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5042-30-8

Basic Information
CAS No.: 5042-30-8
Name: 2,2,2-Trifluoroethylhydrazine
Article Data: 1
Molecular Structure:
Molecular Structure of 5042-30-8 (2,2,2-Trifluoroethylhydrazine)
Formula: C2H5F3N2
Molecular Weight: 114.07
Synonyms: (2,2,2-Trifluoroethyl)hydrazine;1-(2,2,2-Trifluoroethyl)hydrazine;Hydrazine,(2,2,2-trifluoroethyl)-;Trifluoroethylhydrazine;
EINECS: 225-734-0
Density: 1.261 g/cm3
Boiling Point: 83.1 ºC at 760 mmHg
Flash Point: 42.8 ºC
Appearance: clear yellow to green liquid
Hazard Symbols: HarmfulXn
Risk Codes: R10;R20/21/22   
Safety: S36
Transport Information: UN 1993
PSA: 38.05000
LogP: 1.10320
Synthetic route

tert-butyl 2-(2,2,2-trifluoroethyl)hydrazinecarboxylate

5042-30-8

2,2,2,trifluoroethylhydrazine

Conditions
ConditionsYield
With trifluoroacetic acid In dichloromethane at 20℃;
5042-30-8

2,2,2,trifluoroethylhydrazine

105-45-3

acetoacetic acid methyl ester

76552-51-7

3-methyl-1-(2,2,2-trifluoroethyl)-5-pyrazolone

Conditions
ConditionsYield
In ethanol at 20 - 60℃;99%
910553-57-0

4-chloro-N-dimethylaminomethylene-2-thiophene carboxamide

5042-30-8

2,2,2,trifluoroethylhydrazine

5-(4-chloro-thiophen-2-yl)-1-(2,2,2-trifluoro-ethyl)-1H-[1,2,4]triazole

Conditions
ConditionsYield
With acetic acid In water at 90℃; for 0.75h;99%
5042-30-8

2,2,2,trifluoroethylhydrazine

123-54-6

acetylacetone

141354-19-0

3,5-dimethyl-1-(2,2,2-trifluoroethyl)-1H-pyrazole

Conditions
ConditionsYield
In ethanol Reflux;99%
With hydrogenchloride In water at 60℃; for 1.5h;36 g
5042-30-8

2,2,2,trifluoroethylhydrazine

139575-14-7, 120672-87-9

N-(4-bromobenzylidene)glycine methyl ester

5-p-bromophenyl-6-trifluoromethyl-1,2,5,6-tetrahydro-1,2,4-triazine-3-carboxylic acid methyl ester

Conditions
ConditionsYield
Stage #1: N-(4-bromobenzylidene)glycine methyl ester With silver(I) acetate; caesium carbonate In acetonitrile at 20℃; for 0.05h; Schlenk technique;
Stage #2: 2,2,2,trifluoroethylhydrazine In acetonitrile at 20℃; for 48h; Schlenk technique;
99%
5042-30-8

2,2,2,trifluoroethylhydrazine

76862-09-4

methyl N-(4-chlorobenzylidene)glycinate

5-(4-chlorophenyl)-6-trifluoromethyl-1,2,5,6-tetrahydro-1,2,4-triazin-3-carboxylic acid methyl ester

Conditions
ConditionsYield
Stage #1: methyl N-(4-chlorobenzylidene)glycinate With silver(I) acetate; caesium carbonate In tetrahydrofuran at 20℃; for 0.05h; Schlenk technique;
Stage #2: 2,2,2,trifluoroethylhydrazine In tetrahydrofuran at 20℃; for 36h; Schlenk technique;
97%
479499-37-1

(4-fluorobenzylideneamino)acetic acid methyl ester

5042-30-8

2,2,2,trifluoroethylhydrazine

5-p-fluorophenyl-6-trifluoromethyl-1,2,5,6-tetrahydro-1,2,4-triazine-3-carboxylic acid methyl ester

