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6147-53-1

Basic Information
CAS No.: 6147-53-1
Name: Acetic acid, cobalt(2+)salt, tetrahydrate (8CI,9CI)
Molecular Structure:
Molecular Structure of 6147-53-1 (Acetic acid, cobalt(2+)salt, tetrahydrate (8CI,9CI))
Formula: C4H14CoO8
Molecular Weight: 249.08
Synonyms: Bis(acetato)tetraquacobalt;Cobalt acetate tetrahydrate;
EINECS: 200-755-8
Density: 1,71 g/cm3
Melting Point: 140 °C
Boiling Point: 117.1 °C at 760 mmHg
Flash Point: 40 °C
Solubility: 380 g/L (20 ºC)
Appearance: Reddish violet deliequecent crystals.
Hazard Symbols: HarmfulXn; DangerousN
Risk Codes: 38-40-50/53-42/43-36/37/38-20/21/22
Safety: 36/37-61-45-29-24-22
Transport Information: UN 3077
PSA: 117.18000
LogP: -2.74480
Synthetic route

Co(galvinoxyl)2

64-19-7

acetic acid

6147-53-1

cobalt(II) diacetate tetrahydrate

Conditions
ConditionsYield
In pentane byproducts: hydroxygalvinol; aq. acetic acid (0.52 mmol) and n-pentane were added to Co-contg. compd.(0.20 mmol) at room temp.; standing overnight; sepn. of the phases and removing of the solvent in vac.;84%

cobalt(III) hydroxide

7440-48-4

cobalt

64-19-7

acetic acid

6147-53-1

cobalt(II) diacetate tetrahydrate

Conditions
ConditionsYield
In acetic acid 2.5-3.25 atm; 120°C; autoclave;; crystn. on cooling;;
In acetic acid aq. acetic acid; 2.5-3.25 atm; 120°C; autoclave;; crystn. on cooling;;
In acetic acid 2.5-3.25 atm; 120°C; autoclave;; crystn. on cooling;;
64-19-7

acetic acid

759403-02-6

cobalt(II) carbonate

6147-53-1

cobalt(II) diacetate tetrahydrate

Conditions
ConditionsYield
In not given byproducts: CO2, H2O; elem. anal.;
In acetic acid aq. acetic acid; soln. of CoCO3 in aq. acetic acid; crystn.;;
7440-48-4

cobalt

64-19-7

acetic acid

6147-53-1

cobalt(II) diacetate tetrahydrate

Conditions
ConditionsYield
In acetic acid Electrolysis; electrolysis (Cr18Ni10Ti cathode, 35+/-2°C, 12.5 A/dm**2, 10 h, 31-45, 17-35, 33-38 or 37-48 V poten. drop across cell or 35-40 V poten.drop across cell, 1.2, 9.2, 12,5, 8.3 or 0.95 A/dm**2); continous crystn.;
In not given Electrochem. Process;

cobalt(III) nitrate

64-17-5

ethanol

6147-53-1

cobalt(II) diacetate tetrahydrate

Conditions
ConditionsYield
With urea at 90℃; for 10h; Autoclave;

5,10,15,20-tetrakis(pentafluorophenyl)porphyrin

6147-53-1

cobalt(II) diacetate tetrahydrate

129707-78-4

C52H32CoF16N8

Conditions
ConditionsYield
In N,N-dimethyl-formamide refluxed for 12 h; dried, chromy. (neutral alumina) with benzene and CH2Cl2 as eluting solvent, recrystn. (CH2Cl2/benzene 1:9); elem. anal.;100%
3946-91-6

N,N'-bis(salicylidene)-o-phenylenediamine

6147-53-1

cobalt(II) diacetate tetrahydrate

17457-14-6, 39836-45-8

N,N'-bis(salicylidene)-1,2-phenylene diaminocobalt(II)

Conditions
ConditionsYield
In propan-1-ol under N2; suspn. of Co compd. warmed to 50 °C; org. compd. addedin one portion; suspn. refluxed for 6 h; mixt. cooled, filtered under reduced pressure; collected solid washed with Et2O and dried in air to give crystals;100%
With acetic acid In ethanol; dichloromethane at 60℃; for 2h;85.3%
In methanol reflux of a mixture of ligand and Co-acetate in CH3OH for 1 h, cooling; filtration, washing with CH3OH and ether, drying under vac. at 100°C; elem. anal.;73%

