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5763-44-0

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Basic Information
CAS No.: 5763-44-0
Name: Cyclopentane-1,2-dicarboximude
Article Data: 8
Molecular Structure:
Molecular Structure of 5763-44-0 (Cyclopentane-1,2-dicarboximude)
Formula: C7H9NO2
Molecular Weight: 139.154
Synonyms: 3-azabicyclo[3.3.0]octane-2,4-dione;1,2-Cyclopentanedicarboximide;Cyclopenta[c]pyrrole-1,3(2H,3aH)-dione,tetrahydro-;Cyclopentane-1,2-dicarboximide;Cyclopentane-1,2-dicarboximude;
EINECS: 240-071-7
Density: 1.242g/cm3
Melting Point: 168 °C (dec.)
Boiling Point: 322.2°C at 760 mmHg
Flash Point: 162.2°C
PSA: 46.17000
LogP: 0.38790
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Synthetic route
90474-13-8

diethyl cyclopentane-1,2-dicarboxylate

5763-44-0

4,5,6,6a-tetrahydro-3aH-cyclopenta[c]pyrrole-1,3-dione

Conditions
ConditionsYield
With ammonia at 130 - 280℃; for 5h; Product distribution / selectivity; autoclave; Pyrolysis; Industry scale;96%
50483-99-3

trans-DL-1,2-cyclopentanedicarboxylic acid

77287-34-4, 77287-35-5, 60100-09-6

formamide

5763-44-0

4,5,6,6a-tetrahydro-3aH-cyclopenta[c]pyrrole-1,3-dione

Conditions
ConditionsYield
at 170℃; Temperature; Inert atmosphere;93.5%

cyclopentane-1,2-dicarboxamide

2-carbamylcyclopentane-1-carboxylic acid

5763-44-0

4,5,6,6a-tetrahydro-3aH-cyclopenta[c]pyrrole-1,3-dione

Conditions
ConditionsYield
In diphenylether at 240℃; for 2.5h; Temperature; Inert atmosphere; Industrial scale;92.6%
cyclopentane-dicarboxylic acid-(1.2)-anhydride

cyclopentane-dicarboxylic acid-(1.2)-anhydride

5763-44-0

4,5,6,6a-tetrahydro-3aH-cyclopenta[c]pyrrole-1,3-dione

Conditions
ConditionsYield
With ammonia at 180℃;

C13H20N2O

5763-44-0

4,5,6,6a-tetrahydro-3aH-cyclopenta[c]pyrrole-1,3-dione

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: sulfuric acid / toluene; water / 4 h / 120 °C
2: chlorine / 1,2-dichloro-ethane / 10 h / -10 - 0 °C
3: ammonium hydroxide / 5 h / -10 - 0 °C
4: trans-DL-1,2-cyclopentanedicarboxylic acid / 2 h / 220 - 240 °C
View Scheme
22945-27-3

cyclohexanone-2-carboxamide

5763-44-0

4,5,6,6a-tetrahydro-3aH-cyclopenta[c]pyrrole-1,3-dione

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: chlorine / 1,2-dichloro-ethane / 10 h / -10 - 0 °C
2: ammonium hydroxide / 5 h / -10 - 0 °C
3: trans-DL-1,2-cyclopentanedicarboxylic acid / 2 h / 220 - 240 °C
View Scheme

cyclopentane-1,2-dicarboxamide

5763-44-0

4,5,6,6a-tetrahydro-3aH-cyclopenta[c]pyrrole-1,3-dione

Conditions
ConditionsYield
With trans-DL-1,2-cyclopentanedicarboxylic acid at 220 - 240℃; for 2h;
6940-78-9

4-chlorobutyl bromide

5763-44-0

4,5,6,6a-tetrahydro-3aH-cyclopenta[c]pyrrole-1,3-dione

2-(4-chlorobutyl)tetrahydrocyclopenta[c]pyrrole-1,3(2H,3aH)-dione

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 0 - 20℃;98%
5763-44-0

4,5,6,6a-tetrahydro-3aH-cyclopenta[c]pyrrole-1,3-dione

tert-butyl 4-[4-chloro-2-[2-(hydroxymethyl)thieno[3,2-b]pyridin-7-yl]-6-methyl-phenoxy]piperidine-1-carboxylate

tert-butyl 4-(4-chloro-2-(2-((1,3-dioxohexahydrocyclopenta[c]pyrrol-2(1H)-yl)methyl)thieno[3,2-b]pyridin-7-yl)-6-methylphenoxy)piperidine-1-carboxylate

Conditions
ConditionsYield
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 60℃; for 2h; Mitsunobu Displacement;69%
5763-44-0

4,5,6,6a-tetrahydro-3aH-cyclopenta[c]pyrrole-1,3-dione

C7H8ClNO2

Conditions
ConditionsYield
With trichloroisocyanuric acid In dichloromethane at 0 - 20℃; for 4h; Inert atmosphere; Schlenk technique;64%
Raw Materials
90474-13-8
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    5763-44-0

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    Business Type:Trading Company

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    5763-44-0

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    Product name: 1,2-Cyclopentane Dicarboximide CAS No.：5763-44-0 Molecule Formula：C7H9NO2 Molecule Weight：139.15 Purity: 99.0% Package: 25kg/drum Description：Off-white crystalline powder Manufacture Standards：Enterprise Standard

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    5763-44-0

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    Cyclopentane-1,2-dicarboximude Chemical Properties Melting point 168 °C (dec.) Boiling point 322.2±11.0 °C(Predicted) density 1.242±0.06 g/cm3(Predicted) pka 11.

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  • Casno:

    5763-44-0

    5763-44-0

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  • Tetrahydrocyclopenta[c]pyrrole-1,3(2H,3aH)-dione cas no. 5763-44-0 98%

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  • Casno:

    5763-44-0

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    Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe

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  • Casno:

    5763-44-0

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  • Casno:

    5763-44-0

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    R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates

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     China (Mainland)  |  Contact Details

    Business Type:Manufacturers

    Tel:86-571-86465881,86-571-87157530,86-571-88025800

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