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498-45-3

Basic Information
CAS No.: 498-45-3
Name: 3-Oxa-9-azatricyclo[3.3.1.02,4]nonan-7-ol,9-methyl-, (1a,2b,4b,5a,7b)-
Molecular Structure:
Molecular Structure of 498-45-3 (3-Oxa-9-azatricyclo[3.3.1.02,4]nonan-7-ol,9-methyl-, (1a,2b,4b,5a,7b)-)
Formula: C8H13NO2
Molecular Weight: 155.20
Synonyms: 1aH,5aH-Tropan-3a-ol, 6b,7b-epoxy- (8CI);Scopine (6CI,7CI);6,7-Epoxytropine;Scopanol;Scopin;Scopine;
EINECS: 102-503-4
Density: 1.284 g/cm3
Melting Point: 73.0 to 77.0 °C
Boiling Point: 281.3oC at 760 mmHg
Flash Point: 123.9oC
Solubility:
Appearance:
Hazard Symbols:
Risk Codes:
Safety:
Transport Information:
PSA: 36.00000
LogP: -0.47100
Synthetic route
Conditions
ConditionsYield
With 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine In toluene at 25℃; for 48h;99.3%
Stage #1: scopolamine With sodium tetrahydroborate In ethanol at 0 - 20℃; for 24h;
Stage #2: With hydrogenchloride In diethyl ether; ethanol at 20℃; for 24h;
50%
With ammonium chloride; ammonia at 30℃;
114-49-8

hyoscine hydrobromide

498-45-3

scopine

Conditions
ConditionsYield
With sodium tetrahydroborate In ethanol at 20℃; Cooling with ice;87%
182054-94-0

scopine t-butyldimethylsilyl ether

498-45-3

scopine

Conditions
ConditionsYield
With tert-butyl-ammonium fluoride82%
With tetrabutyl ammonium fluoride In tetrahydrofuran for 18h;81%
132622-34-5, 132697-33-7

scopine benzyl ether

498-45-3

scopine

Conditions
ConditionsYield
With hydrogenchloride; hydrogen; potassium carbonate; palladium on activated charcoal 1) EtOH, 5 atm, r.t, 12h; Yield given. Multistep reaction;
(-)-scopolamine

(-)-scopolamine

498-45-3

scopine

Conditions
ConditionsYield
With NH3-NH4Cl-buffer solution
With bis-1-chloroethyl ether anschliessende Hydrolyse mit wss. Ba(OH)2 und dann mit wss. HCl;
O-acetyl-scopine

O-acetyl-scopine

498-45-3

scopine

Conditions
ConditionsYield
With sodium hydroxide; acetone
33250-14-5

Tropilidenoxid

498-45-3

scopine

Conditions
ConditionsYield
Multi-step reaction with 8 steps
1: LiAlH4 / diethyl ether / 1 h
2: Me4N(1+)IO4(1-) / CH2Cl2
3: 1.) Me4N(1+)*IO4(1-), 2.) Imidazole, 3.) Na(Hg), Na3PO4, 4.) MCPBA
4: 1.) n-BuLi / 1.) THF, hexane, 0 deg C, 10 min, 2.) THF, hexane, RT, 1.5 h
5: 64 percent / LiCl / dimethylsulfoxide / 1.5 h / 55 °C
6: 82 percent / NaH / tetrahydrofuran; 1,2-dimethoxy-ethane / 3 h / 20 - 50 °C
7: 95 percent / LiAlH4 / diethyl ether / 2 h / Heating
8: 81 percent / TBAF / tetrahydrofuran / 18 h
View Scheme
1121-63-7

cyclohepta-3,5-dien-1-ol

498-45-3

scopine

Conditions
ConditionsYield
Multi-step reaction with 7 steps
1: Me4N(1+)IO4(1-) / CH2Cl2
2: 1.) Me4N(1+)*IO4(1-), 2.) Imidazole, 3.) Na(Hg), Na3PO4, 4.) MCPBA
3: 1.) n-BuLi / 1.) THF, hexane, 0 deg C, 10 min, 2.) THF, hexane, RT, 1.5 h
4: 64 percent / LiCl / dimethylsulfoxide / 1.5 h / 55 °C
5: 82 percent / NaH / tetrahydrofuran; 1,2-dimethoxy-ethane / 3 h / 20 - 50 °C
6: 95 percent / LiAlH4 / diethyl ether / 2 h / Heating
7: 81 percent / TBAF / tetrahydrofuran / 18 h
View Scheme
Multi-step reaction with 9 steps
1: NaH / tetrahydrofuran / 15 h / 50 °C
2: 63 percent / LiCl, p-benzoquinone, glacial acetic acid / Pd(OAc)2 / acetic acid / 36 h
3: 96 percent / DIBAL / tetrahydrofuran; hexane / 0.75 h / 2 °C
4: 66 percent / Pd(PPh3)4 / acetonitrile / 4 h
5: 76 percent / LiCl, MsCl, 2,4,6-trimethylpyridine / dimethylformamide / 0 deg C to r.t., overnight
6: 86 percent / m-CPBA / CH2Cl2 / 48 h / Ambient temperature
7: 95 percent / K2CO3 / methanol / 56 h / Ambient temperature
8: 1) naphthalene, Na / 1) THF, -78 deg C, 30 min
9: 1) aq.2M HCl, H2, 2) 10percent aq. K2CO3 / 1) 10percent Pd/C / 1) EtOH, 5 atm, r.t, 12h
View Scheme
544-25-2

