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5470-11-1

Basic Information
CAS No.: 5470-11-1
Name: Hydroxylamine,hydrochloride (1:1)
Molecular Structure:
Molecular Structure of 5470-11-1 (Hydroxylamine,hydrochloride (1:1))
Formula: H3NO.HCl
Molecular Weight: 69.4909
Synonyms: Hydroxylamine,hydrochloride (8CI,9CI);Hydroxyammonium chloride;Hydroxylamine chloride;Hydroxylamine chlorohydrate;Hydroxylammonium chloride;Oxammonium hydrochloride;hydroxylamine hydrochloride;Hydroxylamine HCl;
EINECS: 226-798-2
Density: 1.67 g/mL at 25 °C
Melting Point: 155-158 °C
Boiling Point: 56.5 °C at 760 mmHg
Flash Point: N/A
Solubility: 560 g/L (20 °C) in water
Appearance: Colorless or off-white crystalline solid
Hazard Symbols: HarmfulXn, DangerousN
Risk Codes: 22-36/38-43-48/22-50
Safety: 22-24-37-61
Transport Information: UN 2923 8/PG 2
PSA: 46.25000
LogP: 0.83660
Synthetic route

Mo(NO)(NH2O)(C6H4S2C2H4S2C6H4)*C4H8O

{Mo(NO)(Cl)(dttd)}

B

5470-11-1

hydroxylamine hydrochloride

Conditions
ConditionsYield
With hydrogenchloride In methanol byproducts: NH4Cl, N2H5Cl; (N2); HCl bubbled through a soln. of the Mo-complex at 0°C for 15 min; soln. stirred for 1.5 h at room temp.; N2 bubbled through the suspn. for 15 min; ppt. filtered, washed with methanol and diethyl ether; recrystd. from hot THF;A 93%
B n/a
625-58-1

ethyl nitrate

tin(ll) chloride

A

5470-11-1

hydroxylamine hydrochloride

B

7664-41-7

ammonia

C

7646-78-8

tin(IV) chloride

Conditions
ConditionsYield
With hydrogenchloride In hydrogenchloride byproducts: C2H5OH, H2O; in concd. HCl soln.; evapn. of the alcohol,diluting with water,pptg. of the Sn with H2S,evapn. and crystn. from alcohol;A 90%
B <1
C n/a
54515-04-7, 50897-08-0, 14363-30-5

[Ni(II)(salicylaldehyde oximate)2]

18299-54-2

ethylenediamine hydrochloride

A

Ni(C6H4(O)CHNC2H4NH2)2

B

5470-11-1

hydroxylamine hydrochloride

Conditions
ConditionsYield
In methanol stirring the soln. for 30 min between room temp. and 60°C, pptn.; filtration, washing with water, recrystn. from acetone;A 90%
B n/a
7758-09-0

potassium nitrite

5470-11-1

hydroxylamine hydrochloride

Conditions
ConditionsYield
With hydrogenchloride; sulfur dioxide In water byproducts: H2SO4; react. in water contg. ice and K-acetate leading SO2 into it,mixing,at 0°C;filtering,washing with 0.5 n HCl,hydrolysis at 100°C,for 2h; pptg. of H2SO4 with BaCl2,filtering,evapn.;85%
7647-01-0

hydrogenchloride

7697-37-2

nitric acid

A

5470-11-1

hydroxylamine hydrochloride

B

ammonium chloride

Conditions
ConditionsYield
In sulfuric acid Electrolysis; mixing dild. HCl with dild. HNO3 in an amalgated lead cell as cathode under applying lead anode (anode liquid: dild. H2SO4), 15°C, current: 50 A and 25 V; evapn., then cooling, removing of NH4Cl by treating with cold abs. alc., recrystn. from alcohol;A 80%
B n/a
In sulfuric acid aq. H2SO4; Electrolysis; mixing dild. HCl with dild. HNO3 in an amalgated lead cell as cathode under applying lead anode (anode liquid: dild. H2SO4), 15°C, current: 50 A and 25 V; evapn., then cooling, removing of NH4Cl by treating with cold abs. alc., recrystn. from alcohol;A 80%
B n/a

(E,Z)-(4-chlorophenyl)(cyclopropyl)methanone oxime

A

6640-25-1

4-chlorophenyl cyclopropyl ketone

B

5470-11-1

hydroxylamine hydrochloride

7783-06-4

hydrogen sulfide

2696-92-6

nitrosylchloride

A

5470-11-1

hydroxylamine hydrochloride

B

7704-34-9

sulfur

Conditions
ConditionsYield
In neat (no solvent) byproducts: sulfur chloride, HCl, NO; further by-products: N2, NH4Cl;;A 0%
B n/a
In neat (no solvent) byproducts: sulfur chloride, HCl, NO; further by-products: N2, NH4Cl;;A 0%
B n/a

mercury(II) fulminate

5470-11-1

hydroxylamine hydrochloride

Conditions
ConditionsYield
With hydrogenchloride byproducts: HCO2H; under cooling;
With HCl byproducts: HCO2H; under cooling;

hydroxyammonium sulfate

barium(II) chloride

A

barium sulfate

B

5470-11-1

hydroxylamine hydrochloride

Conditions
ConditionsYield
In water excess of BaCl2; evapn., residue extrd. in a Soxhlet apparate with abs. alcohol, crystn.;
In water excess of BaCl2; evapn., residue extrd. in a Soxhlet apparate with abs. alcohol, crystn.;
5470-11-1

hydroxylamine hydrochloride

Conditions
ConditionsYield
With hydrogenchloride with cooled,concd. HCl; evapn.,dissolving in water,removing of the Hg with H2S,evapn.,crystn.;
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  • Hydroxylamine hydrochloride  CAS:5470-11-1

