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5418-51-9

Basic Information
CAS No.: 5418-51-9
Name: 2-Hydroxy-5-nitropyridine
Article Data: 38
Molecular Structure:
Molecular Structure of 5418-51-9 (2-Hydroxy-5-nitropyridine)
Formula: C5H4N2O3
Molecular Weight: 140.098
Synonyms: 5-nitro-3H-pyridin-2-one;5-Nitropyridin-2-ol;5-Nitro-2-hydroxypyridine;2-Hydroxy-5-nitro pyridine;2(1H)-Pyridinone, 5-nitro-;
EINECS: 226-525-7
Density: 1.44 g/cm3
Melting Point: 188-191 °C(lit.)
Boiling Point: 334 °C at 760 mmHg
Flash Point: 155.8 °C
Solubility: Soluble in hot water and alkali liquor, Insoluble in most of organic solvents.
Appearance: light yellow to beige crystalline powder
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-37/39-36
PSA: 78.94000
LogP: 1.21860
Synthetic route
5459-35-8

2-bromo-acrylic acid ethyl ester

75-52-5

nitromethane

122-51-0

orthoformic acid triethyl ester

5418-51-9

5-nitro-2-hydroxypyridine

Conditions
ConditionsYield
Stage #1: 2-bromo-acrylic acid ethyl ester; nitromethane With 1,8-diazabicyclo[5.4.0]undec-7-ene at 40 - 45℃; for 6h;
Stage #2: orthoformic acid triethyl ester With zinc(II) chloride at 90 - 95℃; for 6h;
Stage #3: With ammonium hydroxide; ammonium chloride In ethanol at 50 - 55℃; for 4h;
90.6%
75-52-5

nitromethane

687-46-7

ethyl 2-chloroacrylate

122-51-0

orthoformic acid triethyl ester

5418-51-9

5-nitro-2-hydroxypyridine

Conditions
ConditionsYield
Stage #1: nitromethane; ethyl 2-chloroacrylate With DBN at 60 - 65℃; for 4h;
Stage #2: orthoformic acid triethyl ester With copper(l) chloride at 95 - 100℃; for 3h;
Stage #3: With ammonium hydroxide; ammonium chloride In ethanol at 60 - 65℃; for 4h;
89.9%
4214-76-0

5-nitro-pyridin-2-ylamine

5418-51-9

5-nitro-2-hydroxypyridine

Conditions
ConditionsYield
With hydrogenchloride; sodium nitrite In water at 0 - 6℃; for 0.666667h; Temperature; Concentration;88.02%
With sulfuric acid; sodium nitrite at 0 - 20℃;77%
With ammonium hydroxide; sodium nitrite at 0 - 10℃; Large scale;58.1%
80-63-7

methyl 2-chloroacrylate

75-52-5

nitromethane

122-51-0

orthoformic acid triethyl ester

5418-51-9

5-nitro-2-hydroxypyridine

Conditions
ConditionsYield
Stage #1: methyl 2-chloroacrylate; nitromethane With 1,8-diazabicyclo[5.4.0]undec-7-ene at 50 - 55℃; for 5h;
Stage #2: orthoformic acid triethyl ester With zinc(II) chloride at 95 - 100℃; for 4h;
Stage #3: With ammonium hydroxide; ammonium chloride In methanol at 50 - 55℃; for 6h;
87.8%
75-52-5

nitromethane

4519-46-4

methyl 2-bromoacrylate

122-51-0

orthoformic acid triethyl ester

5418-51-9

5-nitro-2-hydroxypyridine

Conditions
ConditionsYield
Stage #1: nitromethane; methyl 2-bromoacrylate With 1,8-diazabicyclo[5.4.0]undec-7-ene at 40 - 45℃; for 6h;
Stage #2: orthoformic acid triethyl ester With tin(IV) chloride at 95 - 100℃; for 4h;
Stage #3: With ammonium hydroxide; ammonium chloride In methanol at 50 - 55℃; for 4h;
86.4%
2554-75-8

N,N-dimethyl-5-nitropyridin-2-amine

A

5418-51-9

5-nitro-2-hydroxypyridine

B

113509-58-3

2-(methylamino)-5-nitropyridine N1-oxide

Conditions
ConditionsYield
With 3-chloro-benzenecarboperoxoic acid In chloroform for 30h; Ambient temperature;A 24%
B 7%
With 3-chloro-benzenecarboperoxoic acid In chloroform for 720h; Ambient temperature;A 24%
B 7%
4548-45-2

2-chloro-5-nitropyridine

5418-51-9

5-nitro-2-hydroxypyridine

Conditions
ConditionsYield
With 15-crown-5; cumene hydroperoxide sodium salt In dichloromethane at 20℃; for 16h;17.5%
With potassium hydroxide; water
With hydrogenchloride; water at 150℃; unter Druck;
With hydroxide In dimethylsulfoxide-d6; water-d2 Mechanism;
4214-76-0

5-nitro-pyridin-2-ylamine

A

456-24-6

2-Fluoro-5-nitropyridine

B

5418-51-9

5-nitro-2-hydroxypyridine

Conditions
ConditionsYield
With hydrogen fluoride Behandeln der Reaktionsloesung mit Natriumnitrit;
31594-45-3

2-ethoxy-5-nitropyridine

5418-51-9

5-nitro-2-hydroxypyridine

Conditions
ConditionsYield
With hydrogenchloride; water at 160 - 170℃; unter Druck;
With zinc(II) chloride at 160℃;
6854-07-5

2-hydroxy-5-nitropyridine-3-carboxylic acid

5418-51-9

5-nitro-2-hydroxypyridine

Conditions
ConditionsYield
at 330℃;
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    Name: 2-Hydroxy-5-Nitropyridine Molecular Formula:C5H4N2O3 Molecular Weight:140.1 CAS No.:5418-51-9 Appearance:Slight Yellow To Slight Browncrystal Powder Appearance:Slight Yellow To Slight Browncrystal Powder Storage:Store in cool and dry place,

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  • 2-Hydroxy-5-nitropyridine 5418-51-9CAS NO.: 5418-51-9

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    2-Hydroxy-5-nitropyridine Chemical Properties Melting point 188-191 °C (lit.) Boiling point 256.56°C (rough estimate) density 1.5657 (rough estimate) refractive index 1.4800 (estimate) form Crystalline Powder pka 8.06&p

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    Wuhu Nuovo Chemical Technology Co., Ltd. was established in August 2014, mainly engaged in the development, production and sales of ionic liquids, ribose, nucleosides, nucleotides and related chemicals; Products are mainly used in new energy, new ma

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    High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

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    Business Type:Manufacturers

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    Tel:+86-592 599 8717

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Chemistry

MF: C5H4N2O3
MW: 140.1
EINECS: 226-525-7
mp  188-191 °C(lit.)

Uses

2-HYDROXY-5-NITROPYRIDINE is used for pharmaceutical intermediates.

Safety Profile

Hazard Codes  Xi
Risk Statements  36/37/38
Safety Statements  26-37/39-36
WGK Germany  3
Hazard Note  Irritant