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CAS No.: | 56962-11-9 |
---|---|
Name: | 2-Chloro-4-hydroxybenzaldehyde |
Article Data: | 14 |
Molecular Structure: | |
Formula: | C7H5ClO2 |
Molecular Weight: | 156.569 |
Synonyms: | o-Chloro-p-hydroxybenzaldehyde; |
Density: | 1.404 g/cm3 |
Melting Point: | 145-147 °C(lit.) |
Boiling Point: | 272.492 °C at 760 mmHg |
Flash Point: | 118.599 °C |
Hazard Symbols: | Xi |
Risk Codes: | 36/37/38 |
Safety: | 26-37/39 |
PSA: | 37.30000 |
LogP: | 1.85810 |
2-chloro-4-hydroxybenzonitrile
2-chloro-4-hydroxybenzaldehyde
Conditions | Yield |
---|---|
Stage #1: 2-chloro-4-hydroxybenzonitrile With diisobutylaluminium hydride In tetrahydrofuran; hexane at -78 - 20℃; for 19h; Stage #2: With hydrogenchloride In tetrahydrofuran; hexane; water at 0℃; | 84% |
With diisobutylaluminium hydride In tetrahydrofuran; hexane at -78 - 20℃; for 3h; | |
Stage #1: 2-chloro-4-hydroxybenzonitrile With diisobutylaluminium hydride In hexane; chloroform at -50℃; for 1.5h; Stage #2: With hydrogenchloride In methanol; water |
Conditions | Yield |
---|---|
Stage #1: 3-monochlorophenol; chloroform With calcium hydroxide; water; sodium carbonate for 4.33333h; Heating / reflux; Stage #2: With hydrogenchloride In chloroform; water | 16% |
With water; sodium carbonate; calcium hydroxide for 4.33333h; Inert atmosphere; Reflux; | 15.3% |
With sodium carbonate; calcium hydroxide In water for 3h; Reflux; Inert atmosphere; | 15.3% |
Conditions | Yield |
---|---|
With hydrogenchloride; aluminium trichloride; benzene at 30℃; Durch Erhitzen des Reaktionsproduktes mit verd. Salzsaeure; |
2-chloro-4-nitrotoluene
2-chloro-4-hydroxybenzaldehyde
Conditions | Yield |
---|---|
With sodium hydroxide; sulfur Diazotieren des Reaktionsproduktes und nachfolgendes Kochen mit 40prozentiger Schwefelsaeure; |
2,4-dichlorobenzaldeyhde
2-chloro-4-hydroxybenzaldehyde
Conditions | Yield |
---|---|
With potassium carbonate at 220℃; unter Druck; |
3-monochlorophenol
trichloroacetic acid
A
4-chlorosalicylaldehyde
B
2-chloro-4-hydroxybenzaldehyde
Conditions | Yield |
---|---|
With potassium hydroxide; water |
Conditions | Yield |
---|---|
With sodium hydroxide Mengenverhaeltnis zwischen den Produkten; | |
With extinguished lime; sodium carbonate; calcium carbonate |
Conditions | Yield |
---|---|
With sodium hydroxide Mengenverhaeltnis zwischen den Produkten; |
3-monochlorophenol
trichloroacetic acid
A
4-chlorosalicylaldehyde
B
2-chloro-4-hydroxybenzaldehyde
Conditions | Yield |
---|---|
With ammonium hydroxide In methanol; water at 0 - 20℃; for 28h; Inert atmosphere; | 100% |
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