Cyclohepta-1,3,5-triene

norcaradiene-(2.4)

norcaradiene-(2.4)

498-45-3

scopine

Conditions
ConditionsYield
Multi-step reaction with 9 steps
1: aq. CH3COOOH, Na2CO3 / CH2Cl2 / 3 h / 0 °C
2: LiAlH4 / diethyl ether / 1 h
3: Me4N(1+)IO4(1-) / CH2Cl2
4: 1.) Me4N(1+)*IO4(1-), 2.) Imidazole, 3.) Na(Hg), Na3PO4, 4.) MCPBA
5: 1.) n-BuLi / 1.) THF, hexane, 0 deg C, 10 min, 2.) THF, hexane, RT, 1.5 h
6: 64 percent / LiCl / dimethylsulfoxide / 1.5 h / 55 °C
7: 82 percent / NaH / tetrahydrofuran; 1,2-dimethoxy-ethane / 3 h / 20 - 50 °C
8: 95 percent / LiAlH4 / diethyl ether / 2 h / Heating
9: 81 percent / TBAF / tetrahydrofuran / 18 h
View Scheme

1β-hydroxy-4β-<(benzyloxycarbonyl)amino>-6-<(t-butyldimethylsilyl)oxy>cyclohept-2-ene

498-45-3

scopine

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1: 68 percent / MCPBA / CH2Cl2 / 3 h / Ambient temperature
2: 1.) n-BuLi / 1.) THF, hexane, 0 deg C, 10 min, 2.) THF, hexane, RT, 1.5 h
3: 64 percent / LiCl / dimethylsulfoxide / 1.5 h / 55 °C
4: 82 percent / NaH / tetrahydrofuran; 1,2-dimethoxy-ethane / 3 h / 20 - 50 °C
5: 95 percent / LiAlH4 / diethyl ether / 2 h / Heating
6: 81 percent / TBAF / tetrahydrofuran / 18 h
View Scheme
Multi-step reaction with 6 steps
1: MCPBA / CH2Cl2 / 3 h / Ambient temperature
2: 1.) n-BuLi / 1.) THF, hexane, 0 deg C, 10 min, 2.) THF, hexane, RT, 1.5 h
3: 64 percent / LiCl / dimethylsulfoxide / 1.5 h / 55 °C
4: 82 percent / NaH / tetrahydrofuran; 1,2-dimethoxy-ethane / 3 h / 20 - 50 °C
5: 95 percent / LiAlH4 / diethyl ether / 2 h / Heating
6: 81 percent / TBAF / tetrahydrofuran / 18 h
View Scheme
182054-91-7

N-benzyloxycarbonyl-3α-<(t-butyldimethylsilyl)oxy>-6β,7β-epoxy-8-azabicyclo<3.2.1>octane

498-45-3

scopine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 95 percent / LiAlH4 / diethyl ether / 2 h / Heating
2: 81 percent / TBAF / tetrahydrofuran / 18 h
View Scheme

1β-hydroxy-2β,3β-epoxy-4β-<(benzyloxycarbonyl)amino>-6α-<(t-butyldimethylsilyl)oxy>cycloheptane

498-45-3

scopine

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: 1.) n-BuLi / 1.) THF, hexane, 0 deg C, 10 min, 2.) THF, hexane, RT, 1.5 h
2: 64 percent / LiCl / dimethylsulfoxide / 1.5 h / 55 °C
3: 82 percent / NaH / tetrahydrofuran; 1,2-dimethoxy-ethane / 3 h / 20 - 50 °C
4: 95 percent / LiAlH4 / diethyl ether / 2 h / Heating
5: 81 percent / TBAF / tetrahydrofuran / 18 h
View Scheme

1α-chloro-2β,3β-epoxy-4β-<(benzyloxycarbonyl)amino>-6α-<(t-butyldimethylsilyl)oxy>cycloheptane

