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617-86-7

Basic Information
CAS No.: 617-86-7
Name: Silane,triethyl-
Molecular Structure:
Molecular Structure of 617-86-7 (Silane,triethyl-)
Formula: C6H16Si
Molecular Weight: 116.28
Synonyms: Triethylsilyl hydride;
EINECS: 210-535-3
Density: 0.728g/mLat 25°C(lit.)
Melting Point: -157 °C
Boiling Point: 107.499 °C at 760 mmHg
Flash Point: 25°F
Solubility: Miscible with water.
Appearance: Clear liquid
Hazard Symbols: FlammableF, IrritantXi
Risk Codes: 11-36/37/38
Safety: 9-16-29-33-37/39-26
Transport Information: UN 1993 3/PG 2
PSA: 0.00000
LogP: 2.27320
Synthetic route
2117-34-2

triethylmethoxysilane

617-86-7

triethylsilane

Conditions
ConditionsYield
With N,N,N,N,N,N-hexamethylphosphoric triamide; sodium tetrahydroborate; ethyl bromide; tetraoctyl ammonium bromide In benzene-d6 at 20℃; for 24h; Reagent/catalyst; Solvent;96%
13399-93-4

3-(trimethylsilyl)propane-1-thiol

4149-29-5

bis(triethylsilyl)mercury

A

617-86-7

triethylsilane

B

1-Triethylsilanylsulfanyl-3-trimethylsilanyl-propane

Conditions
ConditionsYield
In benzene Heating;A n/a
B 89.5%
994-30-9

triethylsilyl chloride

617-86-7

triethylsilane

Conditions
ConditionsYield
With sodium tetrahydroborate In acetonitrile at 20℃; for 0.25h; Inert atmosphere;88%
With lithium hydride In tetrahydrofuran at 20 - 60℃; Reagent/catalyst; Solvent;82%
Stage #1: triethylsilyl chloride With magnesium In tetrahydrofuran at 75℃; for 12h; Inert atmosphere;
Stage #2: Acidic conditions;
80%
7538-45-6

2-mercaptoethyl(trimethoxysilane)

4149-29-5

bis(triethylsilyl)mercury

A

617-86-7

triethylsilane

B

C11H28O3SSi2

Conditions
ConditionsYield
In benzene Heating;A n/a
B 87.3%
30817-94-8

(mercaptomethyl)trimethoxysilane

4149-29-5

bis(triethylsilyl)mercury

A

617-86-7

triethylsilane

B

triethyl(trimethoxysilylmethylthio)silane

Conditions
ConditionsYield
In benzene at 50℃; for 0.25h;A n/a
B 80%
109-65-9

1-bromo-butane

92465-73-1

triethylsilylcalcium chloride

A

617-86-7

triethylsilane

B

994-96-7

butyltriethylsilane

Conditions
ConditionsYield
for 1h; Ambient temperature;A 1.1%
B 26%
108-86-1

bromobenzene

92465-73-1

triethylsilylcalcium chloride

A

617-86-7

triethylsilane

B

2987-77-1

triethylphenylsilane

Conditions
ConditionsYield
for 1h; Ambient temperature;A 3%
B 24%
462-06-6

fluorobenzene

92465-73-1

triethylsilylcalcium chloride

A

617-86-7

triethylsilane

B

2987-77-1

triethylphenylsilane

Conditions
ConditionsYield
for 1h; Ambient temperature;A 15%
B n/a
92465-73-1

triethylsilylcalcium chloride

108-90-7

chlorobenzene

A

617-86-7

triethylsilane

B

2987-77-1

triethylphenylsilane

Conditions
ConditionsYield
for 1h; Ambient temperature;A 10%
B 5%
78-10-4

tetraethoxy orthosilicate

557-20-0

diethylzinc

617-86-7

triethylsilane

Conditions
ConditionsYield
With sodium
358-43-0

triethylsilyl fluoride

617-86-7

triethylsilane

Conditions
ConditionsYield
With diethylaluminium hydride
Multi-step reaction with 2 steps
1: I2; AlI3
View Scheme
597-67-1

ethoxytriethylsilane

557-20-0

diethylzinc

617-86-7

triethylsilane

Conditions
ConditionsYield
With sodium
With Na In not given
994-49-0

hexaethyl disiloxane

617-86-7

triethylsilane

Conditions
ConditionsYield
With triethylaluminum
925-90-6

ethylmagnesium bromide

617-86-7

triethylsilane

Conditions
ConditionsYield
With diethyl ether; trichlorosilane
With trichlorosilane In diethyl ether
2386-64-3

