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6132-04-3

Basic Information
CAS No.: 6132-04-3
Name: Trisodium citrate dihydrate
Molecular Structure:
Molecular Structure of 6132-04-3 (Trisodium citrate dihydrate)
Formula: C6H9Na3O9
Molecular Weight: 294.10
Synonyms: 1,2,3-Propanetricarboxylicacid, 2-hydroxy-, trisodium salt, dihydrate (9CI);Citric acid, trisodium salt,dihydrate (8CI);N 1560;Sodium citrate dihydrate;
EINECS: 201-069-1
Density: 1.76 g/cm3
Melting Point: >300 °C(lit.)
Boiling Point: 309.6 °C at 760 mmHg
Flash Point: 155.2 °C
Solubility: 720 g/L (25 °C) in water
Appearance: white powder or colourless crystals
Hazard Symbols: IrritantXi
Risk Codes: 37/38-41-36/37/38
Safety: 26-36/37/39-24/25-36
Transport Information:
PSA: 159.08000
LogP: -5.38120
Synthetic route
68-04-2

sodium citrate

6132-04-3

trisodium citrate dihydrate

Conditions
ConditionsYield
In water concentration of aq. soln. at 55°C, 8.6 Torr; pptn.; temp. must be >47°C;; centrifuging;;
In water concentration of aq. soln. at 55°C, 8.6 Torr; pptn.; temp. must be >47°C;; centrifuging;;
6858-44-2

citric acid ; trisodium-salt pentahydrate

A

7732-18-5

water

B

6132-04-3

trisodium citrate dihydrate

Conditions
ConditionsYield
In neat (no solvent) heating at temp. above 145°C;;
In neat (no solvent) heating at temp. above 145°C;;

disodium hydrogen citrate

6132-04-3

trisodium citrate dihydrate

Conditions
ConditionsYield
In water crystn. from Na2HC6H5O7 soln. under ethanol at 23°C;;

trisodium citrate 5.5-hydrate

6132-04-3

trisodium citrate dihydrate

Conditions
ConditionsYield
In neat (no solvent) byproducts: H2O; dehydration at 100°C;;
In neat (no solvent) byproducts: H2O; dehydration at 100°C;;

trisodium citrate 5.5-hydrate

A

7732-18-5

water

B

6132-04-3

trisodium citrate dihydrate

Conditions
ConditionsYield
In neat (no solvent) heating at temp. above 145°C;;
In neat (no solvent) heating at temp. above 145°C;;
117229-22-8

cis-α-dichloro(triethylenetetramine)cobalt(III) chloride

6132-04-3

trisodium citrate dihydrate

82621-19-0

β-[(citrato)(triethylenetetramine)cobalt(III)] pentahydrate

Conditions
ConditionsYield
With (C2H5)3N; H2O In methanol ligand salt, complex and (C2H5)3N refluxed for 40 h in MeOH; evapd. (vac.), solids dissolved in H2O, chromd. (cation-exchange, H(1+)-form, aq. NH3), evapd. (vac.), recrystd. (H2O/MeOH) at 70°C, dried at 100°C overnight; elem. anal.;55.4%
696-59-3