498-45-3

scopine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 82 percent / NaH / tetrahydrofuran; 1,2-dimethoxy-ethane / 3 h / 20 - 50 °C
2: 95 percent / LiAlH4 / diethyl ether / 2 h / Heating
3: 81 percent / TBAF / tetrahydrofuran / 18 h
View Scheme

1β-<(p-toluenesulphonyl)oxy>-2β,3β-epoxy-4β-<(benzyloxycarbonyl)amino>-6α-<(t-butyldimethylsilyl)oxy>cycloheptane

498-45-3

scopine

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 64 percent / LiCl / dimethylsulfoxide / 1.5 h / 55 °C
2: 82 percent / NaH / tetrahydrofuran; 1,2-dimethoxy-ethane / 3 h / 20 - 50 °C
3: 95 percent / LiAlH4 / diethyl ether / 2 h / Heating
4: 81 percent / TBAF / tetrahydrofuran / 18 h
View Scheme

N-benzyloxycarbonyl-3α-hydroxy-6-aza-7-oxabicyclo[3.2.2]non-8-ene

498-45-3

scopine

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1: 1.) Me4N(1+)*IO4(1-), 2.) Imidazole, 3.) Na(Hg), Na3PO4, 4.) MCPBA
2: 1.) n-BuLi / 1.) THF, hexane, 0 deg C, 10 min, 2.) THF, hexane, RT, 1.5 h
3: 64 percent / LiCl / dimethylsulfoxide / 1.5 h / 55 °C
4: 82 percent / NaH / tetrahydrofuran; 1,2-dimethoxy-ethane / 3 h / 20 - 50 °C
5: 95 percent / LiAlH4 / diethyl ether / 2 h / Heating
6: 81 percent / TBAF / tetrahydrofuran / 18 h
View Scheme
115522-58-2

6-(benzyloxy)-1,3-cycloheptadiene

498-45-3

scopine

Conditions
ConditionsYield
Multi-step reaction with 8 steps
1: 63 percent / LiCl, p-benzoquinone, glacial acetic acid / Pd(OAc)2 / acetic acid / 36 h
2: 96 percent / DIBAL / tetrahydrofuran; hexane / 0.75 h / 2 °C
3: 66 percent / Pd(PPh3)4 / acetonitrile / 4 h
4: 76 percent / LiCl, MsCl, 2,4,6-trimethylpyridine / dimethylformamide / 0 deg C to r.t., overnight
5: 86 percent / m-CPBA / CH2Cl2 / 48 h / Ambient temperature
6: 95 percent / K2CO3 / methanol / 56 h / Ambient temperature
7: 1) naphthalene, Na / 1) THF, -78 deg C, 30 min
8: 1) aq.2M HCl, H2, 2) 10percent aq. K2CO3 / 1) 10percent Pd/C / 1) EtOH, 5 atm, r.t, 12h
View Scheme
132622-29-8

1β-hydroxy-4β-chloro-6α-(benzyloxy)-2-cycloheptene

498-45-3

scopine

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1: 66 percent / Pd(PPh3)4 / acetonitrile / 4 h
2: 76 percent / LiCl, MsCl, 2,4,6-trimethylpyridine / dimethylformamide / 0 deg C to r.t., overnight
3: 86 percent / m-CPBA / CH2Cl2 / 48 h / Ambient temperature
4: 95 percent / K2CO3 / methanol / 56 h / Ambient temperature
5: 1) naphthalene, Na / 1) THF, -78 deg C, 30 min
6: 1) aq.2M HCl, H2, 2) 10percent aq. K2CO3 / 1) 10percent Pd/C / 1) EtOH, 5 atm, r.t, 12h
View Scheme
115522-57-1, 150338-86-6

1β-acetoxy-4β-chloro-6α-(benzyloxy)-2-cycloheptene

498-45-3

scopine

Conditions
ConditionsYield
Multi-step reaction with 7 steps
1: 96 percent / DIBAL / tetrahydrofuran; hexane / 0.75 h / 2 °C
2: 66 percent / Pd(PPh3)4 / acetonitrile / 4 h
3: 76 percent / LiCl, MsCl, 2,4,6-trimethylpyridine / dimethylformamide / 0 deg C to r.t., overnight
4: 86 percent / m-CPBA / CH2Cl2 / 48 h / Ambient temperature
5: 95 percent / K2CO3 / methanol / 56 h / Ambient temperature
6: 1) naphthalene, Na / 1) THF, -78 deg C, 30 min
7: 1) aq.2M HCl, H2, 2) 10percent aq. K2CO3 / 1) 10percent Pd/C / 1) EtOH, 5 atm, r.t, 12h
View Scheme
132622-31-2, 132697-30-4

