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4698-11-7

Basic Information
CAS No.: 4698-11-7
Name: 10-Methoxyiminostilbene
Article Data: 19
Molecular Structure:
Molecular Structure of 4698-11-7 (10-Methoxyiminostilbene)
Formula: C15H13NO
Molecular Weight: 223.274
Synonyms: 10-Oxo-10,11-dihydro-5H-dibenzo[b,f]azepine-5-carboxamide;10-Methoxy-5H-dibenz(b,f)azepine;
EINECS: 225-172-6
Density: 1.19 g/cm3
Melting Point: 122-128 °C
Boiling Point: 410.8 °C at 760 mmHg
Flash Point: 162.5 °C
Appearance: Yellowish foam
PSA: 21.26000
LogP: 4.02610
Synthetic route
353497-37-7

10-methoxy-5H-dibenz[b,f]azepine-5-carboxylic acid methyl ester

4698-11-7

10-methoxy-5H-dibenzo[b,f]azepine

Conditions
ConditionsYield
With sodium hydroxide In various solvent(s) at 100℃; for 4h;98%
With sodium hydroxide In water98%
With sodium hydroxide In methanol; water at 105 - 110℃; for 2.5h;97%
731851-94-8

10-methoxy-dibenzo[b,f]azepine-5-carboxylic acid phenyl ester

4698-11-7

10-methoxy-5H-dibenzo[b,f]azepine

Conditions
ConditionsYield
With sodium hydroxide In various solvent(s) at 100℃; for 4h;96%
10465-66-4

5-benzyl-10-methoxyiminostilbene

4698-11-7

10-methoxy-5H-dibenzo[b,f]azepine

Conditions
ConditionsYield
With 5%-palladium/activated carbon; hydrogen at 35 - 40℃; under 1500.15 - 2250.23 Torr; for 5h; Autoclave;93.5%
153261-62-2

5-acetyl-10-methoxy-5H-dibenzazepine

4698-11-7

10-methoxy-5H-dibenzo[b,f]azepine

Conditions
ConditionsYield
With potassium hydroxide In ethylene glycol for 5h; Heating;80%
With triethyl borane; sodium hydroxide In tert-butyl methyl ether at 80℃; for 6h; Inert atmosphere; Sealed tube;67%
Stage #1: 5-acetyl-10-methoxy-5H-dibenzazepine With Triethoxysilane; sodium triethylborohydride In tert-butyl methyl ether at 80℃; for 6h;
Stage #2: With hydrogenchloride In tert-butyl methyl ether; water at 20℃; for 1h; chemoselective reaction;
59%

5-allyl-10-methoxy-5H-dibenzo[b,f]azepine

4698-11-7

10-methoxy-5H-dibenzo[b,f]azepine

Conditions
ConditionsYield
With potassium tert-butylate In dimethyl sulfoxide

5-formyl-10-bromo-11-methoxy-10,11-dihydro-5H-dibenzo[b,f]azepine

4698-11-7

10-methoxy-5H-dibenzo[b,f]azepine

Conditions
ConditionsYield
Stage #1: 5-formyl-10-bromo-11-methoxy-10,11-dihydro-5H-dibenzo[b,f]azepine With 1,8-diazabicyclo[5.4.0]undec-7-ene In toluene for 0.5h; Heating / reflux;
Stage #2: With Deloxan ASP I/7; potassium hydroxide In toluene Product distribution / selectivity; Heating / reflux;
39507-06-7

(2-phenylamino-phenyl)-acetic acid methyl ester

4698-11-7

10-methoxy-5H-dibenzo[b,f]azepine

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: pyridine / toluene / 24 h / 50 °C
1.2: pyridine / 22 h / 100 °C
2.1: 90 percent / aq. NaOH / methanol / 24 h / 25 °C
3.1: 70 percent / polyphosphoric acid / 3 h / 95 °C
4.1: 81 percent / p-TsOH / methanol / 5 h / Heating
5.1: 98 percent / aq. NaOH / various solvent(s) / 4 h / 100 °C
View Scheme
Multi-step reaction with 6 steps
1: pyridine / toluene / 24 h / 50 °C
2: pyridine / 22 h / 100 °C
3: sodium hydroxide / water; methanol / 24 h / 20 °C
4: polyphosphoric acid / 3 h / 90 - 95 °C
5: water / 0 - 98 °C
6: sodium hydroxide / water; methanol / 2.5 h / 105 - 110 °C
View Scheme
353497-31-1

