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| CAS No.: | 571-58-4 |
|---|---|
| Name: | 1,4-Dimethylnaphthalene |
| Article Data: | 100 |
| Molecular Structure: | |
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|
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| Formula: | C12H12 |
| Molecular Weight: | 156.227 |
| Synonyms: | 1,4-Dimethylnaphthalene;NSC 61779 |
| Density: | 1g/cm3 |
| Melting Point: | −18 °C(lit.) |
| Boiling Point: | 268°Cat760mmHg |
| Flash Point: | 109.2°C |
| PSA: | 0.00000 |
| LogP: | 3.45660 |
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- 99170-93-1N-Methyl-2-oxazolamine
- 717878-06-31-(4-fluorophenyl)-4-nitro-1H-imidazole
- 914458-26-7[5-(2-fluorophenyl)-1-pentyl-1H-pyrrol-3-yl]-1-naphthalenyl-Methanone
- 894852-01-87-BROMO-2,2-DIMETHYL-2H-PYRIDO[3,2-B][1,4]OXAZIN-3(4H)-ONE
| Conditions | Yield |
|---|---|
| With chloro-trimethyl-silane; sodium iodide In acetonitrile at 70℃; for 24h; Reagent/catalyst; Solvent; Inert atmosphere; | 97% |
- 59080-17-0
(4-fluoronaphthalen-1-yl)(methyl)sulfane
- 75-16-1
methylmagnesium bromide
- 571-58-4
1,4-dimethylnaphthalene
| Conditions | Yield |
|---|---|
| With [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](triphenylphosphine)nickel(II) dichloride In diethyl ether; toluene at 20℃; for 8h; Schlenk technique; Inert atmosphere; Sealed tube; | 95% |
- 10075-73-7
1,4-bis(methylthio)naphthalene
- 75-16-1
methylmagnesium bromide
- 571-58-4
1,4-dimethylnaphthalene
| Conditions | Yield |
|---|---|
| With [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](triphenylphosphine)nickel(II) dichloride In diethyl ether; toluene at 20℃; for 8h; Schlenk technique; Inert atmosphere; Sealed tube; | 95% |
| Conditions | Yield |
|---|---|
| With chloro-trimethyl-silane; sodium iodide In acetonitrile at 0 - 20℃; for 24h; | 92% |
| With sodium tetrahydroborate; trifluoroacetic acid In tetrahydrofuran at 20 - 25℃; overnight; | 90% |
| With n-butyllithium; tungsten(VI) chloride In tetrahydrofuran; hexane 1.) -78 deg C, 1 h, 2.) from -78 deg C to room temp., 1 h, 3.) 5 h; | 88% |
| With isopropylmagnesium bromide In tetrahydrofuran for 2h; Heating; | 73% |
- 35461-84-8
1,4-dimethylnaphtalene-1,4-endoperoxide
- 75-07-0
acetaldehyde
A
- 571-58-4
1,4-dimethylnaphthalene
- 87051-08-9
(4aS,10aR)-2,4a,9-Trimethyl-4a,10a-dihydro-1,3,4-trioxa-phenanthrene
| Conditions | Yield |
|---|---|
| With trimethylsilyl trifluoromethanesulfonate In dichloromethane at -78℃; for 1h; | A 5% B 87% |
- 75-16-1
methylmagnesium bromide
- 95332-88-0
methyl(4-methylnaphthalen-1-yl)sulfane
- 571-58-4
1,4-dimethylnaphthalene
| Conditions | Yield |
|---|---|
| With [1,3-bis(2,6-diisopropylphenyl)imidazol-2-ylidene](triphenylphosphine)nickel(II) dichloride In diethyl ether; toluene at 20℃; for 8h; Schlenk technique; Inert atmosphere; Sealed tube; | 87% |
- 42409-86-9
1,2-bis-(4-methyl-[1]naphthyl)-ethane
A
- 571-58-4
1,4-dimethylnaphthalene
B
- 2717-33-1
5,8-dimethyl-1,4-dihydronaphthalene
| Conditions | Yield |
|---|---|
| With potassium at 5℃; for 6h; | A 85% B 2% |
- 571-58-4
1,4-dimethylnaphthalene
| Conditions | Yield |
|---|---|
| With chlorosulfonic acid In chloroform at 0℃; | 85% |
- 35461-84-8
1,4-dimethylnaphtalene-1,4-endoperoxide
- 67-64-1
acetone
A
- 571-58-4
1,4-dimethylnaphthalene
- 87051-09-0
3,3,6,10b-tetramethyl-4a,10b-dihydronaphtho<2,1-e><1,2,4>trioxane
| Conditions | Yield |
|---|---|
| With trimethylsilyl trifluoromethanesulfonate In dichloromethane at -78℃; for 1h; | A 5% B 83% |
- 97585-87-0
(4-Methyl-naphthalen-1-ylmethyl)-triphenyl-phosphonium; chloride
A
- 571-58-4
1,4-dimethylnaphthalene
B
- 791-28-6
Triphenylphosphine oxide
| Conditions | Yield |
|---|---|
| With sodium hydroxide In ethanol; water Heating; | A 70% B n/a |
