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523-27-3

Basic Information
CAS No.: 523-27-3
Name: 9,10-Dibromoanthracene
Article Data: 89
Molecular Structure:
Molecular Structure of 523-27-3 (9,10-Dibromoanthracene)
Formula: C14H8Br2
Molecular Weight: 336.026
Synonyms: NSC 6263;
EINECS: 208-342-4
Density: 1.768 g/cm3
Melting Point: 220-225 °C
Boiling Point: 427.1 °C at 760 mmHg
Flash Point: 248.1 °C
Solubility: Soluble in water.
Appearance: yellow to yellow-green fluffy powder
Hazard Symbols: IrritantXi,DangerousN
Risk Codes: 36/37/38-50/53
Safety: 37/39-26-61-60-36
Transport Information: UN 3077
PSA: 0.00000
LogP: 5.51800
Synthetic route
120-12-7

anthracene

523-27-3

9,10-Dibromoanthracene

Conditions
ConditionsYield
With N-Bromosuccinimide; lithium perchlorate; silica gel In dichloromethane at 20℃; for 0.0833333h;100%
With oxygen; 1,2-dibromomethane at 20℃; for 2h;99%
With N-Bromosuccinimide; lithium perchlorate; silica gel In dichloromethane for 0.5h;99%
1564-64-3

9-Bromoanthracene

523-27-3

9,10-Dibromoanthracene

Conditions
ConditionsYield
With N-Bromosuccinimide; C5H13NO3S In n-heptane at 25℃; for 19h; Reagent/catalyst; Darkness;85%
With bis(trifluoroacetoxy)iodobencene; trimethylsilyl bromide In dichloromethane at 20℃; Inert atmosphere;83%
With phosphorus pentabromide; benzene
With nitric acid; acetic acid
With 2,6-di-tert-butyl-pyridine; Bromoform In acetonitrile platinum mesh electrodes, H cell containing 0.1 M Bu4NPF6, constant current 10 mA;57 % Chromat.
120-12-7

anthracene

A

523-27-3

9,10-Dibromoanthracene

B

84-65-1

9,10-phenanthrenequinone

Conditions
ConditionsYield
With potassium permanganate; hydrogen bromide In acetonitrileA 85%
B 3%
120-12-7

anthracene

A

1564-64-3

9-Bromoanthracene

B

523-27-3

9,10-Dibromoanthracene

Conditions
ConditionsYield
With N-Bromosuccinimide; 2,4,6-trimethylaniline In dichloromethane at 0℃; for 8h; Inert atmosphere; regioselective reaction;A 84%
B 7%
With N-Bromosuccinimide; C5H13NO3S In n-heptane at 60℃; for 4.5h; Darkness;A 81%
B 8%
With N-Bromosuccinimide; iodine In tetrachloromethane Bromination; Heating;
67-56-1

methanol

120-12-7

anthracene

A

31750-30-8

trans-9,10-dihydro-9,10-dimethoxyanthracene

B

523-27-3

9,10-Dibromoanthracene

C

2395-96-2

9-methoxyanthracene

D

2395-97-3

9,10-dimethoxyanthracene

Conditions
ConditionsYield
With pyridine; bromine; sodium hydrogencarbonate; water at 20℃; for 0.25h;A 82%
B n/a
C 1%
D 1%
120-12-7

anthracene

7726-95-6

bromine

523-27-3

9,10-Dibromoanthracene

Conditions
ConditionsYield
In dichloromethane for 24h;75%
602-60-8

9-nitroanthracene

A

523-27-3

9,10-Dibromoanthracene

B

14789-48-1

bromo-9 nitro-10 anthracene

Conditions
ConditionsYield
With bromine In nitromethane Heating;A 22%
B 44%
642-31-9

9-anthracene aldehyde

A

523-27-3

9,10-Dibromoanthracene

B

93496-77-6

9,10-bromoanthracene-9-carbaldehyde

Conditions
ConditionsYield
With bromine In tetrachloromethane at 0 - 5℃; for 20h;A n/a
B 22%
613-31-0

9,10-dihydroanthracene

A

523-27-3

9,10-Dibromoanthracene

B

725744-58-1

2,9,10-tribromo-anthracene

Conditions
ConditionsYield
With carbon disulfide; bromine; iodine Ausschluss von Licht;
46491-50-3

9,19-Dibromo-9,10-dihydroanthracene

523-27-3

9,10-Dibromoanthracene

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Chemistry

IUPAC Name: 9,10-Dibromoanthracene
Synonyms of Anthracene, 9,10-dibromo- (CAS NO.523-27-3): 9,10-Dibromoanthracene ; EINECS 208-342-4 ; NSC 6263
CAS NO: 523-27-3
Molecular Formula: C14H8Br2
Molecular Weight: 336.0213
Molecular Structure:

Melting Point: 220-225 °C
ProductCategories: Aromatic Compounds ; Miscellaneous ; Electronic Chemicals ; Anthracenes ; Anthracene series ; Aryl ; C13 to C37+ ; Halogenated Hydrocarbons 
Index of Refraction: 1.748
Molar Refractivity: 77.31 cm3
Molar Volume: 190 cm3
Surface Tension: 54.3 dyne/cm
Density of 1.768 g/cm3
Flash Point: 248.1 °C
Enthalpy of Vaporization: 65.56 kJ/mol
Boiling Point: 427.1 °C at 760 mmHg
Vapour Pressure: 4.19E-07 mmHg at 25°C

Uses

 Anthracene, 9,10-dibromo- (CAS NO.523-27-3) is used as intermediates in organic synthesis.

Safety Profile

Hazard Codes of Anthracene, 9,10-dibromo- (CAS NO.523-27-3): IrritantXi,DangerousN
Risk Statements: 36/37/38-50/53 
R36/37/38: Irritating to eyes, respiratory system and skin. 
R50/53: Very toxic to aquatic organisms, may cause long-term adverse effects in the aquatic environment.
Safety Statements: 37/39-26-61-60-36 
S37/39: Wear suitable gloves and eye/face protection. 
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. 
S61: Avoid release to the environment. Refer to special instructions / safety data sheets. 
S60: This material and its container must be disposed of as hazardous waste. 
S36: Wear suitable protective clothing.
RIDADR UN 3077

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