ethylmagnesium chloride

617-86-7

triethylsilane

Conditions
ConditionsYield
With diethyl ether; trichlorosilane
542-91-6

H2SiEt2

A

617-86-7

triethylsilane

B

2814-79-1

ethylsilane

Conditions
ConditionsYield
With sulfur trioxide; zirconium(IV) oxide at 99.9℃; under 30 Torr; for 0.583333h; Product distribution; other alkylsilanes, var. temp., var. pretreatment of catalyst;
1112-48-7

triethyl-bromo-silane

617-86-7

triethylsilane

Conditions
ConditionsYield
With N,N,N,N,N,N-hexamethylphosphoric triamide; ytterbium In tetrahydrofuran Yield given;
925-90-6

ethylmagnesium bromide

101519-12-4

sodiumtris(benzene-1,2 diolato)silicate

617-86-7

triethylsilane

Conditions
ConditionsYield
With lithium aluminium tetrahydride Yield given. Multistep reaction;
101631-06-5

triethylsilyl hydrotrioxide

617-86-7

triethylsilane

Conditions
ConditionsYield
In dichloromethane at -60℃; for 2.5h;
994-30-9

triethylsilyl chloride

71-43-2

benzene

A

617-86-7

triethylsilane

B

2987-77-1

triethylphenylsilane

Conditions
ConditionsYield
With calcium 1) 900 deg C, 0.005 Torr, 2) 1 h, r.t., 0.005 Torr; Yield given. Multistep reaction. Yields of byproduct given;
617-86-7

triethylsilane

111-87-5

octanol

17957-36-7

1-octyl triethylsilyl ether

Conditions
ConditionsYield
cationic dirhodium(II) complex at 50℃; for 24h;100%
With Rh/AlO(OH) In toluene at 25℃; for 24h; Inert atmosphere;90%
dirhodium(II) tetrakis(perfluorobutyrate) In dichloromethane for 3h; Product distribution; Ambient temperature; var. alcohols; rel. reactivities for triethylsilane alcoholysis; var. catalysts;86%
617-86-7

triethylsilane

597-52-4

Triethylsilanol

Conditions
ConditionsYield
With 5%-palladium/activated carbon; water In ethyl acetate100%
With water at 20℃; for 0.25h;99%
With water In tetrahydrofuran at 25℃; for 0.0166667h; Catalytic behavior;99%
617-86-7

triethylsilane

80-62-6

methacrylic acid methyl ester

18002-64-7

β-triethylsilanyl-isobutyric acid methyl ester

Conditions
ConditionsYield
bis(benzonitrile)dichloroplatinum(II); triethylphosphine for 24h;100%
With platinum on activated charcoal
With dihydrogen hexachloroplatinate
617-86-7

triethylsilane

65-85-0

benzoic acid

1018-20-8

triethylsilyl benzoate

Conditions
ConditionsYield
With indium(III) bromide In dichloromethane-d2 at 20℃;100%
With palladium diacetate In benzene-d6 for 4h; dehydrocoupling reaction; Heating;95%
With zinc(II) chloride In N,N-dimethyl-formamide at 120℃; for 25h;85%
617-86-7

triethylsilane

14355-62-5

triethyl-2-phenylethylsilane

Conditions
ConditionsYield
cerium(IV) oxide; gold In toluene at 70℃; for 8h;100%
With tris(pentafluorophenyl)borate In dichloromethane at 20℃; for 12h;96%
With dimanganese decacarbonyl; bis(3,5-bis(trifluoromethyl)phenyl)(2’,4’,6’-triisopropyl-3,6-dimethoxy-[1,1’-biphenyl]-2-yl)phosphine at 120℃; for 24h; Sealed tube;83%
617-86-7

triethylsilane

592-41-6

1-hexene

13810-04-3

n-hexyltriethylsilane

Conditions
ConditionsYield
at 90℃; for 5h; Inert atmosphere;100%
at 90℃; for 5h; Inert atmosphere;100%
With C26H31F5NZn(1+)*C24BF20(1-) In dichloromethane-d2 at 20℃; for 28h; Reagent/catalyst; Inert atmosphere; Glovebox;100%
617-86-7

triethylsilane

100-52-7

benzaldehyde

13959-92-7

benzyl triethylsilyl ether

Conditions
ConditionsYield
cerium(IV) oxide; gold In toluene at 70℃; for 8h;100%
With C16H25AlBN6(1+)*C19H3BF15(1-) In chloroform-d1 at 75℃; for 0.5h;99%
With (1,3-dimesityl-5-methyl-6-oxo-6H-pyrimidin-2-ylidene-4-olate)-copper(I) lithium(THF)2; sodium t-butanolate In tetrahydrofuran at 65℃; for 2h; Schlenk technique; Inert atmosphere;98%
617-86-7

