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56718-76-4

Basic Information
CAS No.: 56718-76-4
Name: rac 1-Chloro-3-[4-(2-methoxyethyl)phenoxy]-2-propanol
Article Data: 8
Molecular Structure:
Molecular Structure of 56718-76-4 (rac 1-Chloro-3-[4-(2-methoxyethyl)phenoxy]-2-propanol)
Formula: C12H17ClO3
Molecular Weight: 244.718
Synonyms: rac 1-Chloro-3-[4-(2-methoxyethyl)phenoxy]-2-propanol
Density: 1.157g/cm3
Boiling Point: 364.5°C at 760 mmHg
Flash Point: 174.2°C
Hazard Symbols: Xn
Risk Codes: 22
PSA: 38.69000
LogP: 1.85400
Synthetic route
56718-70-8

2-[4-(2'-methoxyethyl)phenoxymethyl]oxirane

56718-76-4

(+/-)-1-[4-(2-methoxyethyl)phenoxy]-3-chloro-2-propanol

Conditions
ConditionsYield
With morpholine; 1,3,5-trichloro-2,4,6-triazine In water at 20℃; for 0.5h;98%
Stage #1: 2-[4-(2'-methoxyethyl)phenoxymethyl]oxirane With β‐cyclodextrin In water; acetone at 60℃;
Stage #2: With thionyl chloride In water; acetone at 20℃; for 10h;
91%
With zirconyl chloride In acetonitrile at 20℃; for 1.16667h;80%
With water; acetyl chloride In dichloromethane for 12h;
56718-71-9

4-(2-methoxyethyl)phenol

106-89-8

epichlorohydrin

A

56718-70-8

2-[4-(2'-methoxyethyl)phenoxymethyl]oxirane

B

56718-76-4

(+/-)-1-[4-(2-methoxyethyl)phenoxy]-3-chloro-2-propanol

Conditions
ConditionsYield
With sodium hydroxideA 90%
B 10%
Stage #1: 4-(2-methoxyethyl)phenol With potassium hydroxide In methanol at 40 - 45℃; for 1h;
Stage #2: epichlorohydrin at 40℃; for 24h;
With sodium hydroxide In water at 30 - 40℃; for 5h; Temperature;
56718-71-9

4-(2-methoxyethyl)phenol

56718-76-4

(+/-)-1-[4-(2-methoxyethyl)phenoxy]-3-chloro-2-propanol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: NaOH / 12 h / 20 °C
2.1: β-cyclodextrin / H2O; acetone / 60 °C
2.2: 91 percent / thionyl chloride / H2O; acetone / 10 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: potassium carbonate / acetonitrile / 24 h / 85 °C
2: water; acetyl chloride / dichloromethane / 12 h
View Scheme
2491-38-5

2-bromo-1-(4'-hydroxyphenyl)-1-ethanone

56718-76-4

(+/-)-1-[4-(2-methoxyethyl)phenoxy]-3-chloro-2-propanol

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: methanol
2: H2; AcOH / Pd/C
3: 10 percent / aq. NaOH
View Scheme
32136-81-5

alpha-methoxy-4-hydroxyacetophenone

56718-76-4

(+/-)-1-[4-(2-methoxyethyl)phenoxy]-3-chloro-2-propanol

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: H2; AcOH / Pd/C
2: 10 percent / aq. NaOH
View Scheme
99-93-4

4-Hydroxyacetophenone

56718-76-4

(+/-)-1-[4-(2-methoxyethyl)phenoxy]-3-chloro-2-propanol

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: CuBr2 / ethyl acetate
2: methanol
3: H2; AcOH / Pd/C
4: 10 percent / aq. NaOH
View Scheme
56718-71-9

4-(2-methoxyethyl)phenol

106-89-8

epichlorohydrin

56718-76-4

(+/-)-1-[4-(2-methoxyethyl)phenoxy]-3-chloro-2-propanol

Conditions
ConditionsYield
Stage #1: 4-(2-methoxyethyl)phenol With potassium hydroxide In methanol at 40 - 45℃; for 1h;
Stage #2: epichlorohydrin at 40℃; for 24h;
Stage #3: With acetic acid; lithium chloride In tetrahydrofuran at 20℃; for 48h;
34.88 g
56718-71-9

