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Basic Information
| CAS No.: | 6080-56-4 |
|---|---|
| Name: | Lead acetate trihydrate |
| Molecular Structure: | |
|
|
|
| Formula: | C4H6O4Pb.3H2O |
| Molecular Weight: | 379.335 |
| Synonyms: | Leadacetate trihydrate (Pb(OAc)2.3H2O);Lead diacetate trihydrate;Lead(II) acetatetrihydrate;Plumbous acetate trihydrate; |
| EINECS: | 206-104-4 |
| Density: | 2,55 g/cm3 |
| Melting Point: | 75 °C (dec.)(lit.) |
| Boiling Point: | 117.1 °C at 760 mmHg |
| Flash Point: | 40 °C |
| Solubility: | 625 g/L in water |
| Appearance: | White crystals |
| Hazard Symbols: |
 T, N
|
| Risk Codes: | 61-33-48/22-50/53-62 |
| Safety: | 53-45-60-61 |
| Transport Information: | UN 1616 6.1/PG 3 |
| PSA: | 80.29000 |
| LogP: | -0.54610 |
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Synthetic route
Conditions
| Conditions | Yield |
|---|---|
| With sodium carbonate In acetic acid preparation of PbCO3 by treatment of PbCl2 with 1.5fold excess Na2CO3, treatment with acetic acid;; | 86.5% |
| With Na2CO3 In acetic acid aq. acetic acid; preparation of PbCO3 by treatment of PbCl2 with 1.5fold excess Na2CO3, treatment with acetic acid;; | 86.5% |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| With lead | |
| With lead(II) oxide | |
| With lead; air |
Conditions
| Conditions | Yield |
|---|---|
| In acetic acid 20% acetic acid, 380°C, stirring until a pH of 5.5 results, treatment of soln. with activated coal, further treatment at 30°C with activated coal and salicylic acid, thiosalicylic acid or thiocyanates;; product contains less than 5E-6% Fe(3+);; | |
| In acetic acid aq. acetic acid; dissolving PbO in dild. acetic acid;; | |
| In acetic acid aq. acetic acid; 20% acetic acid, 380°C, stirring until a pH of 5.5 results, treatment of soln. with activated coal, further treatment at 30°C with activated coal and salicylic acid, thiosalicylic acid or thiocyanates;; product contains less than 5E-6% Fe(3+);; |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| In ethyl acetate treatment with ethyl acetate in presence of H2O;; | |
| In ethyl acetate treatment with ethyl acetate in presence of H2O;; |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| With air In acetic acid aq. acetic acid; treatment of Pb with aq. acetic acid in presence of air;; |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| With sodium hydroxide In acetic acid separation of sulfate with hot NaOH, react. with acetic acid;; | |
| With NaOH In acetic acid aq. acetic acid; separation of sulfate with hot NaOH, react. with acetic acid;; |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| In acetic acid dissolving in hot dild. acetic acid, crystn. on cooling;; | |
| In acetic acid aq. acetic acid; dissolving in hot dild. acetic acid, crystn. on cooling;; |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| In acetic acid | |
| In acetic acid aq. acetic acid; |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| In water | |
| In water with concd. alk. acetate soln. at 25°C;; | |
| In water with concd. alk. acetate soln. at 25°C;; | |
| In water |
Conditions
| Conditions | Yield |
|---|---|
| In water | |
| In water |
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Lead acetate trihydrate
Chemistry
Molecular Formula: C4H12O7Pb
Formula Weight: 379.33
mp : 75 °C (dec.)(lit.)
bp : 280°C
density : 2,55 g/cm3
storage temp. : 2-8°C
Water Solubility : 625 g/L
nature of LEAD ACETATE(II), TRIHYDRATE: Lead acid hydrate three white crystalline powder or flake, and industrial products, is often brown or gray large.
Formula Weight: 379.33
mp : 75 °C (dec.)(lit.)
bp : 280°C
density : 2,55 g/cm3
storage temp. : 2-8°C
Water Solubility : 625 g/L
nature of LEAD ACETATE(II), TRIHYDRATE: Lead acid hydrate three white crystalline powder or flake, and industrial products, is often brown or gray large.
Production
Massicot reacts with acetic acid to obtain LEAD ACETATE(II), TRIHYDRATE.
Toxicity Data With Reference
| 1. | dni-mus-ipr 20 g/kg | ARGEAR Archiv fuer Geschwulstforschung. 51 (1981),605. | ||
| 2. | orl-rat TDLo:8524 mg/kg/78W-C:CAR,TER | ZAPPAN Zentralblatt fuer Allgemeine Pathologie und Pathologische Anatomie. 111 (1)(1968),1. | ||
| 3. | orl-rat LD50:4665 mg/kg | JACTDZ Journal of the American College of Toxicology. 1 (1992),713. | ||
| 4. | ipr-rat LD50:200 mg/kg | INMEAF Industrial Medicine. 10 (1941),15. | ||
| 5. | scu-gpg LDLo:2100 mg/kg | BMJOAE British Medical Journal. 2 (1913),217. |
Consensus Reports
IARC Cancer Review: Animal Sufficient Evidence IMEMDT IARC Monographs on the Evaluation of Carcinogenic Risk of Chemicals to Man . 1 , 1972,p. 40.(World Health Organization, Internation Agency for Research on Cancer,Lyon, France.: ) (Single copies can be ordered from WHO Publications Centre U.S.A., 49 Sheridan Avenue, Albany, NY 12210) . EPA Genetic Toxicology Program. Lead and its compounds are on the Community Right-To-Know List.
Safety Profile
Hazard Codes : T,N
Risk Statements : 61-33-48/22-50/53-62
Safety Statements : 53-45-60-61
RIDADR : UN 1616 6.1/PG 3
WGK Germany : 2
RTECS : OF8050000
HazardClass : 6.1
PackingGroup : III
Confirmed carcinogen with experimental carcinogenic and teratogenic data. Poison by intraperitoneal route. Moderately toxic by subcutaneous route. Experimental reproductive effects. Mutation data reported. When heated to decomposition it emits toxic fumes of Pb. See also LEAD COMPOUNDS.
Risk Statements : 61-33-48/22-50/53-62
Safety Statements : 53-45-60-61
RIDADR : UN 1616 6.1/PG 3
WGK Germany : 2
RTECS : OF8050000
HazardClass : 6.1
PackingGroup : III
Confirmed carcinogen with experimental carcinogenic and teratogenic data. Poison by intraperitoneal route. Moderately toxic by subcutaneous route. Experimental reproductive effects. Mutation data reported. When heated to decomposition it emits toxic fumes of Pb. See also LEAD COMPOUNDS.
Standards and Recommendations
OSHA PEL: TWA 0.05 mg(Pb)/m3
NIOSH REL: (Inorganic Lead) TWA 0.10 mg(Pb)/m3
NIOSH REL: (Inorganic Lead) TWA 0.10 mg(Pb)/m3