Na(1+)*BrC6H4COCHNO(1-)=BrC6H4COCHNONa

6147-53-1

cobalt(II) diacetate tetrahydrate

cobalt(II)(4-BrINAP)2*H2O

Conditions
ConditionsYield
In water addn. of a soln. of organic compound to a soln. of metal salt with stirring; filtn., washing (water), drying (anhydrous calcium chloride), elem. anal.;100%

Na(1+)*CH3C6H4COCHNO(1-)=CH3C6H4COCHNONa

6147-53-1

cobalt(II) diacetate tetrahydrate

cobalt(II)(4-MeINAP)2*H2O

Conditions
ConditionsYield
In water addn. of a soln. of organic compound to a soln. of metal salt with stirring; filtn., washing (water), drying (anhydrous calcium chloride), elem. anal.;100%

Na(1+)*ClC6H4COCHNO(1-)=ClC6H4COCHNONa

6147-53-1

cobalt(II) diacetate tetrahydrate

cobalt(II)(4-ClINAP)2*H2O

Conditions
ConditionsYield
In water addn. of a soln. of organic compound to a soln. of metal salt with stirring; filtn., washing (water), drying (anhydrous calcium chloride), elem. anal.;100%

Na(1+)*NO2C6H4COCHNO(1-)=NO2C6H4COCHNONa

6147-53-1

cobalt(II) diacetate tetrahydrate

87036-30-4

cobalt(II)(4-NO2INAP)2*4-NO2HINAP

Conditions
ConditionsYield
In water addn. of a soln. of organic compound to a soln. of metal salt with stirring; filtn., washing (water), drying (anhydrous calcium chloride), elem. anal.;100%
6147-53-1

cobalt(II) diacetate tetrahydrate

20597-98-2

iso-nitrosoacetophenone sodium salt

87097-49-2

cobalt(II)(INAP)2

Conditions
ConditionsYield
In water addn. of a soln. of organic compound to a soln. of metal salt with stirring; filtn., washing (water), drying (anhydrous calcium chloride), elem. anal.;100%
6147-53-1

cobalt(II) diacetate tetrahydrate

151427-04-2

2-(p-methoxyphenyl)ethan-1,2-dion-1-oxime sodium salt

cobalt(II)(4-OMeINAP)2*H2O

Conditions
ConditionsYield
In water addn. of a soln. of organic compound to a soln. of metal salt with stirring; filtn., washing (water), drying (anhydrous calcium chloride), elem. anal.;100%
609-71-2

2-hydroxy-3-carboxypyridine

6147-53-1

cobalt(II) diacetate tetrahydrate

956331-98-9

diaquabis(2-hydroxynicotinato(1-))cobalt(II)

Conditions
ConditionsYield
With aq. ammonia In water soln. of ligand in H2O added to soln. of Co salt in H2O; pH adjusted to 8 (a few drops of concd. ammonia soln.); stored for a few d; filtered; ppt. washed with H2O; dried in dessicator over NaOH; elem. anal.;100%
1412912-27-6

C102H120N6O6

6147-53-1

cobalt(II) diacetate tetrahydrate

C102H114Co3N6O6

Conditions
ConditionsYield
In methanol; dichloromethane at 25℃; for 1.5h; Schlenk technique; Inert atmosphere;100%
1412912-29-8

C136H160N8O8

6147-53-1

cobalt(II) diacetate tetrahydrate

C136H152Co4N8O8

Conditions
ConditionsYield
In methanol; dichloromethane at 25℃; for 1.5h; Schlenk technique; Inert atmosphere;100%
6147-53-1

cobalt(II) diacetate tetrahydrate

[1,2]benzenobicyclo[2.2.2]octadieneporphyrin

[1,2]benzenobicyclo[2.2.2]octadieneporphyrin cobalt

Conditions
ConditionsYield
In methanol; chloroform for 3h;100%

2N((CH2)3CH3)4(1+)*Mo2O5(O2C6H2(NCHC6H3(OC2H5)OH)2)2(2-)=[N((CH2)3CH3)4]2[Mo2O5(O2C6H2(NCHC6H3(OC2H5)OH)2)2]