cis,trans-2,5-dimethoxytetrahydrofuran

542-05-2

acetonedicarboxylic acid

75-04-7

ethylamine

6132-04-3

trisodium citrate dihydrate

3423-30-1

N-ethylnortropinone

Conditions
ConditionsYield
With hydrogenchloride In water46%
542-05-2

acetonedicarboxylic acid

6132-04-3

trisodium citrate dihydrate

100-46-9

benzylamine

28957-72-4

N-benzyltropinone

Conditions
ConditionsYield
With hydrogenchloride In water44%

acetone dicarboxylic acid

75-31-0

isopropylamine

6132-04-3

trisodium citrate dihydrate

3423-28-7

8-aza-8-isopropyl-bicyclo<3.2.1>octan-3-one

Conditions
ConditionsYield
With hydrogenchloride In water40%
542-05-2

acetonedicarboxylic acid

6132-04-3

trisodium citrate dihydrate

765-30-0

Cyclopropylamine

60206-33-9

8-cyclopropyl-8-azabicyclo-[3.2.1]-octan-3-one

Conditions
ConditionsYield
With hydrogenchloride In water33%
7705-07-9

titanium(III) chloride

6132-04-3

trisodium citrate dihydrate

Na8[Ti(citrato(4-))3]*17H2O

Conditions
ConditionsYield
With NaOH; air In water a soln. of sodium citrate dihydrate added to TiCl3 under N2, air-oxidized, pH increased to 7 using NaOH; crystd. by diffusion of MeOH into the soln. at 4°C; elem. anal.;22.5%

aluminum(III) nitrate nonahydrate

6132-04-3

trisodium citrate dihydrate

[Al(H2O)6][Al3(citrate)2(OH)2(H2O)4]2NO3*6H2O

Conditions
ConditionsYield
With quinoline In water Al(NO3)3*9H2O, Na3C6H5O7*2H2O (1:1 or 10:1 Al to citrate ratios) dissolved in H2O; quinoline added dropwise with const. stirring; soln. stirred for 30 min (optimum pH 1.660, but complex also formed in the pH range 1.2 to 3.0); crystals formed after 48 h; elem. anal.;22%

Iron(III) nitrate nonahydrate

2,9-dimethyl-1,10-phenanthroline monohydrate

6132-04-3

trisodium citrate dihydrate

(2,9-dimethyl-1,10-phenanthrolinium)7[Fe9O(citrate)8(H2O)3] * 2,9-dimethyl-1,10-phenanthroline * 61 H2O

Conditions
ConditionsYield
In water byproducts: neocuproinium nitrate; equimolar amts., stirring at 60°C for 30 min; standing at room temp. for 24 h, filtration off of neocuproininum nitrate, crystn. at 27°C (several d);15%

cadmium(II) nitrate tetrhydrate

872834-46-3

1,4,8,11-tetra(4-pyridylmethyl)-1,4,8,11-tetraazacyclotetradecane

6132-04-3

trisodium citrate dihydrate

sesqui(1,4,8,11-tetra(4-pyridylmethyl)-1,4,8,11-tetraazacyclotetradecane)tricadmium(II) citrate hexahydrate

Conditions
ConditionsYield
In water High Pressure; Cd:citate:amine=0.14:0.071:0.071 molar ratio, heated at 110°C for3 d; mechanical separated; elem. anal.;12%
jones reagent

jones reagent

Zn(Hg)

Zn(Hg)

60232-85-1

1-(1-phenylcyclohexyl)-4-hydroxypiperidine

H2 CrO4

H2 CrO4

7664-93-9

sulfuric acid

7487-94-7

mercury (II) chloride

6132-04-3

trisodium citrate dihydrate

67-63-0

isopropyl alcohol

77179-42-1

1-(1-phenylcyclohexyl)-4-piperidone

Conditions
ConditionsYield
With hydrogenchloride In methanol; chloroform; water; acetic acid
jones reagent

jones reagent

Zn(Hg)

Zn(Hg)

60232-85-1

1-(1-phenylcyclohexyl)-4-hydroxypiperidine

H2 CrO4

H2 CrO4

7487-94-7

mercury (II) chloride

6132-04-3

trisodium citrate dihydrate

67-63-0

isopropyl alcohol

77179-42-1

1-(1-phenylcyclohexyl)-4-piperidone

Conditions
ConditionsYield
With hydrogenchloride; sulfuric acid In methanol; chloroform; water; acetic acid

hydrogen tetrachloroaurate(III) tetrahydrate

6132-04-3

trisodium citrate dihydrate

Conditions
ConditionsYield
In water soln. of HAuCl4 added 1% citrate within period of 5 s while refluxing with vigorous stirring under N2 atm.; Au soln. kept refluxing for period of 1 h and then left to cool to room temp.; detd. by absorption spect.;

nickel(II) chloride hexahydrate

6132-04-3

trisodium citrate dihydrate

Ni(2+)*OOCCH2C(OH)(COO)CH2COO(3-)=Ni(OOCCH2C(OH)(COO)CH2COO)(1-)

