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4651-67-6

Basic Information
CAS No.: 4651-67-6
Name: 3.alpha.-Hydroxy-7-oxo-5.beta.-cholanic acid
Article Data: 70
Cas Database
Molecular Structure:
Molecular Structure of 4651-67-6 (3.alpha.-Hydroxy-7-oxo-5.beta.-cholanic acid)
Formula: C24H38O4
Molecular Weight: 390.563
Synonyms: 3α-Hydroxy-7-keto-5β-cholanic Acid;3ALPHA-HYDROXY-7-OXO-5BETA-CHOLANIC ACID;3α-Hydroxy-7-oxo-5β-cholanic Acid;3a-Hydroxy-7-oxo-5b-cholanic acid;
EINECS: N/A
Density: 1.124g/cm3
Melting Point: 205oC
Boiling Point: 545.9°C at 760 mmHg
Flash Point: 298°C
Solubility: N/A
Appearance: N/A
Hazard Symbols: N/A
Risk Codes: N/A
Safety:
Transport Information: N/A
PSA: 74.60000
LogP: 4.68610
Synthetic route

3α-hydroxy-7-keto-5β-chol-11-en-24-oic acid

4651-67-6

7-Ketolithocholic acid

Conditions
ConditionsYield
With palladium on activated charcoal; hydrogen In methanol at 70℃; under 30003 Torr; for 12h;99%
With palladium on activated charcoal; hydrogen In tetrahydrofuran; methanol at 70℃; under 30003 Torr; for 8h;95%
With palladium on activated charcoal; hydrogen In tetrahydrofuran; methanol at 70℃; under 30003 Torr; for 8h;95%
474-25-9

chenodeoxycholic acid

4651-67-6

7-Ketolithocholic acid

Conditions
ConditionsYield
With dimethyl sulfoxide; triethylamine; trifluoroacetic anhydride In dichloromethane at -30℃; for 1.5h; Temperature; Swern Oxidation;98.6%
With sodium bromate; sulfuric acid; sodium bromide In dichloromethane at 20 - 30℃; for 6h;96.1%
With N-Bromosuccinimide In water; acetone at 20℃; for 2h; Darkness;94%
2646-38-0

sodium chenodeoxycholate

4651-67-6

7-Ketolithocholic acid

Conditions
ConditionsYield
With ethylenediaminetetraacetic acid; Acinetobacter calcoaceticus lwoffii 7α-hydroxysteroid dehydrogenase; sodium pyruvate; NAD; 2-hydroxyethanethiol; lactate dehydrogenase In aq. phosphate buffer at 22℃; pH=8.5; Enzymatic reaction;97%
With Xanthomonas maltophilia BS6 broth In water at 30℃; for 48h;99 % Chromat.

chenodeoxycholic acid

4651-67-6

7-Ketolithocholic acid

Conditions
ConditionsYield
Stage #1: chenodeoxycholic acid With tartaric acid In methanol for 0.5h;
Stage #2: With sodium hypochlorite In methanol at 15 - 22℃; for 1h;
96.1%
10538-59-7

7-ketolithocholic methyl ester

4651-67-6

7-Ketolithocholic acid

Conditions
ConditionsYield
With sodium hydroxide In tetrahydrofuran; methanol for 3h; Reflux;95%
With water; lithium hydroxide In tetrahydrofuran at 20℃; for 4h;74%
With water; sodium hydroxide In methanol for 2h; Solvent; Reflux;32 g
10452-65-0

methyl 3α-acetoxy-7-oxo-5β-cholan-24-oate

4651-67-6

7-Ketolithocholic acid

Conditions
ConditionsYield
With methanol; sodium hydroxide In tetrahydrofuran for 3h; Reflux;95%
With water; sodium hydroxide In ethanol for 2h; Reflux;32 g

C42H52O7

4651-67-6

7-Ketolithocholic acid

Conditions
ConditionsYield
With hydrogen In isopropyl alcohol at 50℃; under 22502.3 Torr; for 24h;95%
With hydrogen In isopropyl alcohol at 50℃; under 22502.3 Torr; for 24h;95%

chenodeoxycholic acid

A

859-97-2

3,7-diketocholanic acid

B

4651-67-6

7-Ketolithocholic acid

Conditions
ConditionsYield
Stage #1: chenodeoxycholic acid With tartaric acid In methanol for 0.5h;
Stage #2: With calcium hypochlorite In methanol at 15 - 22℃; for 1h;
A 5.13%
B 93.3%

