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| CAS No.: | 5470-70-2 |
|---|---|
| Name: | Methyl 6-methylnicotinate |
| Article Data: | 28 |
| Molecular Structure: | |
|
|
|
| Formula: | C8H9NO2 |
| Molecular Weight: | 151.165 |
| Synonyms: | 3-pyridinecarboxylic acid, 6-methyl-, methyl ester;3-(Methoxycarbonyl)-6-methylpyridine;5-Methoxycarbonyl-2-methylpyridine;6-Methyl-3-pyridinecarboxylic acid methylester;6-Methylnicotinic acid methyl ester;Methyl6-methyl-3-pyridinecarboxylate;Methyl 6-methylaminonicotinate;6-Methyl nicotinic acid methyl ester;methyl 6-methylpyridine-3-carboxylate; |
| EINECS: | 1308068-626-2 |
| Density: | 1.104 g/cm3 |
| Melting Point: | 34-37 °C(lit.) |
| Boiling Point: | 228.4 °C at 760 mmHg |
| Flash Point: | 80.6 °C |
| Appearance: | Brown Solid |
| Hazard Symbols: |
 Xi
|
| Risk Codes: | 36/37/38 |
| Safety: | 26 |
| PSA: | 39.19000 |
| LogP: | 1.17660 |
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- 5470-70-2
Methyl 6-methylnicotinate
| Conditions | Yield |
|---|---|
| With indium; cobalt(II) chloride In methanol at 20℃; for 2h; sonication; | 80% |
| Conditions | Yield |
|---|---|
| With sulfuric acid for 17h; Reflux; | 75% |
| With sulfuric acid for 21h; Heating; Yield given; | |
| With sulfuryl dichloride |
| Conditions | Yield |
|---|---|
| In benzene for 5h; Heating; | 41% |
- 646-06-0
1,3-DIOXOLANE
- 93-60-7
methyl 3-pyridinecarboxylate
A
- 5470-70-2
Methyl 6-methylnicotinate
B
- 69971-44-4
Methyl 4,6-Dimethylnicotinate
| Conditions | Yield |
|---|---|
| With sulfuric acid for 7h; Irradiation; | A 21% B 5% |
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N-methoxylamine hydrochloride
- 5470-70-2
Methyl 6-methylnicotinate
| Conditions | Yield |
|---|---|
| With sodium acetate In ethanol at 150℃; for 3h; Inert atmosphere; Microwave irradiation; | 14% |
- 67-56-1
methanol
- 93-60-7
methyl 3-pyridinecarboxylate
A
- 33402-75-4
4-methylnicotinic acid methyl ester
B
- 5470-70-2
Methyl 6-methylnicotinate
C
- 67367-26-4
2-methoxynicotinic acid methyl ester
D
- 26218-80-4
6-methoxy-nicotinic acid methyl ester
| Conditions | Yield |
|---|---|
| With sulfuric acid for 1h; Product distribution; Mechanism; Irradiation; effect of additives; variation of temp., acid concn.; further alcohol; | A 7.1% B 9.5% C 8.8% D 3.8% |
| With sulfuric acid for 1h; Irradiation; | A 7.1% B 9.5% C 8.8% D 3.8% |
| With sulfuric acid at 32℃; for 0.833333h; Product distribution; Mechanism; Irradiation; var. reagent, acid concentration and time; |
| Conditions | Yield |
|---|---|
| In dichloromethane Ambient temperature; | |
| With triethylamine for 3h; |
- 93-60-7
methyl 3-pyridinecarboxylate
- 676-58-4
methylmagnesium chloride
- 1885-14-9
phenyl chloroformate
A
- 33402-75-4
4-methylnicotinic acid methyl ester
B
- 5470-70-2
Methyl 6-methylnicotinate
| Conditions | Yield |
|---|---|
| With sulfur Yield given. Multistep reaction; | |
| With sulfur Yield given. Multistep reaction; |
- 5470-70-2
Methyl 6-methylnicotinate
| Conditions | Yield |
|---|---|
| With hydrogenchloride |
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: SOCl2 / 2 h / Heating 2: CH2Cl2 / Ambient temperature View Scheme | |
| Multi-step reaction with 2 steps 1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 3 h / 0 - 20 °C / Inert atmosphere 2: triethylamine / 3 h View Scheme |
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Chemistry
Molecular Structure of Methyl 6-methylnicotinate (CAS NO.5470-70-2):
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IUPAC Name: methyl 6-methylpyridine-3-carboxylate
BRN: 122940
Empirical Formula: C8H9NO2
Molecular Weight: 151.1626
Packaging: 1.10 g in glass btl
H bond acceptors: 3
H bond donors: 0
Freely Rotating Bonds: 2
Polar Surface Area: 39.19 Å2
Index of Refraction: 1.51
Molar Refractivity: 40.94 cm3
Molar Volume: 136.8 cm3
Surface Tension: 39.9 dyne/cm
Density: 1.104 g/cm3
Flash Point: 80.6 °C
Enthalpy of Vaporization: 46.5 kJ/mol
Boiling Point: 228.4 °C at 760 mmHg
Vapour Pressure: 0.0736 mmHg at 25°C
Melting point: 34-37 °C(lit.)
Product Categories: Carboxylicester; Acids and Derivatives; Heterocycles; Esters; Pyridines; Organic acids; Nicotine Derivatives; Pyridine
Safety Profile
Hazard Codes: 
Xi
Risk Statements information :
36/37/38: Irritating to eyes, respiratory system and skin
The Safety Statements information of Methyl-6-methylnictinate (CAS NO.5470-70-2):
26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
WGK Germany: 3
Hazard Note: Irritant
Specification
Methyl 6-methylnicotinate , with CAS number of 5470-70-2, can be called 3-pyridinecarboxylic acid, 6-methyl-, methyl ester ; 3-(Methoxycarbonyl)-6-methylpyridine ; 5-Methoxycarbonyl-2-methylpyridine ; 6-Methyl-3-pyridinecarboxylic acid methylester ; 6-Methylnicotinic acid methyl ester ; Methyl6-methyl-3-pyridinecarboxylate ; Methyl 6-methylaminonicotinate ; 6-Methyl nicotinic acid methyl ester . It is a brown solid.