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598-74-3

Basic Information
CAS No.: 598-74-3
Name: 1,2-Dimethylpropylamine
Article Data: 30
Molecular Structure:
Molecular Structure of 598-74-3 (1,2-Dimethylpropylamine)
Formula: C5H13 N
Molecular Weight: 87.1649
Synonyms: Propylamine,1,2-dimethyl- (6CI,7CI,8CI); (3-Methylbutan-2-yl)amine; (?à)-3-Methyl-2-butanamine; (?à)-3-Methyl-2-butylamine;1,2-Dimethylpropanamine; 1,2-Dimethylpropylamine; 2-Amino-3-methylbutane;3-Methyl-2-aminobutane; 3-Methyl-2-butanamine; 3-Methyl-2-butylamine
EINECS: 209-949-7
Density: 0.757
Melting Point: -50 ºC
Boiling Point: 84-87 ºC
Flash Point: -18 ºF
Solubility: miscible in water
Appearance: colorless to yellow liquid
Hazard Symbols:
Risk Codes: R11;R21/22;R34   
Safety: Poison by intraperitoneal route. A flammable liquid. When heated to decomposition it emits toxic vapors of NOx.
Transport Information: UN 3286
PSA: 26.02000
LogP: 1.68990
Synthetic route
72-18-4

L-valine

A

110-96-3

diisobutylamine

B

78-81-9

isobutylamine

C

598-74-3

2-amino-3-methylbutane

Conditions
ConditionsYield
Stage #1: L-valine With cyclopentyl methyl ether; ammonia at 200℃; under 4500.45 Torr; Sealed tube; Green chemistry;
Stage #2: With cyclopentyl methyl ether; ammonia; hydrogen at 200℃; under 42004.2 Torr; for 6.5h; Cooling with ice; Green chemistry;
A 5%
B 50%
C 7%
563-80-4

3-methyl-butan-2-one

598-74-3

2-amino-3-methylbutane

Conditions
ConditionsYield
With platinum(IV) oxide; ammonia; ammonium chloride under 735.5 - 2206.5 Torr; Hydrogenation;
(i) NH2OH, NaOAc, (ii) LiAlH4; Multistep reaction;
(reductive amination);
563-80-4

3-methyl-butan-2-one

A

99868-53-8

bis-(1,2-dimethyl-propyl)-amine

B

598-74-3

2-amino-3-methylbutane

Conditions
ConditionsYield
With methanol; platinum(IV) oxide; ammonia; ammonium chloride under 735.5 - 2206.5 Torr;
19838-95-0

bis-(1,2-dimethyl-propylidene)-hydrazine

A

99868-53-8

bis-(1,2-dimethyl-propyl)-amine

B

598-74-3

2-amino-3-methylbutane

Conditions
ConditionsYield
With hydrogen; nickel at 180 - 200℃;
600-20-4

3-methyl-butan-2-one oxime

598-74-3

2-amino-3-methylbutane

Conditions
ConditionsYield
With i-Amyl alcohol; sodium
With lithium aluminium tetrahydride
With sodium In ethanol
3238-16-2

2-chloro-2-methylbutan-3-one oxime

598-74-3

2-amino-3-methylbutane

Conditions
ConditionsYield
With hydrogenchloride; diethyl ether; tin(ll) chloride
2625-35-6

2-nitro-3-methyl-butane

598-74-3

2-amino-3-methylbutane

Conditions
ConditionsYield
With hydrogenchloride; iron at 100℃;
3378-43-6

3-Chlor-3-methyl-2-nitrosobutan-5t,9t-dien-Dimer

598-74-3

2-amino-3-methylbutane

Conditions
ConditionsYield
With lithium aluminium tetrahydride In tetrahydrofuran; diethyl ether
17123-14-7

2-Amino-1.1.2-trimethyl-aethanthiol

598-74-3

2-amino-3-methylbutane

Conditions
ConditionsYield
With water; nickel
513-35-9

2-methyl-but-2-ene

598-74-3

2-amino-3-methylbutane

Conditions
ConditionsYield
With chloro-trimethyl-silane; lithium dihydrido dimethyl borate; hydroxylamine-O-sulfonic acid 1) diethyl ether, 25 deg C, 4 h, 2) THF, 25 deg C, 12 h; Yield given. Multistep reaction;
Multi-step reaction with 2 steps
1: diethyl ether; nitrosyl chloride / anschliessend mit Chlorwasserstoff
2: tin (II)-chloride; hydrogen chloride; diethyl ether
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    CAS Number: 598-74-3 Molecular formula: C5H13N Molecular Weight: 87.16 EINECS number: 209-949-7 Related Categories: Organic Building Blocks; General Reagents; Health Supplements; Amines;Amines and Aniline

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    598-74-3

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    598-74-3

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    598-74-3

    CSR081605-64390

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    Price, Purity Application:reagent

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  • 598-74-3

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    598-74-3

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Toxicity Data With Reference

1.   

ipr-mus LD50:279 mg/kg

    JJPAAZ    Japanese Journal of Pharmacology. 17 (1967),475.

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

Poison by intraperitoneal route. A flammable liquid. When heated to decomposition it emits toxic vapors of NOx.

Standards and Recommendations

DOT Classification:  8; Label: Corrosive, Flammable Liquid (UN 2734); DOT Class: 3; Label: Flammable Liquid, Corrosive (UN 2733)