4-(2-methoxyethyl)phenol

106-89-8

epichlorohydrin

A

C21H28O5

B

56718-70-8

2-[4-(2'-methoxyethyl)phenoxymethyl]oxirane

C

56718-76-4

(+/-)-1-[4-(2-methoxyethyl)phenoxy]-3-chloro-2-propanol

Conditions
ConditionsYield
With tetrabutyl-ammonium chloride at 110℃; under 2100.21 Torr; for 0.95h; Flow reactor;
111-63-7

vinyl stearate

56718-76-4

(+/-)-1-[4-(2-methoxyethyl)phenoxy]-3-chloro-2-propanol

1107647-82-4

(2S)-1-chloro-3-[4-(2-methoxyethyl)phenoxy]-2-propyl stearate

Conditions
ConditionsYield
With Novozym 435 In hexane; acetone at 37℃; for 28h; Molecular sieve;35.4%
108-05-4

vinyl acetate

56718-76-4

(+/-)-1-[4-(2-methoxyethyl)phenoxy]-3-chloro-2-propanol

A

Acetic acid (R)-1-chloromethyl-2-[4-(2-methoxy-ethyl)-phenoxy]-ethyl ester

B

Acetic acid (S)-1-chloromethyl-2-[4-(2-methoxy-ethyl)-phenoxy]-ethyl ester

Conditions
ConditionsYield
In various solvent(s) at 25℃; for 144h; native lipase B from Candida antarctica; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
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    Our company mainly engage in product research and production. Our company has been committed to providing products of high service , high levels and low impurities for biomedical r

  • Hebei Huanchang Metallurgical Materials Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86-18532084303

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  • rac 1-Chloro-3-[4-(2-methoxyethyl)phenoxy]-2-propanol

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    rac 1-Chloro-3-[4-(2-methoxyethyl)phenoxy]-2-propanol

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    Prime Molecular Co., Ltd. is a high-tech enterprise providing comprehensive customer service for pharmaceutical companies at home and abroad in accordance with international standards. Two R&D centers and two production sites in China, all well-equip

    Prime Molecular Co., Ltd. is an advanced chemical intermediates manufacture with ?two R&D centers and two production sites in China, all well-equipped with dedicated and profession

  • PRIME MOLECULAR CO.,LIMITED

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

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  • rac 1-Chloro-3-[4-(2-methoxyethyl)phenoxy]-2-propanol

  • Casno:

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    rac 1-Chloro-3-[4-(2-methoxyethyl)phenoxy]-2-propanol

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    1.Fast and safety delivery by well-reputed shipping line;2.we have our own chemical laboratory and factory3.Reasonable price, excellent quality and attentive service.4.prompt reply.we can reply your inquiry within 12 hours.5.sample free(depends on pr

    We are a manufacturer and trader in China, with 10 years of experience in the export of chemical and pharmaceutical raw materials and 320 employees. We are all promoted on Made in

  • Hebei Zhaojun New Material Technology Co., LTD

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+8617320695765

    Address:Qiu County gucheng ying Town Zhang Zhang Lu villag

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  • Metoprolol USP Related Compound B

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    Metoprolol USP Related Compound B

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    Topbatt Chemical Co., Ltd., Established in 2019, located in Shenzhen, Guangdong Province, is a Manufacturer and Trading company which specialized in fine chemicals like Pharmaceutical Reference Standards and Stable Isotopes. Our Stable Isotopes produ

    Topbatt Chemical Co. Ltd., Established in 2019, located in Shenzhen, Guangdong Province, is a Manufacturer and Trading company which specialized in fine chemicals like Pharmaceutic

  • Topbatt Chemical Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:13828841343

    Address:Rm#A802, National Engineering Laboratory Building, Nanshan District, Shenzhen, China

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  • 56718-76-4

  • Casno:

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    56718-76-4

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    Supply top quality products with a reasonable price Application:api

    Hebei Ruishun Trade Co.,Ltd registered capital one million, we have a production of pharmaceutical raw materials, pharmaceutical raw materials factory reagent r&d center, we do

  • Hebei Ruishun Trade Co.,Ltd

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86-311-68037669

    Address:WanDa commerce building ,yuhua district

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  • Metoprolol USP Related Compound B

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    56718-76-4

    Metoprolol USP Related Compound B

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    1. Our staff are all biomedical related majors with rich experience in the pharmaceutical industry, and can provide you with more professional services.2. Our supplier has a good quality management system, and the quality of products is reliable and

  • Shenzhen Sumshine Biotech Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:15914108025

    Address:229A, No.15, Xinbeli Industrial Zone, Xinshi Community, Dalang Street, Longhua District

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  • Metoprolol Related Compound B

  • Casno:

    56718-76-4

    Metoprolol Related Compound B

    Min.Order: 0

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    High purity Application:Pharmaceutical intermediates, Material synthesis and analyzing the expectant ingredients

    Novachemistry offers a broad range of specialty chemicals and customized synthesis services to a range of pharmaceutical, agrochemical and biochemical industries. Novachemistry has

  • NovaChemistry

    United Kingdom  |  Contact Details

    Business Type:Trading Company

    Tel:+44 (0)208 191 7890

    Address:Unit11, Ark Business Centre, Gorden Road, Loughborough, United Kingdom

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