Conditions
ConditionsYield
In water
6132-04-3

trisodium citrate dihydrate

trisodium citrate 5.5-hydrate

Conditions
ConditionsYield
In water dissoln. in H2O; crystn. at ambient temp.;;
In water dissoln. in H2O; crystn. at ambient temp.;;

silver nitrate

6132-04-3

trisodium citrate dihydrate

126-45-4

silver(I) citrate

Conditions
ConditionsYield
In water sodium citrate soln. in water added dropwise into the silver nitrate soln. in water; centrifugation, washed with distilled water, absolute alcohol in sequence and dried in air;

Iron(III) nitrate nonahydrate

6132-04-3

trisodium citrate dihydrate

2Na(1+)*Fe2(OH)2(H2O)2(C6H5O7)2(2-)*6H2O*0.8Na(1+)*0.4C6H6O7(2-)*0.8H2O=Na2Fe2(OH)2(H2O)2(C6H5O7)2*6.8H2O*0.4Na2C6H6O7

Conditions
ConditionsYield
With sodium carbonate In water mixing of solns. of equimolar amts. of salts, adjusting pH to 5.5 with Na2CO3, refluxed; pptn. with methanol, washing with 80% methanol-water, drying in vac.; elem. anal.;
7631-95-0

sodium molybdate dihydrate

7664-93-9

sulfuric acid

6132-04-3

trisodium citrate dihydrate

3Na(1+)*4H(1+)*(MoO4)2(C6H5O7)(7-)=Na3H4(MoO4)2(C6H5O7)

Conditions
ConditionsYield
With Na3H2MoO4(C6H5O7) In water soln. of Na2MoO4 and Na3C6H5O7 mixed in various proportions, pH adjusted by H2SO4 to 5.00;

copper(ll) sulfate pentahydrate

6132-04-3

trisodium citrate dihydrate

3Na(1+)*OOCCH2C(OH)(COO)CH2COO(3-)*2H2O=Na3(C6H5O7)*2H2O#dotCu(2+)

3Na(1+)*OOCCH2C(OH)(COO)CH2COO(3-)*2H2O=Na3(C6H5O7)*2H2O#dotCu(2+)

Conditions
ConditionsYield
In water aq. soln. of sodium citrate and 0.1 wt.-% of CuSO4*5H2O slowly evapd. for a few days;

vanadyl sulfate trihydrate

6132-04-3

trisodium citrate dihydrate

VO(2+) doped trisodium citrate dihydrate

VO(2+) doped trisodium citrate dihydrate

Conditions
ConditionsYield
In water VOSO4*3H2O (0.01 mol%) mixed with aq. soln. of sodium citrate; crystd. by slow evapn. of satd. soln.; single crystals obtained;

cobalt(II) nitrate hexahydrate

copper(II) nitrate trihydrate

calcium nitrate * 3-hydrate

6132-04-3

trisodium citrate dihydrate

Ca2.8Na0.2Co3.8Cu0.2O9

Conditions
ConditionsYield
With citric acid; polyethylene glycol 400; NH3 In water sol-gel method: salts dissolved in aq. citric acid, polyethylene glycol 400 added, NH3 added to adjust pH to 1.0-2.0, mixt. stirred, heated to m80 °C for 24 h, dried at 120 °C for 12 h, xerogel cacined (750 °C, 4 h, air); detd. by XRD;

cobalt(II) nitrate hexahydrate

copper(II) nitrate trihydrate

calcium nitrate * 3-hydrate

6132-04-3

trisodium citrate dihydrate

Ca2.7Na0.3Co3.8Cu0.2O9

Conditions
ConditionsYield
With citric acid; polyethylene glycol 400; NH3 In water sol-gel method: salts dissolved in aq. citric acid, polyethylene glycol 400 added, NH3 added to adjust pH to 1.0-2.0, mixt. stirred, heated to m80 °C for 24 h, dried at 120 °C for 12 h, xerogel cacined (750 °C, 4 h, air); detd. by XRD;