1β-(p-toluenesulfonamido)-4-chloro-6α-(benzyloxy)-2-cycloheptene

498-45-3

scopine

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 86 percent / m-CPBA / CH2Cl2 / 48 h / Ambient temperature
2: 95 percent / K2CO3 / methanol / 56 h / Ambient temperature
3: 1) naphthalene, Na / 1) THF, -78 deg C, 30 min
4: 1) aq.2M HCl, H2, 2) 10percent aq. K2CO3 / 1) 10percent Pd/C / 1) EtOH, 5 atm, r.t, 12h
View Scheme
132622-32-3

1β-(p-toluenesulfonamido)-2β,3β-epoxy-4α-chloro-6α-(benzyloxy)-2-cycloheptene

498-45-3

scopine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 95 percent / K2CO3 / methanol / 56 h / Ambient temperature
2: 1) naphthalene, Na / 1) THF, -78 deg C, 30 min
3: 1) aq.2M HCl, H2, 2) 10percent aq. K2CO3 / 1) 10percent Pd/C / 1) EtOH, 5 atm, r.t, 12h
View Scheme
132622-30-1, 132697-31-5

1β-(p-toluenesulfonamido)-4β-hydroxy-6α-(benzyloxy)-2-cycloheptene

498-45-3

scopine

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: 76 percent / LiCl, MsCl, 2,4,6-trimethylpyridine / dimethylformamide / 0 deg C to r.t., overnight
2: 86 percent / m-CPBA / CH2Cl2 / 48 h / Ambient temperature
3: 95 percent / K2CO3 / methanol / 56 h / Ambient temperature
4: 1) naphthalene, Na / 1) THF, -78 deg C, 30 min
5: 1) aq.2M HCl, H2, 2) 10percent aq. K2CO3 / 1) 10percent Pd/C / 1) EtOH, 5 atm, r.t, 12h
View Scheme
132622-33-4, 132697-32-6

3α-(benzyloxy)-6β,7β-epoxy-8-(p-toluenesulfonyl)-1β-azabicyclo<3.2.1>octane

498-45-3

scopine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 1) naphthalene, Na / 1) THF, -78 deg C, 30 min
2: 1) aq.2M HCl, H2, 2) 10percent aq. K2CO3 / 1) 10percent Pd/C / 1) EtOH, 5 atm, r.t, 12h
View Scheme
149-64-4

hyoscine-N-butyl bromide

498-45-3

scopine

Conditions
ConditionsYield
With ruthenium trichloride; potassium metaperiodate; diperiodatocuprate(III) dihydrate; water; potassium nitrate; potassium hydroxide at 28℃; for 6h; Kinetics; Catalytic behavior; Concentration; Temperature; Inert atmosphere;
498-45-3

scopine

74-88-4

methyl iodide

21662-36-2

(1R,2R,4S,5S,7S)-7-hydroxy-9,9-dimethyl-3-oxa-9-azatricyclo[3.3.1.02,4]nonan-9-iumiodide (N-methylscopinium)

Conditions
ConditionsYield
In dichloromethane at 20℃; for 48h; Inert atmosphere;85%
4408-82-6

2,2-di(thiophen-2-yl)acetic acid

498-45-3

scopine

1336913-21-3

C18H19NO3S2

Conditions
ConditionsYield
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 16h; Product distribution / selectivity;83%
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 16h; Reagent/catalyst; Solvent; Concentration;83%
With dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 16h; Product distribution / selectivity;
498-45-3

scopine

305-03-3

chlorambucil

C22H30Cl2N2O3

Conditions
ConditionsYield
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 4h;82.3%
26447-85-8

hydroxy-di-thiophen-2-yl-acetic acid methyl ester

498-45-3

scopine

136310-64-0

N-demethyltiotropium

Conditions
ConditionsYield
With potassium tert-butylate; 1-butyl-3-methylimidazolium Tetrafluoroborate In tetrahydrofuran at 20℃; for 18h; Solvent; Concentration; Reagent/catalyst; Temperature; Time; Molecular sieve;73%
Stage #1: hydroxy-di-thiophen-2-yl-acetic acid methyl ester; scopine at 70℃; under 210 Torr; for 1h;
Stage #2: With sodium hydride at 70℃; under 210 Torr; for 3h;
42%
With sodium hydride In toluene; mineral oil at 90℃; for 2h;33%
With potassium carbonate In 1-methyl-pyrrolidin-2-one at 70℃; under 15.0015 Torr; for 19h;
65-85-0

benzoic acid

498-45-3

scopine

(1R,2R,4S,5S,7r)-9-methyl-3-oxa-9-azatricyclo[3.3.1.02,4]nonan-7-yl benzoate

Conditions
ConditionsYield
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at -35 - 20℃;67.9%
26447-85-8

