorite In methanol at 15 - 22℃; for 1h;		96.1%
10538-59-7

7-ketolithocholic methyl ester

4651-67-6

7-Ketolithocholic acid

Conditions
ConditionsYield
With sodium hydroxide In tetrahydrofuran; methanol for 3h; Reflux;95%
With water; lithium hydroxide In tetrahydrofuran at 20℃; for 4h;74%
With water; sodium hydroxide In methanol for 2h; Solvent; Reflux;32 g
10452-65-0

methyl 3α-acetoxy-7-oxo-5β-cholan-24-oate

4651-67-6

7-Ketolithocholic acid

Conditions
ConditionsYield
With methanol; sodium hydroxide In tetrahydrofuran for 3h; Reflux;95%
With water; sodium hydroxide In ethanol for 2h; Reflux;32 g

C42H52O7

4651-67-6

7-Ketolithocholic acid

Conditions
ConditionsYield
With hydrogen In isopropyl alcohol at 50℃; under 22502.3 Torr; for 24h;95%
With hydrogen In isopropyl alcohol at 50℃; under 22502.3 Torr; for 24h;95%

chenodeoxycholic acid

A

859-97-2

3,7-diketocholanic acid

B

4651-67-6

7-Ketolithocholic acid

Conditions
ConditionsYield
Stage #1: chenodeoxycholic acid With tartaric acid In methanol for 0.5h;
Stage #2: With calcium hypochlorite In methanol at 15 - 22℃; for 1h;		A 5.13%
B 93.3%

C31H42O4

4651-67-6

7-Ketolithocholic acid

Conditions
ConditionsYield
With palladium on activated charcoal; hydrogen In tetrahydrofuran; methanol at 70℃; under 30003 Torr; for 8h;90%
With palladium on activated charcoal; hydrogen In tetrahydrofuran; methanol at 70℃; under 30003 Torr; for 8h;90%
474-25-9

chenodeoxycholic acid

A

859-97-2

3,7-diketocholanic acid

B

4651-67-6

7-Ketolithocholic acid

Conditions
ConditionsYield
With sodium bromate; ammonium cerium (IV) nitrate In water; acetonitrile at 60℃; for 0.5h; Green chemistry;A 9%
B 83%
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  •  Hangzhou Lingrui Chemical Co.,Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:86 571-88092529-

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  • 3.alpha.-Hydroxy-7-oxo-5.beta.-cholanic acid

  • Casno:

    4651-67-6

    3.alpha.-Hydroxy-7-oxo-5.beta.-cholanic acid

    Min.Order: 0

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    J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

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  •  Hangzhou J&H Chemical Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-87396432

    Address:No.200 Zhenhua Rd.Xihu Industrial Park, Hangzhou 310030, China

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  • Casno:

    4651-67-6

    3-alpha-hydroxy-7-oxo-5-beta-cholan-24-oic acid

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    Appearance:liquid Storage:Store the container tightly closed in a dry, cool and well-ventilated place. Store apart from foodstuff containers or incompatible materials. Package:Grams, Kilograms Application:For R&D and commerical use Transportati

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  •  Chemlyte Solutions

    China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:+86-189 8945 5137

    Address:Jian Qiao Community, 789 Shenhua Road, Xihu District, Hangzhou, China, 310000

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    3a-hydroxy-7-oxo-5b-cholanic/High quality/Best price

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  •  Shanghai Massive Chemical Technology Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86 21 34943721

    Address:Room 435, 4th floor, Building 9, No. 2568 Gudai Road,Minhang District, Shanghai,

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  • Casno:

    4651-67-6

    3-Hydroxy-7-oxocholan-24-oic acid

    Min.Order: 10 Gram

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    Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

    Hangyu Biotech is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and O

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    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-15965530500

    Address:Room1701, Tianxing Building,Licheng district, jinan, Shandong, China

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  • Casno:

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    Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as

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     China (Mainland)  |  Contact Details