manganese(II) chloride tetrahydrate

6132-04-3

trisodium citrate dihydrate

manganese(II)carbonate

Conditions
ConditionsYield
With aq. NH3 In water High Pressure; Mn salt and citrate were added to H2O under stirring; aq. NH3 added at room temp. soln. stirred for several min; transferred in Teflon lined stainless steel autoclave; sealed; heated at 160°C for 2 h; collected; washed; dried in vac.;

zinc(II) nitrate hexahydrate

100-97-0

hexamethylenetetramine

6132-04-3

trisodium citrate dihydrate

zinc(II) oxide

Conditions
ConditionsYield
at 95℃; for 12h; Temperature; Time; Autoclave;
Downstream Products
28957-72-4
3423-30-1
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  • TIANFU-CHEM CAS:6132-04-3 Trisodium citrate dihydrate

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    TIANFU-CHEM CAS:6132-04-3 Trisodium citrate dihydrate

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Specification

1. Introduction of Trisodium citrate dihydrate
Trisodium citrate dihydrate is also called citric acid trisodium salt dehydrate, it is the sodium salt of citric acid combined with 2 water molecules. The IUPAC name of Trisodium citrate dihydrate is trisodium 2-hydroxypropane-1,2,3-tricarboxylate dehydrate. It is white powder or colourless crystals,odorless and salty cool. And the product categories are inorganic & organic chemicals;food additives;food and feed additive. 

2. Properties of Trisodium citrate dihydrate
Nominal Mass: 294 Da
Average Mass: 294.0996 Da
Monoisotopic Mass: 293.993967 Da
Flash Point: 155.2 °C
Enthalpy of Vaporization: 63.82 kJ/mol
Boiling Point: 309.6 °C at 760 mmHg
Storage temp: Store at RT.
Water Solubility: 720 g/L (25 ºC)
Merck: 14,8602
BRN: 6104939
Stability: Stable. Incompatible with bases, reducing agents, oxidizing agents.
Vapour Pressure: 5.73E-05 mmHg at 25°C

3. Structure Descriptors of Trisodium citrate dihydrate
InChI=1/C6H8O7.3Na.2H2O/c7-3(8)1-6(13,5(11)12)2-4(9)10;;;;;/h13H,1-2H2,(H,7,8)(H,9,10)(H,11,12);;;;2*1H2/q;3*+1;;/p-3
Smiles
O=C([O-])CC(C([O-])=O)(O)CC([O-])=O.[Na+].[Na+].[Na+].O.O
Classification Code: Alkalizer [systemic]

4. Safety Information of Trisodium citrate dihydrate
Hazard Codes: Xi
Risk Statements: 37/38-41-36/37/38
R37/38: Irritating to respiratory system and skin
R41: Risk of serious damage to the eyes
R36/37/38: Irritating to eyes, respiratory system and skin
Safety Statements: 26-36/37/39-24/25-36
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
S36/37/39: Wear suitable protective clothing, gloves and eye/face protection
S24/25: Avoid contact with skin and eyes
S36: Wear suitable protective clothing
WGK Germany: 1
RTECS: GE7810000

5. Use of Trisodium citrate dihydrate
Trisodium citrate dihydrate has a sour taste similar to citric acid, and is salty as well. It is often used as a food preservative, and as a flavoring in the food industry. In the pharmaceutical industry it is used to control pH. And trisodium citrate dihydrate may be used as an alkalizing agent, buffering agent, emulsifier, or sequestering agent. What’s more, it is used in nonhydrogen electroplation as well as widely in tail gas absorption process of sulfur dioxide for chemical and metallurgy industries. Its absorptivity reaches 99%. The waste absorbed may be regenerated into sulfur dioxide liquid and potassium citrate for cyclic utilization. The daily-use chemical detergent with potassium citrate. As raw material instead of sodium phosphate trimer, it is non-toxic and non-pollution.