CAS No.598-57-2,N-nitromethylamine Suppliers

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Basic Information

Molecular Structure:
CAS No.:	598-57-2
Name:	N-nitromethylamine
Article Data:	26

Formula:	CH4 N2 O2
Molecular Weight:	76.055
Synonyms:	Methylamine,N-nitro- (6CI,7CI,8CI); Methylnitramine; Methylnitroamine; N-Methylnitramine;N-Nitromethylamine; NSC 137855
Density:	1.236g/cm³
Melting Point:	38°C
Boiling Point:	155.2°Cat760mmHg
Flash Point:	47.6°C
Safety:	Moderately toxic by intraperitoneal route. Questionable carcinogen with carcinogenic data. Mutation data reported. Explodes on contact with concentrated sulfuric acid. When heated to decomposition it emits toxic fumes of NO_x. See also NITRO COMPOUNDS and AMINES.
PSA:	57.85000
LogP:	0.31160

Synthetic route

: 96-31-1
N,N'-Dimethylurea

: 598-57-2
methylnitroamine

Conditions

Conditions	Yield
Stage #1: N,N'-Dimethylurea With sulfuric acid; nitric acid In dichloromethane at -5 - 0℃; Stage #2: In water at 20℃; for 1h; Temperature;	89.2%

: 141-52-6
sodium ethanolate

: 99647-88-8
1-phenyl-3-(methylnitroamino)-2-propen-1-one

A: 36234-10-3
3-Oxo-3-phenylpropanal 1-(diethylacetal)

B: 598-57-2
methylnitroamine

Conditions

Conditions	Yield
In ethanol at 35 - 40℃; for 3h;	A 65% B n/a

...Expand

: 186581-53-3, 908094-01-9
diazomethane

: 556-89-8
nitrourea

: 598-57-2
methylnitroamine

: 186581-53-3, 908094-01-9
diazomethane

: N-nitro-N'-ethyl-urea

A: 598-57-2
methylnitroamine

B: 4164-28-7
N-nitrodimethylamine

C: 109-90-0
ethyl isocyanate

...Expand

: 687-48-9
ethyl N,N-dimethylcarbamate

: 598-57-2
methylnitroamine

Conditions

Conditions	Yield
With nitric acid nimmt das erhaltene Nitromethylurethan mit Aether auf und leitet in die aether. Loesung trocknes NH3 ein;

: 14442-54-7
methyl-nitro-carbamic acid methyl ester

: 598-57-2
methylnitroamine

Conditions

Conditions	Yield
With diethyl ether; ammonia der Entstandene Niederschlag des Ammoniumsalzes mit Aether gewaschen und durch Kochen mit Alkohol zersetzt wird;

: 91086-49-6
bis-(N-methyl-N-ethoxycarbonylamino)methane

: 598-57-2
methylnitroamine

Conditions

Conditions	Yield
With nitric acid at -8℃; Leiten von NH3 in die aether.Loesung des Reaktionsprodukts;

: 14760-99-7
N,N’-dimethyl-N,N’-dinitrooxalamide

: 598-57-2
methylnitroamine

Conditions

Conditions	Yield
With ammonium hydroxide Entsteht als Ammoniumsalz;
With barium dihydroxide; water man faellt freien Baryt durch CO2, dammpft die Loesung ein, versetzt den Rueckstand mit der theoretischen Menge Schwefelsaeure und nimmt das freie Methylnitramin in Aether auf;
With ammonia at 5 - 20℃; under 6000.6 Torr; for 0.333333h; Autoclave;	0.61 g

: 60-29-7
diethyl ether

: N-methyl-N-nitro-N'-phenyl-urea

: 62-53-3
aniline

A: 598-57-2
methylnitroamine

B: 603-54-3
N,N-diphenylurea

...Expand

: 598-50-5
N-Methylurea

: 598-57-2
methylnitroamine

Conditions

Conditions	Yield
Nitrierung von Methylharnstoff und letzterer zerfaellt bei der Aufarbeitung des Reaktionsprodukts durch Behandeln mit Ammoniak;

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Chemistry

IUPAC Name: Nitromethanamine
Synonyms of N-Nitromethylamine (CAS NO.598-57-2) : Methanamine, N-nitro- (9CI) ; Methyl nitramine (dry) [Forbidden] ; Nitramine, methyl-
InChI:InChI=1/CH4N2O2/c2-1-3(4)5/h1-2H2
CAS NO:598-57-2
Molecular Formula:CH₄N₂O₂
Molecular Weight :76.0547
Molecular Structure :
Index of Refraction: 1.44
Surface Tension: 45.2 dyne/cm
Density: 1.236 g/cm³
Flash Point: 47.6 °C
Enthalpy of Vaporization: 39.19 kJ/mol
Boiling Point: 155.2 °C at 760 mmHg
Vapour Pressure: 3.07 mmHg at 25°C

Toxicity Data With Reference

Organism	Test Type	Route	Reported Dose (Normalized Dose)	Effect	Source
mouse	LD50	intraperitoneal	500mg/kg (500mg/kg)		Pharmaceutical Chemistry Journal Vol. 10, Pg. 1504, 1976.

Safety Profile

N-Nitromethylamine (CAS NO.598-57-2) is moderately toxic by intraperitoneal route. Questionable carcinogen with carcinogenic data. Mutation data reported. Explodes on contact with concentrated sulfuric acid. When N-Nitromethylamine (CAS NO.598-57-2) is heated to decomposition ,it emits toxic fumes of NO_x. See also NITRO COMPOUNDS and AMINES.

Standards and Recommendations

DOT Classification: Forbidden