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| CAS No.: | 5411-63-2 |
|---|---|
| Name: | 2-ButenaMide, N,N-diethyl-3-Methyl- |
| Article Data: | 10 |
| Molecular Structure: | |
|
|
|
| Formula: | C9H17NO |
| Molecular Weight: | 155.24 |
| Synonyms: | N,N-Diaethyl-3-methyl-crotonamid;N,N-diethyl-3-methyl-but-2-enamide;N,N-dimethylamino-3,3-diethylacrylamide;N,N-Diethyl-3-methyl-2-butenamide;N,N-diethyl seneciamide;3-methyl-crotonic acid diethylamide;N,N-diethylsenecioamide;N,N-diethyl-3,3-dimethylacrylic amide; |
| Density: | 0.887g/cm3 |
| Boiling Point: | 259.3°Cat760mmHg |
| Flash Point: | 109°C |
| PSA: | 20.31000 |
| LogP: | 1.82100 |
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- 548773-13-32-amino-4,6-dimethylpyrimidine-5-carboxylic acid
- 3350-78-5
3,3-Dimethylacryloyl chloride
- 109-89-7
diethylamine
- 5411-63-2
N,N-dimethylamino-3,3-diethylacrylamide
| Conditions | Yield |
|---|---|
| 90% | |
| With diethyl ether |
- 109-72-8, 29786-93-4
n-butyllithium
- 686-10-2
N,N-diethyl-1,2,2-trichlorovinylamine
- 67-64-1
acetone
- 5411-63-2
N,N-dimethylamino-3,3-diethylacrylamide
| Conditions | Yield |
|---|---|
| (i), (ii) /BRN= 635680/, (iii) (hydrolysis); Multistep reaction; |
- 5674-01-1
2-methylallylmagnesium chloride
A
- 5411-63-2
N,N-dimethylamino-3,3-diethylacrylamide
B
- 62721-80-6
N,N-diethyl-3-methyl-3-butenamide
| Conditions | Yield |
|---|---|
| In tetrahydrofuran; hexane at 20℃; for 1h; Yield given. Yields of byproduct given; | |
| With lithium diisopropyl amide In tetrahydrofuran; hexane at 20℃; for 1h; Yield given. Yields of byproduct given; |
- 201230-82-2
carbon monoxide
- 109-89-7
diethylamine
- 563-47-3
3-Chloro-2-methylpropene
A
- 19737-36-1
diethyl-methallyl-amine
B
- 5411-63-2
N,N-dimethylamino-3,3-diethylacrylamide
C
- 62721-80-6
N,N-diethyl-3-methyl-3-butenamide
| Conditions | Yield |
|---|---|
| With bis-triphenylphosphine-palladium(II) chloride In benzene under 76000 Torr; Ambient temperature; |
- 5411-63-2
N,N-dimethylamino-3,3-diethylacrylamide
- 73183-34-3
bis(pinacol)diborane
| Conditions | Yield |
|---|---|
| With methanol; water; caesium carbonate; bis(1,5-cyclooctadiene)nickel (0); tricyclohexylphosphine In toluene at 20℃; for 7h; | 80% |
- 994-30-9
triethylsilyl chloride
- 5411-63-2
N,N-dimethylamino-3,3-diethylacrylamide
A
- 1174909-04-6
(Z)-N,N-diethyl-3-methyl-4-triethylsilyl-but-2-enamide
B
- 1174909-05-7
(E)-N,N-diethyl-3-methyl-4-triethylsilyl-but-2-enamide
| Conditions | Yield |
|---|---|
| Stage #1: N,N-dimethylamino-3,3-diethylacrylamide With lithium diisopropyl amide In tetrahydrofuran at -78 - -75℃; for 1h; Inert atmosphere; Stage #2: triethylsilyl chloride In tetrahydrofuran at -78℃; for 18.5h; Inert atmosphere; Reflux; Stage #3: With water; ammonium chloride In tetrahydrofuran Saturated solution; optical yield given as %de; diastereoselective reaction; | A 21% B 47% |
- 5411-63-2
N,N-dimethylamino-3,3-diethylacrylamide
- 7051-13-0
1-chloro-2,4-dimethoxybenzene
- 106914-39-0
5,7-dimethoxy-2-methyl-4-naphthol
| Conditions | Yield |
|---|---|
| With lithium cyclohexylisopropylamide In tetrahydrofuran -78 deg C, 1 h, rt; | 46% |
- 75-77-4
chloro-trimethyl-silane
- 5411-63-2
N,N-dimethylamino-3,3-diethylacrylamide
A
- 1174909-02-4
(Z)-N,N-diethyl-3-methyl-4-trimethylsilyl-but-2-enamide
B
- 1174909-03-5
(E)-N,N-diethyl-3-methyl-4-trimethylsilyl-but-2-enamide
C
- 62721-80-6
N,N-diethyl-3-methyl-3-butenamide
| Conditions | Yield |
|---|---|
| Stage #1: N,N-dimethylamino-3,3-diethylacrylamide With lithium diisopropyl amide In tetrahydrofuran at -78 - -75℃; for 1h; Inert atmosphere; Stage #2: chloro-trimethyl-silane In tetrahydrofuran at -78℃; for 17.5h; Inert atmosphere; Reflux; Stage #3: With water; ammonium chloride In tetrahydrofuran Saturated solution; optical yield given as %de; diastereoselective reaction; | A 39% B 35% C n/a |
- 2398-37-0
3-methoxyphenyl bromide
- 5411-63-2
N,N-dimethylamino-3,3-diethylacrylamide
- 22273-56-9
4-hydroxy-5-methoxy-2-methyl-naphthalene
| Conditions | Yield |
|---|---|
| Stage #1: N,N-dimethylamino-3,3-diethylacrylamide With n-butyllithium; N-cyclohexylisopropylamine In tetrahydrofuran at -78℃; for 1h; Inert atmosphere; Stage #2: 3-methoxyphenyl bromide In tetrahydrofuran at 20℃; for 18h; Diels-Alder reaction; Inert atmosphere; | 35% |
| With lithium cyclohexylisopropylamide 1) THF, hexane, -78 deg C, 1 h; 2) THF, -20 deg C, then room temp., overnight; Yield given. Multistep reaction; |
- 3350-78-5
3,3-Dimethylacryloyl chloride
- 109-89-7
diethylamine
- 5411-63-2
N,N-dimethylamino-3,3-diethylacrylamide
| Conditions | Yield |
|---|---|
| 90% | |
| With diethyl ether |
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