hydroxy-di-thiophen-2-yl-acetic acid methyl ester

498-45-3

scopine

A

136310-64-0

N-demethyltiotropium

B

scopoline

C

di-(2-thienyl)glycolic acid scopoline ester

Conditions
ConditionsYield
Stage #1: hydroxy-di-thiophen-2-yl-acetic acid methyl ester; scopine With sodium t-butanolate In tetrahydrofuran; toluene at 70 - 90℃; under 375.038 Torr; for 4.41667h; Inert atmosphere;
Stage #2: With hydrogenchloride In dichloromethane; water Cooling with ice;
Stage #3: With sodium carbonate In water Reagent/catalyst; Solvent; Time; Temperature; Pressure; Concentration; Overall yield = 37.2 g;
A 58%
B 5.3 %Chromat.
C 6.1 %Chromat.
Stage #1: hydroxy-di-thiophen-2-yl-acetic acid methyl ester; scopine With potassium tert-butylate In toluene at 70 - 90℃; under 225.023 - 300.03 Torr; for 4.25h; Inert atmosphere;
Stage #2: With hydrogenchloride In dichloromethane; water Cooling with ice;
Stage #3: With sodium carbonate In water Reagent/catalyst; Temperature; Time; Overall yield = 0.82 g;
A 41%
B 18.4 %Chromat.
C 5.6 %Chromat.
Stage #1: hydroxy-di-thiophen-2-yl-acetic acid methyl ester; scopine With sodium hydride In toluene; mineral oil at 70 - 90℃; under 225.023 - 300.03 Torr; for 4.25h; Inert atmosphere;
Stage #2: With hydrogenchloride In water; toluene; mineral oil Cooling with ice;
Stage #3: With sodium carbonate In water Overall yield = 1.01 g;
A 21%
B 35.7 %Chromat.
C 30.4 %Chromat.
40997-78-2

2,2-diphenylpropionyl chloride

498-45-3

scopine

scopine 2,2-diphenylpropionate

Conditions
ConditionsYield
In dichloromethane at 40℃; for 24h;47%
26447-85-8

hydroxy-di-thiophen-2-yl-acetic acid methyl ester

498-45-3

scopine

A

136310-64-0

N-demethyltiotropium

B

scopoline

Conditions
ConditionsYield
Stage #1: hydroxy-di-thiophen-2-yl-acetic acid methyl ester; scopine With sodium t-butanolate In toluene at 70 - 90℃; under 225.023 - 300.03 Torr; for 4.25h; Inert atmosphere;
Stage #2: With hydrogenchloride In dichloromethane; water Cooling with ice;
Stage #3: With sodium carbonate In water Time; Concentration;
A 33%
B 26.3 %Chromat.
Stage #1: hydroxy-di-thiophen-2-yl-acetic acid methyl ester; scopine With sodium methylate In toluene at 70 - 90℃; under 75.0075 - 225.023 Torr; for 5.25h; Inert atmosphere;
Stage #2: With hydrogenchloride In water; toluene Cooling with ice;
Stage #3: With sodium carbonate In water
A 11.6 %Chromat.
B 57.3 %Chromat.
32315-10-9

bis(trichloromethyl) carbonate

1717-22-2

2-amino-5-fluorobiphenyl

498-45-3

scopine

(1R,2R,4S,5S,7s,9r)-7-(((5-fluorobiphenyl-2-yl)carbamoyl)oxy)-9-methyl-3-oxa-9-azatricyclo[3.3.1.02,4]nonan-9-ium chloride

Conditions
ConditionsYield
Stage #1: bis(trichloromethyl) carbonate; scopine In acetonitrile at 0 - 20℃; for 36h;
Stage #2: 2-amino-5-fluorobiphenyl With pyridine at 60℃; for 24h;
8%
1140-33-6

1-chloro-4-(diazo(phenyl)methyl)benzene

498-45-3

scopine

116603-25-9

7t-(4-chloro-benzhydryloxy)-9-methyl-(1rN,2tH,4tH,5cN)-3-oxa-9-aza-tricyclo[3.3.1.02,4]nonane

Conditions
ConditionsYield
In benzene at 95 - 100℃; for 5.5h;
908093-98-1

diazodiphenylmethane

498-45-3

scopine

112018-04-9

7t-benzhydryloxy-9-methyl-(1rN,2tH,4tH,5cN)-3-oxa-9-aza-tricyclo[3.3.1.02,4]nonane