6147-53-1

cobalt(II) diacetate tetrahydrate

2N((CH2)3CH3)4(1+)*Mo2O5(O2C6H2(NCHC6H3(OC2H5)O)2Co)2(2-)=[N((CH2)3CH3)4]2[Mo2O5(O2C6H2(NCHC6H3(OC2H5)O)2Co)2]

Conditions
ConditionsYield
In methanol; acetone byproducts: H2O; inert atmosphere; dropwise addn. of metal acetate (in MeOH) to 0.5 equiv. Mn-complex (in Me2CO), stirring for 1 h; solvent removal (vac.), dissoln. in THF/CH2Cl2=10:1, pptn. on Et2O addn., standing overnight;99%

2N((CH2)3CH3)4(1+)*Mo2O5(O2C6H2(NCHC6H2(C(CH3)3)2OH)2)2(2-)=[N((CH2)3CH3)4]2[Mo2O5(O2C6H2(NCHC6H2(C(CH3)3)2OH)2)2]

6147-53-1

cobalt(II) diacetate tetrahydrate

2N((CH2)3CH3)4(1+)*Mo2O5(O2C6H2(NCHC6H2(C4H9)2O)2Co)2(2-)=[N((CH2)3CH3)4]2[Mo2O5(O2C6H2(NCHC6H2(C4H9)2O)2Co)2]

Conditions
ConditionsYield
In methanol; acetone byproducts: H2O; inert atmosphere; dropwise addn. of metal acetate (in MeOH) to 0.5 equiv. Mn-complex (in Me2CO), stirring for 1 h; solvent removal (vac.), dissoln. in PhMe, pptn. on addn. of hexanes, standing overnight;99%
116655-21-1

4-palmitoyl-1-phenyl-3-methyl-2-pyrazolone

6147-53-1

cobalt(II) diacetate tetrahydrate

Co(C6H5C3N2(CH3)(CO(CH2)14CH3)O)2*2H2O

Conditions
ConditionsYield
In ethanol; water warming a soln. of Co(CH3COO)2*4H2O in water, addn. of a hot ethanolic soln. of ligand with stirring, pptn.; washing with water/ethanol, drying in air, storing in a desiccator, elem. anal.;99%

C20H10N4(C6H4NHC(O)C6H4CH2N2C3H2C6H4CF3)(C6H4NHC(O)CH3)3

6147-53-1

cobalt(II) diacetate tetrahydrate

Co[C20H8N4(C6H4NHC(O)C6H4CH2N2C3H2C6H4CF3)(C6H4NHC(O)CH3)3]

Conditions
ConditionsYield
In tetrahydrofuran N2; stirring of THF soln. of ligand and Co salt overnight at room temp.; evapn. of the solvent, chromy. on neutral Al2O3 (benzene/methanol, 90:10), evapn. of the solvent;99%
64-17-5

ethanol

47644-69-9, 69678-00-8, 18531-91-4

dimethyl 2,2'-dihydroxy-1,1'-binaphthalene-3,3'-dicarboxylate

6147-53-1

cobalt(II) diacetate tetrahydrate

1072832-01-9

[Co(EtOH)(H2O)(2,2'-dihydroxy-3,3'-di(carboxymethyl)-1,1'-binaphthyl(-2H))]2*H2O

Conditions
ConditionsYield
With sodium acetate In ethanol; 1,2-dichloro-ethane byproducts: CH3COOH; addn. of soln. of Co(CH3COO)2*4H2O in 1,1'-dichloroethane to EtOH soln. of 2,2'-dihydroxy-2,2'-di(carboxymethyl)-1,1'-binaphthyl with stirring; reflux for 1 h; adjusting pH to 6.0 by addn. of NaCH3COO; heating at 90°C for 0.5 h; addn. of H2O; pptn., filtration, washing with hot EtOH; drying in desiccator over P4O10; elem. anal.;99%
109-99-9

tetrahydrofuran

6147-53-1

cobalt(II) diacetate tetrahydrate

(1R,4R)-3-trifluoroacetyl-1,7,7-trimethylbicyclo[2.2.1]heptan-2-one

bis[2,2,2-trifluoromethyl-1-[(1R,4S)-1,7,7-trimethyl-2-(oxo-κO)bicyclo[2.2.1]hept-3-yliden]ethanolato-κO]cobalt(II)*tetrahydrofuran*water

