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6051-41-8

Basic Information
CAS No.: 6051-41-8
Name: Benzamide, 4-formyl-
Article Data: 45
Molecular Structure:
Molecular Structure of 6051-41-8 (Benzamide, 4-formyl-)
Formula: C8H7 N O2
Molecular Weight: 149.149
Synonyms: Terephthalaldehydamide(8CI); 4-Aminocarbonylbenzaldehyde; 4-Carbamoylbenzaldehyde; 4-Formylbenzamide
Density: 1.2021 (rough estimate)
Melting Point: 153-158℃
Boiling Point: 290.25°C (rough estimate)
Hazard Symbols: Xi
Risk Codes: R36/37/38;
PSA: 60.16000
LogP: 1.29830
Synthetic route
105-07-7

4-cyanobenzaldehyde

6051-41-8

4-formylbenzamide

Conditions
ConditionsYield
With manganese(IV) oxide; water In isopropyl alcohol at 100℃; under 5171.62 Torr; for 0.333333h;99%
With [RuH(tBu-PNP(-))(CO)]; water In tetrahydrofuran; tert-butyl alcohol at 20℃; for 24h;99%
With sodium perborate In ethanol; water for 0.0333333h; microwave irradiation;97%

4-formylbenzoyl azide

6051-41-8

4-formylbenzamide

Conditions
ConditionsYield
With benzyltriethylammonium tetrathiomolybdate In water; acetonitrile at 25℃; for 3h;88%
1122-91-4

4-bromo-benzaldehyde

6051-41-8

4-formylbenzamide

Conditions
ConditionsYield
With 1H-imidazole; 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; ammonium chloride; N-ethyl-N,N-diisopropylamine In 1,4-dioxane at 90℃; for 3h; Sealed tube;82%
619-55-6

para-methylbenzamide

6051-41-8

4-formylbenzamide

Conditions
ConditionsYield
With carbon tetrabromide; oxygen In acetonitrile at 20℃; for 3.5h; Irradiation; Green chemistry;79%
15164-44-0

p-(iodophenyl)carboxaldehyde

6051-41-8

4-formylbenzamide

Conditions
ConditionsYield
With 1H-imidazole; 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; ammonium chloride; N-ethyl-N,N-diisopropylamine In 1,4-dioxane at 90℃; for 3h; Sealed tube;77%
623-27-8

terephthalaldehyde,

6051-41-8

4-formylbenzamide

Conditions
ConditionsYield
With tert.-butylhydroperoxide; sodium carbonate; ammonium chloride In acetonitrile at 50℃; for 0.666667h; Inert atmosphere; Green chemistry;76%
201230-82-2

carbon monoxide

1122-91-4

4-bromo-benzaldehyde

6051-41-8

4-formylbenzamide

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); (2R)-1-[(1R)-1-[bis(1,1-dimethylethyl)phosphino]ethyl]-2-(diphenylphosphino)ferrocene; ammonium carbamate; sodium hydrogencarbonate In 1,4-dioxane at 100℃; for 20h; Inert atmosphere;65%
619-66-9

4-Carboxybenzaldehyde

6051-41-8

4-formylbenzamide

Conditions
ConditionsYield
Stage #1: 4-Carboxybenzaldehyde With 4-methyl-morpholine In dichloromethane at 0℃;
Stage #2: With isobutyl chloroformate at 0℃; for 0.5h;
Stage #3: With ammonium hydroxide at 0℃; for 1h;
48%
Stage #1: 4-Carboxybenzaldehyde With 4-methyl-morpholine; chloroformic acid ethyl ester In tetrahydrofuran at -5 - 0℃; for 0.583333h;
Stage #2: With ammonia In tetrahydrofuran; 1,4-dioxane at -5 - 0℃; for 0.616667h;
33%
Stage #1: 4-Carboxybenzaldehyde In tetrahydrofuran at 0℃; for 16h;
Stage #2: With ammonia In tetrahydrofuran; water
30%
Multi-step reaction with 2 steps
1: Vilsmeier reagent / tetrahydrofuran / 16 h / 0 °C
2: ammonia / water / Cooling
View Scheme
84545-14-2

tert-butyl 4-(chloromethyl)benzamide

6051-41-8

4-formylbenzamide

Conditions
ConditionsYield
With 4-methylmorpholine N-oxide In tetrahydrofuran at 20℃; for 12h; Reflux;45%
36735-42-9

4-cyanobenzylidene diacetate

A

6051-41-8

4-formylbenzamide

B

105-07-7

4-cyanobenzaldehyde

Conditions
ConditionsYield
With sulfuric acid
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