Conditions
ConditionsYield
In benzene at 80 - 85℃; for 3h;
14510-37-3

3-acetoxy-2-phenyl-propionyl chloride

98-95-3

nitrobenzene

498-45-3

scopine

(+-)-O-acetyl-scopolamine hydrochloride

(+-)-O-acetyl-scopolamine hydrochloride

110-86-1

pyridine

498-45-3

scopine

CrO3

CrO3

A

498-47-5

6exo,7exo-epoxy-tropan-3-one

B

(+-)-N-formyl-norscopolin

(+-)-N-formyl-norscopolin

498-45-3

scopine

dl-scopolin

dl-scopolin

Conditions
ConditionsYield
bei der Destillation;
498-45-3

scopine

Cr2O3-H2SO4

Cr2O3-H2SO4

dl-scopolin

dl-scopolin

Conditions
ConditionsYield
at 50 - 60℃;
498-45-3

scopine

n KOH-solution

n KOH-solution

dl-scopolin

dl-scopolin

Conditions
ConditionsYield
at 20℃;
14510-37-3

3-acetoxy-2-phenyl-propionyl chloride

98-95-3

nitrobenzene

498-45-3

scopine

O-<3-acetoxy-2-phenyl-propionyl>-scopolamine hydrochloride

O-<3-acetoxy-2-phenyl-propionyl>-scopolamine hydrochloride

14510-37-3

3-acetoxy-2-phenyl-propionyl chloride

498-45-3

scopine

A

O-acetyl-scopine hydrochloride

O-acetyl-scopine hydrochloride

B

O-<3-acetoxy-2-phenyl>-propionyl>-scopolamine hydrochloride

O-<3-acetoxy-2-phenyl>-propionyl>-scopolamine hydrochloride

498-45-3

scopine

salts of scopolin

salts of scopolin

7790-94-5

chlorosulfonic acid

498-45-3

scopine

A

scopinesulfuric acid

scopinesulfuric acid

B

dl-scopolinsulfuric acid

dl-scopolinsulfuric acid

Downstream Products
139404-48-1
136310-64-0
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  • (1R,2R,4S,5S,7s)-9-Methyl-3-oxa-9-azatricyclo[3.3.1.02,4]nonan-7-ol

  • Casno:

    498-45-3

    (1R,2R,4S,5S,7s)-9-Methyl-3-oxa-9-azatricyclo[3.3.1.02,4]nonan-7-ol

    Min.Order: 20 Kilogram

    FOB Price:  USD $ 2000.0-2000.0/Kilogram

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    Business Type:Manufacturers

    Tel:86-0311-66561638

    Address:Zhang zhe, guangzong county, xingtai city, hebei province

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    498-45-3

    Scopine

    Min.Order: 10 Milligram

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    Business Type:Lab/Research institutions

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    498-45-3

    Scopine

    Min.Order: 1 Gram

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    Business Type:Manufacturers

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  • Casno:

    498-45-3

    Scopine

    Min.Order: 0

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    498-45-3

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    Business Type:Lab/Research institutions

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    Address:9/F, Unit 2 Changdi Torch Building, 259# WenSan Road, Xihu District, Hangzhou City 310012, P.R.China

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    498-45-3

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    Min.Order: 1 Gram

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    Scopine Basic information Product Name: Scopine Synonyms: SCOPINE;(1alpha,2beta,4beta,5alpha,7beta)-9-Methyl-3-oxa-9-azatricyclo[3.3.1.02.4]nonan-7-ol;SCOPINE, 97+%;(1α,2β,4β,5α)-9-Methyl-3-oxa-9-azatricyclo[3.3.1.02,4]non

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    Address:Fine chemical industry park, Nantong,Jiangsu

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  • 498-45-3

  • Casno:

    498-45-3

    498-45-3

    Min.Order: 1 Kilogram

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-371-55170693/55170694

    Address:Zhengzhou International Trade New Territory,Jinshui District,Zhengzhou ,China

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    498-45-3

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    Zhuo Zhou Wen Xi Import and Export Co., Ltd. is a company mainly engaged in the export of pharmaceutical raw materials. Its parent company is (Wen Xi Pharma), including three subs

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    Business Type:Trading Company

    Tel:+86-13111626072

    Address:Room 1710, Baoxin International Phase I, 19 Guanyun East Road, Zhuozhou, Hebei

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    498-45-3

    MSDS/COA Download

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    Min.Order: 1 Gram

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    Business Type:Lab/Research institutions

    Tel:+86-29-86470566

    Address:Block A of Central Mansion, No.113 of Weiyang Rd, ETDZ, Xi'an, Shaanxi 710016, China

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    498-45-3

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    Scopine

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    HUBEI AOKS TRADE CO.,LTD is located in Hubei province of China.We specialized in Active pharmaceutical ingredient,pharmaceutical intermediates,veterinary drug intermediates and dy

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     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86-27-52345788

    Address:28F,China Construction Third Bureau,Wuhan,Hubei Province, China

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    498-45-3

    Competitive Price Scopine CAS498-45-3

    Min.Order: 100 Gram

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    Business Type:Trading Company