    Business Type:Manufacturers

    Tel:0731-85567275

    Address:No.10048, xiangjiang centry bulding ,kaifu district ,changsha city ,Hunan

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  • Casno:

    4651-67-6

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    SHANGHAI SYSTEAM BIOCHEM CO., LTD. is one of the professional suppliers in Chinese pharmaceutical market and is specialized in custom synthesis, chemical/pharmaceutical/ pesticides

  •  SHANGHAI SYSTEAM BIOCHEM CO., LTD

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-021-58380978

    Address:Building 87，Lane 669， Dong Jing Road Shanghai,P.R.China

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  • Casno:

    4651-67-6

    3ALPHA-HYDROXY-7-OXO-5BETA-CHOLANIC ACID

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    TaiChem was established in 2015 and registered in China medical city - Taizhou, Jiangsu Province. The company has about 1800 square meters of class A plant facility. TaiChem focuse

  •  TaiChem Taizhou Limited

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-0523-86810091

    Address:Changjiang Dadao 18

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  • Casno:

    4651-67-6

    High Quality 3Alpha-Hydroxy-7-Oxo-5Beta-Cholanic Acid

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    Product name: 3Alpha-Hydroxy-7-Oxo-5Beta-Cholanic Acid CAS No.：4651-67-6 Molecule Formula：C24H38O4 Molecule Weight：390.56 Purity: 98.0% Package: 25kg/drum Description：White powder Manufacture Standards：Enterprise Standard

    Siwei Development Group Ltd. is a reputed professional enterprise in China dedicated to the Amino Acids production and sales of fine chemical products.Over the years we have been m

  •  Siwei Development Group Ltd.

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:86-571-82881840

    Address:Rm2-2-503 Zhongdingyuan, Xianghurenjia Wenyan Xiaoshan, Hangzhou China

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  • Casno:

    4651-67-6

    3-alpha-hydroxy-7-oxo-5-beta-cholan-24-oic acid

    Min.Order: 1 Gram

    FOB Price:  USD $ 0.0-0.0

    Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

    Zibo Dorne chemical technology co., LTD. is a biotechnology enterprise engaged in the R&D, production and sales of drugs, steroids, peptides, raw materials, vitamins, food additive

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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    1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualified

    Wuhan Circle Star Chem-medic Technology co.,Ltd is located in wuhan, the central city of China, the core of the Changjiang river economic belt and known as the "thoroughfare of ni

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-13437180835

    Address:Room 02-31, 13 / F, Building 9, Guannan Fuxing Medical Park Phase II, No.58, Guanggu Avenue, East Lake New Technology Development Zone, Wuhan, Hubei, China (Wuhan Area, Free Trade Zone)

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  • Casno:

    4651-67-6

    3ALPHA-HYDROXY-7-OXO-5BETA-CHOLANIC ACID

    Min.Order: 1 Kilogram

    FOB Price:  USD $ 18.0-20.0

    factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

    Founded in 2008, East Chemsources Limited is a professional manufacturer of supplier in food and beverage, pharmaceuticals, cosmetics and other industries. pharmaceutical field in

  •  EAST CHEMSOURCES LIMITED

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:15053231572

    Address:No.1581-12,Jinshui Road, Licang, Qingdao,China

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  • 3ALPHA-HYDROXY-7-OXO-5BETA-CHOLANIC ACID

  • Casno:

    4651-67-6

    3ALPHA-HYDROXY-7-OXO-5BETA-CHOLANIC ACID

    Min.Order: 1 Kilogram

    FOB Price:  USD $ 0.0-0.0

    Hangzhou ZeErRui Chemical Co., Ltd. located in Lingang industrial areas, our plant covers an area of 6000 square meters.ZeErRui dedicated to the development, production and marketing of chemicals. We have earned ourselves a good reputation at home an

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  •  Hangzhou ZeErRui Chemical Co., Ltd.

    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-82512721

    Address:No 317,Jingling Road,Guali Town,Xiaoshan District

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