triethylsilane

98-86-2

acetophenone

112473-30-0, 18442-52-9

triethyl(1-phenylethoxy)silane

Conditions
ConditionsYield
With (1,3-dimesityl-5-methyl-6-oxo-6H-pyrimidin-2-ylidene-4-olate)-copper(I) lithium(THF)2; sodium t-butanolate In tetrahydrofuran at 65℃; for 1h; Reagent/catalyst; Temperature; Time; Schlenk technique; Inert atmosphere;100%
With C42H43BN3P2(1+)*C18HBF15(1-) In chloroform at 40℃; for 2h; Reagent/catalyst; Temperature; Schlenk technique; Glovebox;99%
Stage #1: acetophenone With C8H10BiCl2N; C4H6AgN2(1+)*C24H12BCl8(1-) In dichloromethane-d2 at 25℃;
Stage #2: triethylsilane In dichloromethane at 25℃;
99%
617-86-7

triethylsilane

821-10-3

1,4-Dichloro-2-butyne

1,4-dichloro 2-triethylsilylbut-2-ene
108930-44-5

1,4-dichloro 2-triethylsilylbut-2-ene

Conditions
ConditionsYield
With dihydrogen hexachloroplatinate In tetrahydrofuran at 85℃; for 4h;100%
With platinum(IV) oxide In toluene at 100℃; for 24h; diastereoselective reaction;75%
dihydrogen hexachloroplatinate
With dihydrogen hexachloroplatinate at 170℃; for 1h;
617-86-7

triethylsilane

100-51-6

benzyl alcohol

13959-92-7

benzyl triethylsilyl ether

Conditions
ConditionsYield
{Rh2(OAc)3[(R)-PhCH2SCH(Me)C(O)OEt]2}BF4 In dichloromethane at 50℃; for 24h;100%
With C23H26IrN2(1+)*C32H12BF24(1-) In 1,2-dichloro-ethane at 20℃; for 0.0166667h; Catalytic behavior; Schlenk technique; Inert atmosphere;100%
With Pd/XC-72-700-Ar at 25℃; for 0.03h;99%
109-99-9

tetrahydrofuran

617-86-7

triethylsilane

2751-87-3

n-butoxytriethylsilane

Conditions
ConditionsYield
nickel at 100℃; for 1h;100%
With [(POCOP)Ir(H)(acetone)]+[B(C6F5)4]- In dichloromethane-d2 at 22℃; for 3h;100 %Spectr.
617-86-7

triethylsilane

622-97-9

1-ethenyl-4-methylbenzene

75476-54-9

(E)-1-(p-methylphenyl)-2-(triethylsilyl)ethylene

Conditions
ConditionsYield
dodecacarbonyl-triangulo-triruthenium In benzene at 80℃; for 5h;100%
With dimanganese decacarbonyl; N,N-bis(diphenylphosphino)isopropylamine at 140℃; for 24h; Sealed tube;82%
With norborn-2-ene; chloro(1,5-cyclooctadiene)rhodium(I) dimer; triphenylphosphine In tetrahydrofuran at 100℃; for 2h; Schlenk technique; Inert atmosphere; Sealed tube;82%
617-86-7

triethylsilane

141-79-7

4-methyl-pent-3-en-2-one

57137-74-3

(E)-4-methyl-2-(triethylsilyloxy)pent-2-ene

Conditions
ConditionsYield
RhCl(PPh3)3 at 40℃;100%
617-86-7

triethylsilane

4526-07-2

1,4-bis(trimethylsilyl)-1,3-butadiyne

103716-77-4

(E)-2-triethylsilyl-1,4-bis(trimethylsilyl)-1-buten-3-yne

Conditions
ConditionsYield
With tetrakis(triphenylphosphine)platinum at 100℃; for 1h;100%
617-86-7

triethylsilane

4526-07-2

1,4-bis(trimethylsilyl)-1,3-butadiyne

103716-76-3

1,3-bis(triethylsilyl)-1,4-bis(trimethylsilyl)-1,2-butadiene

Conditions
ConditionsYield
dihydrogen hexachloroplatinate In isopropyl alcohol at 80℃; for 0.5h;100%
With dihydrogen hexachloroplatinate In isopropyl alcohol at 80℃; for 0.5h;100%
617-86-7