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    498-45-3

    3-Oxa-9-azatricyclo[3.3.1.02,4]nonan-7-ol,9-methyl-, (1a,2b,4b,5a,7b)- 498-45-3

    Min.Order: 1 Kilogram

    FOB Price:  USD $ 0.0-0.0/Kilogram

    1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

    Shanghai Upbio Tech Co.,Ltd (Former Onchem (China)Co.,Ltd) is a comprehensive manufacturer and an international distribution of chemicals throughout the world, The predecessor of

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-21-52196435

    Address:No.2 Floor,No.979 Yunhan Rd,Nicheng,Pudong New Area,Shanghai,China

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    498-45-3

    Scopine CAS NO.498-45-3

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    We, Jilin Tely Imp & Exp Co., Ltd. mainly supply and export products including: pharmaceutical raw materials,Chemical reagents, Food additives, pharmaceutical and pesticide interme

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     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:86-431-81915458

    Address:Room 302, 47 Changping Street, Chaoyang District, Changchun, Jilin Province,China

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    498-45-3

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    Unique advantages for Scopine Cas498-45-3 Guaranteed the purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:White crystalline powder Package:1kg/foil bag;25kg/drum Application:Pharmaceutic

    Wuhan Fortuna Chemical Co., Ltd, located in the predominant Wu Han City where is a traffic hinge of China, is a big integrative chemical enterprise being engaged in producing and

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     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:86-27-59207852

    Address:A2705,Dong Yi Shi Qu,129# XinHua Road,WuHan,China

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    498-45-3

    3-Oxa-9-azatricyclo[3.3.1.02,4]nonan-7-ol,9-methyl-, (1a,2b,4b,5a,7b)-

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0/

    Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

    Shandong Hanjiang Chemical Co., Ltd. is located in Qilu Petrochemical Industrial Park, Zibo City, Shandong Province, involving pesticide, medicine, chemical industry, coating, dy

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:18369939125

    Address:95A, Xingyuan East Road, Zhangdian District

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  • Scopine Manufactory best quality

  • Casno:

    498-45-3

    Scopine Manufactory best quality

    Min.Order: 100 Gram

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    Product Name: Scopine Synonyms: SCOPINE;(1alpha,2beta,4beta,5alpha,7beta)-9-Methyl-3-oxa-9-azatricyclo[3.3.1.02.4]nonan-7-ol;SCOPINE, 97+%;(1α,2β,4β,5α)-9-Methyl-3-oxa-9-azatricyclo[3.3.1.02,4]nonan-7β-ol;(1β,2&al

    Wuhan Zenuo Biopharmaceutical Technology Co., Ltd. is a global biopharmaceutical and chemical enterprise, mainly engaged in the customized synthesis, large-scale production and sal

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:(+86-27)8700-2750

    Address:Floor 19th,No.76,Longyang Road

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  • Casno:

    498-45-3

    Scopine

    Min.Order: 0

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     China (Mainland)  |  Contact Details

    Business Type:Manufacturers

    Tel:86-592-3327115

    Address:Unit 603,No.879,Xiahe Road,Meixin Building,Xiamen,China

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    498-45-3

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-371-86658258

    Address:Building 3 of Innovation Park, East District of the National University Science Park

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  • Casno:

    498-45-3

    Scopine

    Min.Order: 1 Gram

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    Business Type:Other

    Tel:86-15158040660

    Address:Xiaoshan district

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  • Casno:

    498-45-3

    Scopine

    Min.Order: 1 Kilogram

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    Business Type:Lab/Research institutions

    Tel:15318988277

    Address:Weicheng District,Weifang City,Shandong Province

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  • Casno:

    498-45-3

    Scopine

    Min.Order: 1 Kilogram

    FOB Price:  USD $ 1.0-100000.0/Kilogram

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    AFINE CHEMICALS LIMITED is specialized in the fine chemicals and pharmaceuticals and we have enjoyed great popularity in world markets. Since 2005, we have been rapidly growing to

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-85134551

    Address:No. 206 Zhen Hua Road, Hangzhou 310030, Zhejiang, China

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    498-45-3

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    Hebei Shengweiya Biotechnology Co., Ltd. is a manufacturer specializing in pharmaceutical and chemical raw materials and related derivatives. Its products are widely used in the fi

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     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+8618503271668

    Address:Zhonghua South Street

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    498-45-3

    Scopine

    Min.Order: 1 Kilogram

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     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86-371-86658258

    Address:University Science Park

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    498-45-3

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     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86-13349903920

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    498-45-3

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     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:18932722228

    Address:Building 6, No.4299, Jindu Road, Minhang District, Shanghai

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    498-45-3

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    The company is a high-tech enterprise providing comprehensive customer service for pharmaceutical companies at home and abroad in accordance with international standards. Our business includes research, development, process optimization and product

