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Basic Information
| CAS No.: | 504-74-5 |
|---|---|
| Name: | Imidazolidine |
| Article Data: | 7 |
| Molecular Structure: | |
|
|
|
| Formula: | C3H8 N2 |
| Molecular Weight: | 72.1099 |
| Synonyms: | 1,3-Diazacyclopentane;Imidazole, tetrahydro- |
| Density: | 0.892g/cm3 |
| Melting Point: | 68.2-68.8 °C |
| Boiling Point: | 92.8°Cat760mmHg |
| Flash Point: | °C |
| PSA: | 24.06000 |
| LogP: | -0.20570 |
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Synthetic route
Conditions
| Conditions | Yield |
|---|---|
| With magnesium sulfate; potassium carbonate In chloroform at 20℃; for 18h; | 71% |
| at 100℃; for 0.5h; | |
| With magnesium sulfate; potassium carbonate In chloroform for 17h; Ambient temperature; |
- 1367520-68-0
endo-3,5-di(p-tolyl)-3,5-diazatricyclo[5.2.1.0]dec-8-ene
- 107-15-3
ethylenediamine
A
- 504-74-5
tetrahydroimidazole
B
- 1367903-87-4
cis-endo-N,N'-di(p-tolyl)bicyclo[2.2.1]hept-5-ene-2,3-diamine
Conditions
| Conditions | Yield |
|---|---|
| With toluene-4-sulfonic acid at 150℃; for 48h; | A n/a B 22% |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| With water |
- 51-46-7
1,3,6,8-tetraazatricyclo[4.4.1.13,8]dodecane
A
- 504-74-5
tetrahydroimidazole
B
- 280-29-5
1,3,5-triazabicyclo[3.2.1]-octane
C
- 100-97-0
hexamethylenetetramine
Conditions
| Conditions | Yield |
|---|---|
| With ammonium fluoride In water-d2 at 23℃; for 8h; Title compound not separated from byproducts.; |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| With copper(l) chloride In toluene at 100℃; for 8h; Mannich Aminomethylation; Inert atmosphere; | 62% |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| With copper(l) chloride In toluene at 100℃; for 8h; Mannich Aminomethylation; Inert atmosphere; | 51% |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| With sodium hydroxide In water at -20 - -10℃; for 1h; | 50% |
Conditions
| Conditions | Yield |
|---|---|
| With sodium hydroxide at 25℃; for 1h; | 40% |
| With sodium hydroxide | |
| With pyridine In chloroform Yield given; |
- 504-74-5
tetrahydroimidazole
- 123476-78-8
5-Chlor-3-(4-chlorphenyl)-4-phenylisoxazol
A
- 123476-97-1
N1-[3-(4-Chloro-phenyl)-4-phenyl-isoxazol-5-yl]-ethane-1,2-diamine
B
- 130719-54-9
5-(Tetrahydroimidazolo)-3-(4-chlorphenyl)-4-phenylisoxazol
Conditions
| Conditions | Yield |
|---|---|
| In tetrahydrofuran for 24h; Heating; | A n/a B 19% |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| With diethyl ether |
Downstream Products