triethylsilane

123239-66-7

(3-methoxynaphthalen-2-yl)phenylmethanol

Triethyl-[(3-methoxy-naphthalen-2-yl)-phenyl-methoxy]-silane

Conditions
ConditionsYield
In dichloromethane at 0℃;100%
617-86-7

triethylsilane

103716-81-0

(E)-2-dimethylphenylsilyl-1,4-bis(trimethylsilyl)-1-buten-3-yne

103716-84-3

3-dimethylphenylsilyl-1-triethylsilyl-1,4-bis(trimethylsilyl)-1,2-butadiene

Conditions
ConditionsYield
With RhCl(PPh3)3 at 100℃; for 13h;100%
dihydrogen hexachloroplatinate93%
617-86-7

triethylsilane

104106-61-8

4aβ,8-dimethyl-4a,5,6,8aα-tetrahydro-2<1H>-naphthalenone

104504-88-3

7-triethylsilyloxy-1,4aβ-dimethyl-3,4,4a,5,8,8aα-hexahydronaphthalene

Conditions
ConditionsYield
Wilkinson's catalyst for 6h; Ambient temperature;100%
617-86-7

triethylsilane

151545-05-0

C72H140Si14

2-<2,4,6-trisphenyl>-1,1,1-triethyl-2-mesityldisilane

Conditions
ConditionsYield
In toluene at 70℃;100%
In tetrahydrofuran for 10h; Heating;77%
In toluene at 60℃; Rate constant; Mechanism; Kinetics; energy data: Ea, ΔH(excit.), SDS(excit.); var. temp.;
In toluene at 81.3℃; Rate constant; Kinetics; Thermodynamic data; Ea, ΔH(excit.), SDS(excit.); var. temp.;
617-86-7

triethylsilane

98-83-9

isopropenylbenzene

17911-16-9

triethyl(2-phenylpropyl)silane

Conditions
ConditionsYield
platinum(II) chloride at 24.9℃; for 96h;100%
With fluorotris(pentafluorophenyl)phosphonium tetrakis(pentafluorophenyl)borate In dichloromethane at 20℃; for 1h; Inert atmosphere;99%
With tris(pentafluorophenyl)borate In dichloromethane at 20℃;97%
617-86-7

triethylsilane

536-74-3

phenylacetylene

21209-32-5

(E)-1-(triethylsilyl)-2-phenylethene

Conditions
ConditionsYield
carbonylhydridetris(triphenylphosphine)rhodium(I) at 20℃; for 72h; magnetic field 40 Oe;100%
With dicyclohexylphosphino-2′,4′,6′-triisopropylbiphenyl; platinum(II) chloride In tetrahydrofuran at 60℃; for 1.25h;98%
With sodium iodide In tetrahydrofuran at 20℃; for 1h; Catalytic behavior; stereoselective reaction;98%
617-86-7

triethylsilane

(2RS,3RS,4RS,5RS,6RS,7RS)-3,6-dimesityl-3,6-bis<2,4,6-trisphenyl>-3,6-disilatetracyclo<6.4.02,4.05,7>dodeca-1(8),9,11-triene

A

91-20-3

naphthalene

B

2-<2,4,6-trisphenyl>-1,1,1-triethyl-2-mesityldisilane

Conditions
ConditionsYield
In (2)H8-toluene at 120℃; for 30h;A n/a
B 100%
617-86-7

triethylsilane

(Z)-4,8-dimesityl-4,8-bis<2,4,6-trisphenyl>-4,8-disilabicyclo<5.1.0>octa-2,5-diene

A

2-<2,4,6-trisphenyl>-1,1,1-triethyl-2-mesityldisilane

B

71-43-2

benzene

Conditions
ConditionsYield
In (2)H8-toluene at 120℃; for 30h;A 100%
B n/a
617-86-7

triethylsilane

218937-15-6

2α,9α,10β,13α-tetraacetoxy-taxa-4(20),11-dien-5α-ol

325691-23-4

2α,9α,10β,13α-tetraacetoxy-5α-triethylsilyloxytaxa-4(20),11-diene

Conditions
ConditionsYield
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; for 2h;100%
617-86-7

triethylsilane

51060-11-8

2,2,4-trimethyl-hept-6-yn-3-one

(4RS,5SR)-4,6,6-trimethyl-5-phenyl-5-triethylsilyloxyhept-1-yne

Conditions
ConditionsYield
With tris(pentafluorophenyl)borate In toluene at 0℃; for 1h;100%
617-86-7

triethylsilane

552890-39-8

Acetic acid (2R,3S,5R,6S)-6-allyl-5-benzyloxy-2-phenylsulfanylethynyl-tetrahydro-pyran-3-yl ester