C31H42O4

4651-67-6

7-Ketolithocholic acid

Conditions
ConditionsYield
With palladium on activated charcoal; hydrogen In tetrahydrofuran; methanol at 70℃; under 30003 Torr; for 8h;90%
With palladium on activated charcoal; hydrogen In tetrahydrofuran; methanol at 70℃; under 30003 Torr; for 8h;90%
474-25-9

chenodeoxycholic acid

A

859-97-2

3,7-diketocholanic acid

B

4651-67-6

7-Ketolithocholic acid

Conditions
ConditionsYield
With sodium bromate; ammonium cerium (IV) nitrate In water; acetonitrile at 60℃; for 0.5h; Green chemistry;A 9%
B 83%
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    High quality 99% 3-alpha-hydroxy-7-oxo-5-beta-cholan-24-oic acid CAS No.4651-67-6

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     China (Mainland)  |  Contact Details

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    3ALPHA-HYDROXY-7-OXO-5BETA-CHOLANICACID 4651-67-6

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    The company is a high-tech enterprise providing comprehensive customer service for pharmaceutical companies at home and abroad in accordance with international standards. Our business includes research, development, process optimization and productio

    Prime Molecular Co., Ltd. is an advanced chemical intermediates manufacture with ?two R&D centers and two production sites in China, all well-equipped with dedicated and profession

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    Business Type:Trading Company

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    Address:Hong Kong

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  • 7-KETOLITHOCHOLIC ACID

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    4651-67-6

    7-KETOLITHOCHOLIC ACID

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    Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments

    AFINE CHEMICALS LIMITED is specialized in the fine chemicals and pharmaceuticals and we have enjoyed great popularity in world markets. Since 2005, we have been rapidly growing to

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-85134551

    Address:No. 206 Zhen Hua Road, Hangzhou 310030, Zhejiang, China

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    4651-67-6

    3.alpha.-Hydroxy-7-oxo-5.beta.-cholanic acid

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-87396432

    Address:No.200 Zhenhua Rd.Xihu Industrial Park, Hangzhou 310030, China

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    4651-67-6

    3-Hydroxy-7-oxocholan-24-oic acid

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    HangYu Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. HangYu Chemical consis

    Zibo HangYu Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals

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    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-15988566987

    Address:Room1701, Tianxing Building,Licheng district, jinan, Shandong, China

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    4651-67-6

    3a-hydroxy-7-oxo-5b-cholanic/High quality/Best price

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86 21 34943721

    Address:Room 435, 4th floor, Building 9, No. 2568 Gudai Road,Minhang District, Shanghai,

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    -3ALPHA-HYDROXY-7-OXO-5BETA-CHOLANIC ACID CAS NO.4651-67-6

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    Changchun Haofei Import and Export Trade Co. , Ltd is located in Changchun, Changchun, Jilin Province. We are a modern high-tech private enterprise specializing in the R & D, Produ

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    Business Type:Trading Company

    Tel:+8615643102578

    Address:Guanghui Park, Huanghe Road, Kuancheng District

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    3-alpha-hydroxy-7-oxo-5-beta-cholan-24-oic acid

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    Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as

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  •  Hunan chemfish Pharmaceutical co.,Ltd

     China (Mainland)  |  Contact Details

    Business Type:Manufacturers

    Tel:0731-85567275

    Address:No.10048, xiangjiang centry bulding ,kaifu district ,changsha city ,Hunan

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  • Supply CAS 4651-67-6  7-oxolithocholic acid

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    Supply CAS 4651-67-6 7-oxolithocholic acid

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    Xi’an JunYuan Biotech Co., Ltd., which is specialized in fine chemicals research, production and sales. It has strong professional research and development team, talented personne

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     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86-29-86106815

    Address:Block C of XINJIE, No. 398, Fengcheng 6 Road, Xi'an Economic & Technological Development Zone

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  • Casno:

    4651-67-6

    3α-Hydroxy-7-Oxo-5β-Cholanic Acid/Factory in stock-SCZK

    Min.Order: 10 Gram

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    Shenzhen Tianyuan Pharmaceutical Technology Co., Ltd. is a manufacturer specializing in targeted anticancer drug research and is devoted to researching, manufacturing and marketing medical raw materials. Tianyuan pharmaceutical company in Zhangjiang

    Tianyuan pharmaceutical company in Zhangjiang Eastern has built 500 square meters of pilot laboratories, equipped with two sets of 50L glass reactor, four sets of 100L double react

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-755-23284190

    Address:B302,2 unit, Jin Lian Building, No. 134 Qianjin 2 Road, Taoyuan village, Xixiang Street, Baoan,Shenzhen,China

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