    Prime Molecular Co., Ltd. is an advanced chemical intermediates manufacture with ?two R&D centers and two production sites in China, all well-equipped with dedicated and profession

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    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:0852-95636137

    Address:Hong Kong

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    498-45-3

    Good Price Top Quality Powder Scopine

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    Strong backup of facotry: high R&D ability, favorable quality and competitive price 2. Stock avaliability 3. Flexible business way, like payment term and product delivery 4. Fast response 24*7 5. A good troubleshooter/very positive atti

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    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:86-010-60404860

    Address:Xuhui Plaza, Shunyi district, Beijing

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    498-45-3

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    J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

    J&H Chemical is one of China's leading providers of integrated fine chemical services including offering, research and development, Custom manufacturing business, as well as other

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-571-87396432

    Address:No.200 Zhenhua Rd.Xihu Industrial Park, Hangzhou 310030, China

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    498-45-3

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    HangYu Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. HangYu Chemical consis

    Zibo HangYu Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals

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    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-15988566987

    Address:Room1701, Tianxing Building,Licheng district, jinan, Shandong, China

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    498-45-3

    Hot Sale Scopine

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    BaiFuChem is a Professional chemical raw material supplier in China, our main products include Biochemical , Pharma Intermediate and Organic chemical etc. BaiFuChem have wealth of products,experience , expertise and state-of-the-art

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     China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:+86 592 605 6448

    Address:No.31 Pingshan South Road, HaiCang District, Xiamen, China

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    498-45-3

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    Qingdao Sigma Chemical Ltd is is a global chemical industry manufacturers and suppliers of pharmaceuticals and intermediates, peptide,Nootropis etc API, food and feed additives, herbal extracts, agrochemicals and fine chemicals etc. Our Labo

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     China (Mainland)  |  Contact Details

    Business Type:Trading Company

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    Address:shandong qingdao

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    498-45-3

    Scopine

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  • scopineCAS NO.: 498-45-3

  • Casno:

    498-45-3

    scopineCAS NO.: 498-45-3

    Min.Order: 1 Gram

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  • Scopine-Low price promotion CAS NO.498-45-3

  • Casno:

    498-45-3

    Scopine-Low price promotion CAS NO.498-45-3

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  • (1R,2R,4S,5S,7s)-9-Methyl-3-oxa-9-azatricyclo[3.3.1.02,4]nonan-7-ol

  • Casno:

    498-45-3

    (1R,2R,4S,5S,7s)-9-Methyl-3-oxa-9-azatricyclo[3.3.1.02,4]nonan-7-ol

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  • Scopine

  • Casno:

    498-45-3

    Scopine

    Min.Order: 1 Metric Ton

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  • 498-45-3

  • Casno:

    498-45-3

    498-45-3

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0/

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Specification

Scopine, with the CAS NO.498-45-3, is a tropane alkaloid found in a variety of plants including Mandragora root, Senecio mikanoides (Delairea odorata), Scopolia carniolica, and Scopolia lurida. It is also called 1α,2β,4β,5α)-9-Methyl-3-oxa-9-azatricyclo[3.3.1.02,4]nonan-7β-ol;(1β,2α,4α,5β,7α)-9-Methyl-3-oxa-9-azatricyclo[3.3.1.02,4]nonan-7-ol. Scopine can be prepared by the hydrolysis of scopolamine.

Physical properties about Scopine are: (1)ACD/LogP: -0.295; (2)ACD/LogD (pH 5.5): -3.23; (3)ACD/LogD (pH 7.4): -1.82; (4)ACD/BCF (pH 5.5): 1.00; (5)ACD/BCF (pH 7.4): 1.00; (6)ACD/KOC (pH 5.5): 1.00; (7)ACD/KOC (pH 7.4): 1.00; (8)#H bond acceptors: 3; (9)#H bond donors: 1; (10)#Freely Rotating Bonds: 1; (11)Molar Refractivity: 39.857 cm3; (12)Molar Volume: 120.794 cm3; (13)Polarizability: 15.801 10-24cm3; (14)Surface Tension: 46.4469985961914 dyne/cm; (15)Density: 1.285 g/cm3; (16)Flash Point: 123.928 °C; (17)Enthalpy of Vaporization: 60.366 kJ/mol; (18)Boiling Point: 281.303 °C at 760 mmHg

You can still convert the following datas into molecular structure:
(1)InChI=1S/C8H13NO2/c1-9-5-2-4(10)3-6(9)8-7(5)11-8/h4-8,10H,2-3H2,1H3/t4-,5-,6+,7-,8+;
(2)InChIKey=FIMXSEMBHGTNKT-RZVDLVGDSA-N;
(3)SmilesO1[C@H]2[C@H]1[C@H]1C[C@H](C[C@@H]2N1C)O;