617673-36-6

Acetic acid (2R,3S,5R,6S)-6-allyl-5-benzyloxy-2-((Z)-2-phenylsulfanyl-2-triethylsilanyl-vinyl)-tetrahydro-pyran-3-yl ester

Conditions
ConditionsYield
biscobalthexacarbonyl-2-methyl-but-3-yn-2-ol In 1,2-dichloro-ethane at 60℃; for 1.5h;100%
biscobalthexacarbonyl-2-methyl-but-3-yn-2-ol In 1,2-dichloro-ethane
617-86-7

triethylsilane

109660-11-9

4,4-dimethyl-2-(naphthalen-2-yl)-4,5-dihydrooxazole

4,4-dimethyl-2-(3-triethylsilanylnaphthalen-2-yl)-4,5-dihydro-oxazole

Conditions
ConditionsYield
With norborn-2-ene; dodecacarbonyl-triangulo-triruthenium In toluene for 20h; Heating;100%
617-86-7

triethylsilane

3-methyl-2-(naphthalen-1-yl)pyridine

2-(2-(triethylsilyl)naphthalene-1-yl)-3-methylpyridine

Conditions
ConditionsYield
With norborn-2-ene; dodecacarbonyl-triangulo-triruthenium In toluene for 20h; Heating;100%
With norborn-2-ene; dodecacarbonyl-triangulo-triruthenium In toluene for 36h; Inert atmosphere; Schlenk technique; Reflux;59.6 mg
617-86-7

triethylsilane

13019-22-2

9-Decen-1-ol

566189-62-6

1-(triethylsilyl)oxy-9-decene

Conditions
ConditionsYield
AuCl(xanthphos) In acetone at 50℃; for 8h;100%
With copper (I) tert-butoxide; 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In toluene at 25℃; for 2h;95%
617-86-7

triethylsilane

107-05-1

3-chloroprop-1-ene

2290-35-9

(3-chloropropyl)triethylsilane

Conditions
ConditionsYield
copper dichloride at 200℃; for 45h;100%
copper diacetate at 200℃; for 45h;100%
copper(II) sulfate at 200℃; for 45h;100%
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Specification

The Triethylsilane is an organic compound with the formula C6H16Si. The IUPAC name of this chemical is triethylsilicon. With the CAS registry number 617-86-7, it is also named as Silane, triethyl-. The product's categories are Other Reagents; Reduction; Si (Classes of Silicon Compounds); Si-H Compounds; Silicon Compounds (for Synthesis); Synthetic Organic Chemistry; Alkyl Silanes; Hydrogensilanes Hydrogensiloxanes; Reducing Agents; Chemistry; Silanes; Synthetic Reagents. Besides, it is clear liquid, which should be stored in a dark closed and dry place. It is often used in organic synthesis, specifically for the hydrosilation of olefins to give alkyl silanes. It can also be used as a reducing agent since it has an active hydride.

Physical properties about Triethylsilane are: (1)ACD/LogP: 3.65; (2)ACD/LogD (pH 5.5): 3.65; (3)ACD/LogD (pH 7.4): 3.65; (4)ACD/BCF (pH 5.5): 349.789; (5)ACD/BCF (pH 7.4): 349.789; (6)ACD/KOC (pH 5.5): 2303.888; (7)ACD/KOC (pH 7.4): 2303.888; (8)#Freely Rotating Bonds: 3; (9)Enthalpy of Vaporization: 33.2 kJ/mol; (10)Boiling Point: 107.499 °C at 760 mmHg; (11)Vapour Pressure: 31.55 mmHg at 25°C.

Uses of Triethylsilane: it can be used to produce ethoxy-triethyl-silane. It will need reagent NaOEt.

When you are using this chemical, please be cautious about it as the following:
It is highly flammable. Please keep away from sources of ignition - No smoking. In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. Besides, this chemical is irritating to eyes, respiratory system and skin. When you are using it, wear suitable gloves and eye/face protection, do not breathe dust and take precautionary measures against static discharges.

You can still convert the following datas into molecular structure:
(1)SMILES: CC[SiH](CC)CC
(2)InChI: InChI=1/C6H16Si/c1-4-7(5-2)6-3/h7H,4-6H2,1-3H3
(3)InChIKey: AQRLNPVMDITEJU-UHFFFAOYAL
(4)Std. InChI: InChI=1S/C6H16Si/c1-4-7(5-2)6-3/h7H,4-6H2,1-3H3
(5)Std. InChIKey: AQRLNPVMDITEJU-UHFFFAOYSA-N