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    Hydroxylamine hydrochloride CAS:5470-11-1

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    CAS No.: 5470-11-1 EINECS RN: 226-798-2 Molecular Formula: H3NO·HCl Molecular Weight: 69.49 Properties: white crystal. Specific wt. (

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  • 5470-11-1	Hydroxylamine hydrochloride

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    5470-11-1

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    Hydroxylamine hydrochloride CAS NO 5470-11-1

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  • HydroxylamineHydrochloride/HydroxylamineHCLCAS5470-11-1

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    5470-11-1

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Chemistry

Molecular Structure of Hydroxylamine hydrochloride (CAS NO.5470-11-1):

IUPAC Name: Hydroxylamine hydrochloride 
Molecular Formula: H3NO.HCl
Molecular Weight: 69.49
EINECS: 226-798-2
H-Bond Donor: 3
H-Bond Acceptor: 2 
storage temp.: Store at RT.
Water Solubility :560 g/L (20 °C)
Sensitive: Hygroscopic 
Density: 1.67 g/mL at 25 °C(lit.)
Melting Point: 155-157 °C (dec.)(lit.)
Enthalpy of Vaporization: 34.9 kJ/mol
Boiling Point: 56.5 °C at 760 mmHg
Vapour Pressure: 179 mmHg at 25 °C
Appearance: Colorless or off-white crystalline solid
Classification Code: Mutation data 
Canonical SMILES: NO.Cl
InChI: InChI=1S/ClH.H3NO/c;1-2/h1H;2H,1H2
InChIKey: WTDHULULXKLSOZ-UHFFFAOYSA-N
Stability: Substances to be avoided include strong oxidizing agents. Heating above 115 C may cause explosion; do not store above 65C. Moisture and air sensitive.

Uses

 Hydroxylamine hydrochloride (CAS NO.5470-11-1) is used in organic synthesis for preparation of oximes and hydroxamic acids from carboxylic acids, N- and O- substituted hydroxyamines, and addition reactions of carbon-carbon double bond. It is also used as a fixative for textile dyes, auxiliary in some dyeing processes, as a metal extraction and flotation aid, as an antioxidant in fatty acids and soaps, and as a color stabilizer and emulsion additive in color films. Hydroxylamine hydrochloride can be used to remove bromine and polybromide from the solution.
 In surface treatments, Hydroxylamine hydrochloride is used in the preparation of anti-skinning agents, corrosion inhibitors, and cleaner additives. It is also a starting material for pharmaceuticals and agrochemicals manufacturing. In the rubber and plastics industries, it is an antioxidant, vulcanization accelerator, and radical scavenger.

Toxicity Data With Reference

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
dog LDLo subcutaneous 70mg/kg (70mg/kg)   "Abdernalden's Handbuch der Biologischen Arbeitsmethoden." Vol. 4, Pg. 1289, 1935.
mouse LD50 intraperitoneal 10mg/kg (10mg/kg)   National Technical Information Service. Vol. AD277-689,
mouse LD50 oral 408mg/kg (408mg/kg)   Acta Pharmacologica et Toxicologica. Vol. 6, Pg. 285, 1950.
mouse LD50 subcutaneous 125mg/kg (125mg/kg)   Acta Biologica et Medica Germanica. Vol. 21, Pg. 635, 1968.
rat LD50 oral 141mg/kg (141mg/kg) BEHAVIORAL: CONVULSIONS OR EFFECT ON SEIZURE THRESHOLD National Technical Information Service. Vol. OTS0555279,

Consensus Reports

Reported in EPA TSCA Inventory. EPA Genetic Toxicology Program.

Safety Profile

Poison by intraperitoneal and subcutaneous routes. Moderately toxic by ingestion. Mutation data reported. When heated to decomposition it emits very toxic fumes of HCl and NOx.
Safety Information of Hydroxylamine hydrochloride (CAS NO.5470-11-1):
Hazard Codes: HarmfulXn,DangerousN
Risk Statements: 22-36/38-43-48/22-50 
R22:Harmful if swallowed. 
R36/38:Irritating to eyes and skin. 
R43:May cause sensitization by skin contact. 
R48/22:Harmful: danger of serious damage to health by prolonged exposure if swallowed. 
R50:Very toxic to aquatic organisms.
Safety Statements: 22-24-37-61 
S22:Do not breathe dust. 
S24:Avoid contact with skin. 
S37:Wear suitable gloves. 
S61:Avoid release to the environment. Refer to special instructions / safety data sheets.
RIDADR: UN 2923 8/PG 2
WGK Germany: 3
RTECS: NC3675000
F: 21
HazardClass: 8
PackingGroup: III

Specification

 Hydroxylamine hydrochloride (CAS NO.5470-11-1), its Synonyms are Hydroxyamine hydrochloride ; Hydroxyammonium chloride ; Hydroxylamine chloride ; Hydroxylamine chloride (1:1) ; Hydroxylamine-1-hydrochloride ; Hydroxylammonium chloride ; Oxammonium hydrochloride .