Conditions
ConditionsYield
In ethanol (under N2); soln. of ligand in EtOH added to suspn. of Co(CH3CO2)2*4H2O in EtOH, stirred for 30 min at 20°C; volatiles removed under reduced pressure, dried under reduced pressure, pentane diffused into THF soln.; elem. anal.;99%

(1R,4R)-3-[1-[3,5-bis(trifluoromethyl)phenyl]]-1,7,7-trimethylbicyclo[2.2.1]heptan-2-one

6147-53-1

cobalt(II) diacetate tetrahydrate

bis[1-[3,5-bis(trifluoromethyl)benzoyl]-1-[(1R,4S)-1,7,7-trimethyl-2-(oxo-κO)bicyclo[2.2.1]hept-3-yliden]methanolato-κO]cobalt(II)

Conditions
ConditionsYield
In sodium hydroxide; ethanol (under N2); soln. of ligand in EtOH and aq. NaOH added to suspn. of Co(CH3CO2)2*4H2O in EtOH and aq. NaOH, stirred for 30 min at 20°C; volatiles removed under reduced pressure, dried under reduced pressure;99%
22934-51-6

5-allyl-2-hydroxy-3-methoxybenzaldehyde

lutidinium p-toluene sulfonate

20439-47-8

(1R,2R)-1,2-diaminocyclohexane

6147-53-1

cobalt(II) diacetate tetrahydrate

[((R,R)-C6H10(NCHC6H2(OMe)(allyl)O)2)Co(p-toluene sulfonate)]

Conditions
ConditionsYield
With air In ethanol refluxing mixt. of benzaldehyde deriv. and diamine deriv. in ethanol for30 min, cooling, addn. of cobalt compd. and then lutidinium salt, stirr ing at room temp. for 30 min; concg., addn. of CH2Cl2, filtration through celite, concg., addn. of hexane, filtration, drying in air, NMR and MS;99%
326-06-7

1-Phenyl-4,4,4-trifluorobutane-1,3-dione

6147-53-1

cobalt(II) diacetate tetrahydrate

bis-[1,1,1-trifluoro-4-phenyl-2-(oxo-κO)-but-3-en-4(olato-κO)]cobalt(II) dihydrate

Conditions
ConditionsYield
In ethanol 20°C;99%

lutidinium p-toluene sulfonate

(R,R,R,R)-HO(tBu)2C6H2CHNC6H10NCHC6H2(OMe)(OH)CH2CHCHCH2C6H2(OMe)(OH)CHNC6H10NCHC6H2(tBu)2OH*Et3NHCl*3water

6147-53-1

cobalt(II) diacetate tetrahydrate

[((R,R,R,R)-O(tBu)2C6H2CHNC6H10NCHC6H2(OMe)(O)CH2CHCHCH2C6H2(OMe)(O)CHNC6H10NCHC6H2(tBu)2O)Co2(p-toluene sulfonate)2]

Conditions
ConditionsYield
With air In methanol; dichloromethane addn. of degassed soln. of cobalt compd. in methanol to degassed soln. of phenol deriv. in CH2Cl2 under Ar, stirring for 30 min, addn. of tosylate salt, stirring for 18 h in air; concg., washing with diethyl ether, drying in vac., NMR and MS;99%
873975-75-8

[3,5-bis(4-methoxyphenyl)-1H-pyrrol-2-yl]-[3,5-bis(4-methoxyphenyl)pyrrol-2-ylidene]amine

6147-53-1

cobalt(II) diacetate tetrahydrate

1407495-77-5

bis[3,5-bis(4-methoxyphenyl)-1H-pyrrol-2-yl-3,5-bis(4-methoxyphenyl)-2-ylideneamine]cobalt(II)

Conditions
ConditionsYield
With potassium tert-butylate In butan-1-ol for 0.25h; Microwave irradiation;99%
64-17-5

ethanol

14691-35-1

2-(2-hydroxyphenyl)-4,5-diphenyl-1H-imidazole

6147-53-1

cobalt(II) diacetate tetrahydrate

Co(2-(4,5-diphenyl-1H-imidazol-2-yl)phenol(-1H))2*2EtOH

Conditions
ConditionsYield
for 0.5h; Reflux;99%
22112-89-6

5,15-diphenylporphyrin

6147-53-1

cobalt(II) diacetate tetrahydrate

204841-08-7

[5,15-diphenylporphyrinato]cobalt(II)

