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CAS No.: | 5833-18-1 |
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Name: | BIS(2,4-DINITROPHENYL)ACETIC ACID ETHYL ESTER |
Molecular Structure: | |
Formula: | C16H12 N4 O10 |
Molecular Weight: | 420.292 |
Synonyms: | Aceticacid, bis(2,4-dinitrophenyl)-, ethyl ester (7CI,8CI); Ethylbis(2,4-dinitrophenyl)acetate; NSC 8659 |
Density: | 1.556g/cm3 |
Melting Point: | 156 °C |
Boiling Point: | 629.3°Cat760mmHg |
Flash Point: | 269.3°C |
Appearance: | yellow to ochre fine crystalline powder |
PSA: | 209.58000 |
LogP: | 5.10720 |
2,4-dinitrobromobenzene
ethanol
(2,4-dinitro-phenyl)-malonic acid diethyl ester; sodium-compound
ethyl 2,2-bis(2,4-dinitrophenyl)acetate
2,4-dinitrobromobenzene
α-(2,4-dinitrophenyl)ethyl acetate
ethyl 2,2-bis(2,4-dinitrophenyl)acetate
Conditions | Yield |
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With ethanol; sodium ethanolate |
2,4-dinitrobromobenzene
sodium ethyl acetylacetate enolate
ethyl 2,2-bis(2,4-dinitrophenyl)acetate
Conditions | Yield |
---|---|
With sodium hydroxide Behandeln mit 4-Brom-1.3-dinitro-benzol; |
Conditions | Yield |
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With nitric acid at -18℃; Behandeln der Loesung mit rauchender Schwefelsaeure; | |
(nitration); |
2,4-dinitrobromobenzene
ethyl acetoacetate
A
ethyl 2,2-bis(2,4-dinitrophenyl)acetate
B
2-(2,4-dinitrophenyl)-3-oxobutyric acid ethyl ester
Conditions | Yield |
---|---|
With ethanol; sodium ethanolate |
ethyl acetoacetate
1-chloro-2,4-dinitro-benzene
A
ethyl 2,2-bis(2,4-dinitrophenyl)acetate
B
2-(2,4-dinitrophenyl)-3-oxobutyric acid ethyl ester
Conditions | Yield |
---|---|
With ethanol; sodium ethanolate |
2-(2,4-dinitrophenyl)-3-oxobutyric acid ethyl ester
sodium ethanolate
1-chloro-2,4-dinitro-benzene
ethyl 2,2-bis(2,4-dinitrophenyl)acetate
sodium diethylmalonate
sodium ethanolate
1-chloro-2,4-dinitro-benzene
A
diethyl (2,4-dinitrophenyl)malonate
B
ethyl 2,2-bis(2,4-dinitrophenyl)acetate
Conditions | Yield |
---|---|
With ethanol Behandeln einer wss. Loesung des Reaktionsprodukts mit wss. Schwefelsaeure; |
Conditions | Yield |
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Multi-step reaction with 2 steps 1: alcohol 2: NaOH-solution / Behandeln mit 4-Brom-1.3-dinitro-benzol View Scheme |