10,11-dihydro-10-oxo-5H-dibenz[b,f]azepine-5-carboxylic acid methyl ester

4698-11-7

10-methoxy-5H-dibenzo[b,f]azepine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 81 percent / p-TsOH / methanol / 5 h / Heating
2: 98 percent / aq. NaOH / various solvent(s) / 4 h / 100 °C
View Scheme
Multi-step reaction with 2 steps
1: water / 0 - 98 °C
2: sodium hydroxide / water; methanol / 2.5 h / 105 - 110 °C
View Scheme
805236-74-2

[2-(methoxycarbonyl-phenyl-amino)-phenyl]-acetic acid methyl ester

4698-11-7

10-methoxy-5H-dibenzo[b,f]azepine

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 90 percent / aq. NaOH / methanol / 24 h / 25 °C
2: 70 percent / polyphosphoric acid / 3 h / 95 °C
3: 81 percent / p-TsOH / methanol / 5 h / Heating
4: 98 percent / aq. NaOH / various solvent(s) / 4 h / 100 °C
View Scheme
Multi-step reaction with 4 steps
1: sodium hydroxide / water; methanol / 24 h / 20 °C
2: polyphosphoric acid / 3 h / 90 - 95 °C
3: water / 0 - 98 °C
4: sodium hydroxide / water; methanol / 2.5 h / 105 - 110 °C
View Scheme
353497-35-5

2-[(methoxycarbonyl)phenylamino]benzeneacetic acid

4698-11-7

10-methoxy-5H-dibenzo[b,f]azepine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 70 percent / polyphosphoric acid / 3 h / 95 °C
2: 81 percent / p-TsOH / methanol / 5 h / Heating
3: 98 percent / aq. NaOH / various solvent(s) / 4 h / 100 °C
View Scheme
Multi-step reaction with 3 steps
1: polyphosphoric acid / 3 h / 90 - 95 °C
2: water / 0 - 98 °C
3: sodium hydroxide / water; methanol / 2.5 h / 105 - 110 °C
View Scheme
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    Product name: 10-Methoxy Iminostilbene CAS No.:4698-11-7 Molecule Formula:C15H13NO Molecule Weight:223.27 Purity: 99.0% Package: 25kg/drum Description:Bright yellow crystalline powder Manufacture Standards:Enterprise Standard

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Chemistry

Molecular Structure of 10-Methoxy-5H-dibenz(b,f)azepine (CAS NO.4698-11-7):

Molecular Formula: C15H13NO
Molecular Weight: 223.2698
IUPAC Name: 6-Methoxy-11H-benzo[b][1]benzazepine
Synonyms of 10-Methoxy-5H-dibenz(b,f)azepine (CAS NO.4698-11-7): EINECS 225-172-6 ; 10-Methoxyiminostilbene ; 10-Methoxy-2,2'-iminostilbene
CAS NO: 4698-11-7
Product Categories: Stilbenes (substituted) ; Aromatics Compounds ; Aromatics ; Heterocycles
Melting point: 122-128°C 
Index of Refraction: 1.651
Molar Refractivity: 68.37 cm3
Molar Volume: 187 cm3
Surface Tension: 49.8 dyne/cm
Density: 1.19 g/cm3
Flash Point: 162.5 °C
Enthalpy of Vaporization: 66.32 kJ/mol
Boiling Point: 410.8 °C at 760 mmHg
Vapour Pressure of 10-Methoxy-5H-dibenz(b,f)azepine (CAS NO.4698-11-7): 5.86E-07 mmHg at 25°C

Uses

 10-Methoxy-5H-dibenz(b,f)azepine (CAS NO.4698-11-7) is used as Drug Oxcarbazepine.