Conditions
ConditionsYield
Stage #1: (4-fluorobenzylideneamino)acetic acid methyl ester With caesium carbonate; silver carbonate In tetrahydrofuran at 20℃; for 0.05h; Schlenk technique;
Stage #2: 2,2,2,trifluoroethylhydrazine In tetrahydrofuran at 20℃; for 2h; Schlenk technique;
96%
5042-30-8

2,2,2,trifluoroethylhydrazine

methyl 2-(1-naphthalenemethyleneamino)acetate

5-(1-naphthyl)-6-trifluoromethyl-1,2,5,6-tetrahydro-1,2,4-triazine-3-carboxylic acid methyl ester

Conditions
ConditionsYield
Stage #1: methyl 2-(1-naphthalenemethyleneamino)acetate With silver fluoride; caesium carbonate In tetrahydrofuran at 20℃; for 0.05h; Schlenk technique;
Stage #2: 2,2,2,trifluoroethylhydrazine In tetrahydrofuran at 20℃; for 30h; Schlenk technique;
96%
5042-30-8

2,2,2,trifluoroethylhydrazine

104249-92-5

methyl 2-((naphthalen-2-yl)methyleneamino)-acetate

5-(2-naphthyl)-6-trifluoromethyl-1,2,5,6-tetrahydro-1,2,4-triazine-3-carboxylic acid methyl ester

Conditions
ConditionsYield
Stage #1: methyl 2-((naphthalen-2-yl)methyleneamino)-acetate With silver(I) acetate; caesium carbonate In tetrahydrofuran at 20℃; for 0.05h; Schlenk technique;
Stage #2: 2,2,2,trifluoroethylhydrazine In tetrahydrofuran at 20℃; for 24h; Schlenk technique;
95%
958462-15-2

(3E)-1-benzoyl-3-(dimethylamino)methylidenepyrrolidin-2-one

5042-30-8

2,2,2,trifluoroethylhydrazine

958462-23-2

N-{2-[5-hydroxy-1-(2,2,2-trifluoroethyl)-1H-pyrazol-4-yl]ethyl}benzamide

Conditions
ConditionsYield
With hydrogenchloride In propan-1-ol for 4h; Heating;94%
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Chemistry


IUPAC Name: 2,2,2-Trifluoroethylhydrazine
Molecular Formula: C2H5F3N2
Molecular Weight: 114.07 g/mol
Canonical SMILES: C(C(F)(F)F)NN
InChI: InChI=1S/C2H5F3N2/c3-2(4,5)1-7-6/h7H,1,6H2
EINECS: 225-734-0
Product Categories: Aliphatics; Hydrazines; Nitrogen Compounds; Organic Building Blocks
Storage temperature: Flammables area
XLogP3-AA: 0.2
H-Bond Donor: 2
H-Bond Acceptor: 5
Surface Tension: 20.4 dyne/cm
Density: 1.261 g/cm3
Flash Point: 42.8 °C
Enthalpy of Vaporization: 32.36 kJ/mol
Boiling Point: 83.1 °C at 760 mmHg
Vapour Pressure of 2,2,2-Trifluoroethylhydrazine (CAS NO.5042-30-8): 76.5 mmHg at 25 °C

Safety Profile

Hazard Codes: HarmfulXn
Risk Statements: 10-20/21/22 
R10: Flammable. 
R20/21/22: Harmful by inhalation, in contact with skin and if swallowed.
Safety Statements: 36 
S36: Wear suitable protective clothing.
RIDADR: UN 1993 3/PG 3
Hazard Note: Harmful
HazardClass: 3.2
PackingGroup of 2,2,2-Trifluoroethylhydrazine (CAS NO.5042-30-8): III

Specification

 2,2,2-Trifluoroethylhydrazine (CAS NO.5042-30-8), its Synonyms are 2,2,2-Trifluoroethylhydrazine,aqueoussolution ; 2,2,2-Trifluoroethylhydrazine, 70 wt% aqueous solution ; 2,2,2-trifluoroethylhydrazine solution ; Trifluoroethylhydrazine ; 2,2,2-Trifluoroethylhydrazine, 70% aqueous solution . It is clear yellow to green liquid.