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 130℃; for 3h; Inert atmosphere;99%
6147-53-1

cobalt(II) diacetate tetrahydrate

574-93-6

29H,31H-Phthalocyanine

3317-67-7

cobalt(II) phthalocyanine

Conditions
ConditionsYield
With butyl(2-hydroxyethyl)dimethylammonium acetate at 100℃; Ionic liquid; Inert atmosphere;99%
With tributyl-amine In pentan-1-ol at 160℃; for 2h; Inert atmosphere;20 mg

2,4-dibromo-6-{[2-(4,5-diphenyl-1H-imidazol-2-yl)phenylimino]methyl}phenol

6147-53-1

cobalt(II) diacetate tetrahydrate

C56H36Br4CoN6O2

C56H36Br4CoN6O2

Conditions
ConditionsYield
In ethanol at 20℃; for 4h;99%
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    Acetic acid, cobalt(2+)salt, tetrahydrate (8CI,9CI)

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Consensus Reports

Cobalt and its compounds are on the Community Right-To-Know List. IARC Cancer Review: Group 2B IMEMDT    IARC Monographs on the Evaluation of Carcinogenic Risk of Chemicals to Man .

Specification

The Cobalt acetate tetrahydrate with CAS registry number of 6147-53-1 is also called Bis(acetato)tetraquacobalt. The EINECS registry number is 200-755-8. The IUPAC name is cobalt(2+) acetate hydrate (1:2:4). In addition, the molecular formula is C4H14CoO8 and the molecular weight is 249.08. It belongs to the class of Inorganic Chemicals.

Physical properties about this chemical are: (1)ACD/LogP: -0.29; (2)ACD/LogD (pH 5.5): -1.07; (3)ACD/LogD (pH 7.4): -2.86; (4)ACD/BCF (pH 5.5): 1; (5)ACD/BCF (pH 7.4): 1; (6)ACD/KOC (pH 5.5): 2.73; (7)ACD/KOC (pH 7.4): 1; (8)#H bond acceptors: 2; (9)#H bond donors: 1; (10)Polar Surface Area: 37.3 Å2; (11)Flash Point: 40 °C; (12)Enthalpy of Vaporization: 23.7 kJ/mol; (13)Boiling Point: 117.1 °C at 760 mmHg; (14)Vapour Pressure: 13.9 mmHg at 25°C.

Preparation of Cobalt acetate tetrahydrate: this chemical can be prepared by cobalt carbonate and acetic acid. The cobalt carbonate can be prepared by cobalt nitroate and sodium carbonate. Then you can go through the operation of filtering and crystallization to get the product. The equation is as follows: CoCO3 + 2CH3COOH → (CH3COO)2Co + CO2 + H2O.

Uses of Cobalt acetate tetrahydrate: it can be used as analytical reagents, catalysts and paint driers. And it can be used for the production of paint drying, dyeing mordant and fiberglass curing accelerant.

When you are using this chemical, please be cautious about it as the following:
This chemical is harmful by inhalation, in contact with skin and if swallowed. It is irritating to eyes, respiratory system and skin. It may cause sensitization by inhalation and skin contact. In addition, it is very toxic to aquatic organisms, may cause long-term adverse effects in the aquatic environment. When you are using it, wear suitable protective clothing and gloves and do not breathe dust. Avoid contact with skin. In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. In addition, do not empty into drains. In case of accident or if you feel unwell, seek medical advice immediately (show label where possible). Moreover, this material and its container must be disposed of as hazardous waste.

You can still convert the following datas into molecular structure:
(1)SMILES: [Co+2].[O-]C(=O)C.[O-]C(=O)C.O.O.O.O
(2)InChI: InChI=1/2C2H4O2.Co.4H2O/c2*1-2(3)4;;;;;/h2*1H3,(H,3,4);;4*1H2/q;;+2;;;;/p-2
(3)InChIKey: ZBYYWKJVSFHYJL-NUQVWONBAZ

The toxicity data is as follows:

Organism Test Type Route Reported Dose (Normalized Dose) Effect Source
rat LD50 oral 708mg/kg (708mg/kg) BEHAVIORAL: SOMNOLENCE (GENERAL DEPRESSED ACTIVITY)

LUNGS, THORAX, OR RESPIRATION: DYSPNEA
Food and Chemical Toxicology. Vol. 20, Pg. 311, 1982.