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54255-11-7

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Basic Information
CAS No.: 54255-11-7
Name: 1H-IMidazole, 2-chloro-4,5-dihydro-
Article Data: 6
Molecular Structure:
Molecular Structure of 54255-11-7 (1H-IMidazole, 2-chloro-4,5-dihydro-)
Formula: C3H5ClN2
Molecular Weight: 104.539
Synonyms: 2-chloro-4,5-dihydroimidazole;2-Chloro-2-imidazoline;2-chloroimidazoline;2-chloro-3,4-dihydroimidazole;
Density: 1.48g/cm3
Boiling Point: 141.4°Cat760mmHg
Flash Point: 39.3°C
PSA: 24.39000
LogP: -0.05120
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Synthetic route
120-93-4

imidazolidone

54255-11-7

2-chloro-4,5-dihydro-1H-imidazole

Conditions
ConditionsYield
With phosphorus pentachloride In acetonitrile at 20℃; for 72h;55%
With triethylamine; Dimethyl chlorophosphate In dichloromethane at 35℃; for 5h;
120-93-4

imidazolidone

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chlorophosphoric acid diphenyl ester

A

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tetraphenyl pyrophosphate

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54255-11-7

2-chloro-4,5-dihydro-1H-imidazole

Conditions
ConditionsYield
With triethylamine In N,N-dimethyl-formamide at 35℃; for 0.0666667h;
...Expand
54255-12-8

2-Chloro-4,5-dihydro-1H-imidazole sulfate

54255-11-7

2-chloro-4,5-dihydro-1H-imidazole

Conditions
ConditionsYield
With sodium hydroxide In diethyl ether; water at 0℃;
With sodium hydroxide In water Cooling with ice;
96-45-7

N,N'-ethylenethiourea

54255-11-7

2-chloro-4,5-dihydro-1H-imidazole

Conditions
ConditionsYield
With chlorine In water at 45℃; for 2.5h;
75-31-0

isopropylamine

54255-11-7

2-chloro-4,5-dihydro-1H-imidazole

(4,5-dihydro-1H-imidazol-2-yl)-isopropyl-amine

Conditions
ConditionsYield
In dichloromethane97%
14453-85-1

4-[(4-methoxyphenyl)thio]benzenamine

54255-11-7

2-chloro-4,5-dihydro-1H-imidazole

(4,5-dihydro-1H-imidazol-2-yl)-[4-(4-methoxyphenylsulfanyl)phenyl]amine hydrochloride

Conditions
ConditionsYield
In 2-methyl-propan-1-ol for 2h; Heating / reflux;96%
54255-11-7

2-chloro-4,5-dihydro-1H-imidazole

77737-90-7

1,2,4,5-Tetrahydro-12bH-3,3b,6,6b,12c-pentaaza-dicyclopenta[a,c]phenanthrene

Conditions
ConditionsYield
With potassium carbonate at 5℃;95%
62-53-3

aniline

54255-11-7

2-chloro-4,5-dihydro-1H-imidazole

1848-75-5

N-phenyl-N-(4,5-dihydro-1H-imidazol-2-yl)amine

Conditions
ConditionsYield
In dichloromethane95%
100-46-9

benzylamine

54255-11-7

2-chloro-4,5-dihydro-1H-imidazole

38941-36-5

benzyl-(4,5-dihydro-1H-imidazol-2-yl)-amine

Conditions
ConditionsYield
In dichloromethane95%
2735-04-8

2,4-Dimethoxyaniline

54255-11-7

2-chloro-4,5-dihydro-1H-imidazole

(4,5-dihydro-1H-imidazol-2-yl)-(2,4-dimethoxy-phenyl)-ammonium chloride

Conditions
ConditionsYield
In dichloromethane94%
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