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CAS No.: | 6306-60-1 |
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Name: | 2,4-Dichlorophenylacetonitrile |
Article Data: | 23 |
Molecular Structure: | |
Formula: | C8H5Cl2N |
Molecular Weight: | 186.04 |
Synonyms: | Acetonitrile,(2,4-dichlorophenyl)- (6CI,7CI,8CI);2,4-Dichlorobenzyl cyanide;2-(2,4-Dichlorophenyl)acetonitrile;NSC 22988; |
EINECS: | 228-621-4 |
Density: | 1.333 g/cm3 |
Melting Point: | 58-61 °C(lit.) |
Boiling Point: | 286.9 °C at 760 mmHg |
Flash Point: | 124 °C |
Appearance: | white to light yellow crystal powder |
Hazard Symbols: | Xi,Xn |
Risk Codes: | 36/37/38-20/21/22 |
Safety: | 26-36/37/39 |
PSA: | 23.79000 |
LogP: | 3.05948 |
Conditions | Yield |
---|---|
With tetrabutylammomium bromide In water; 1,2-dichloro-ethane at 70℃; for 5h; | 88.1% |
With sodium iodide In methanol for 6h; Finkelstein reaction; Reflux; | 87% |
With polyethylene glycol functionalized magnetic dicationic ionic liquid In water for 1.25h; Reflux; Green chemistry; | 84% |
2,4-dichloro-1-(methoxymethoxy)methyl benzene
tetra-n-butylammonium cyanide
2,4-Dichlorophenylacetonitrile
Conditions | Yield |
---|---|
With phosphotungstic acid at 130 - 142℃; for 0.05h; Microwave irradiation; Ionic liquid; chemoselective reaction; | 89% |
With 1-(n-butyl)-3-methylimidazolium tetrachloroindate at 135 - 140℃; for 0.0916667h; Microwave irradiation; Neat (no solvent); chemoselective reaction; | 82% |
With 1-methyl-3H-imidazolium nitrate at 135 - 140℃; for 0.075h; Microwave irradiation; | 82% |
2,4-dichlorophenylacetic acid
2,4-Dichlorophenylacetonitrile
Conditions | Yield |
---|---|
With sodium azide; TEA; triethylphosphine; (bis-(2-methoxyethyl)amino)sulfur trufluoride In dichloromethane; dimethyl sulfoxide at 0℃; for 30h; | 92% |
sodium cyanide
2,4-dichlorobenzyl bromide
2,4-Dichlorophenylacetonitrile
Conditions | Yield |
---|---|
In ethanol; water | 93% |
With silica-coated Fe3O4 nanoparticles-functionalized polycalix[4]resorcinarene In water at 90℃; for 0.333333h; Green chemistry; | 80% |
2,4-dichloro-1-[(ethoxymethoxy)methyl]benzene
tetra-n-butylammonium cyanide
2,4-Dichlorophenylacetonitrile
Conditions | Yield |
---|---|
With 1-(n-butyl)-3-methylimidazolium tetrachloroindate at 135 - 140℃; for 0.0916667h; Microwave irradiation; Neat (no solvent); chemoselective reaction; | 80% |
Conditions | Yield |
---|---|
With ethanol |
Conditions | Yield |
---|---|
In dimethyl sulfoxide at 40 - 50℃; for 5h; Yield given; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: PBr3 / CH2Cl2 View Scheme | |
Multi-step reaction with 2 steps 1: phosphorus tribromide / dichloromethane; N,N-dimethyl-formamide / 80 °C 2: ethanol; water View Scheme | |
Multi-step reaction with 3 steps 1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / -78 - 20 °C 2: tris(pentafluorophenyl)borate / 1,2-dichloro-ethane / 0.08 h / 20 °C / Glovebox; Schlenk technique 3: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 18 h / 20 °C View Scheme |
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 18h; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: SOCl2, (PhCO)2O2 View Scheme | |
Multi-step reaction with 2 steps 1: 2,2'-azobis(isobutyronitrile); chlorine / 3 h / 110 °C 2: tetrabutylammomium bromide / 1,2-dichloro-ethane; water / 5 h / 70 °C View Scheme |
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2,4-Dichlorophenylacetonitrile is also named as 2-(2,4-Dichlorophenyl)acetonitrile;2,4-Dichlorobenzeneacetonitrile;Acetonitrile, (2,4-dichlorophenyl)-;2,4-dichloro cyanobenzene;2,4-Dichlorophenylacetonitrile,98%,and so on.2,4-Dichlorophenylacetonitrile is usually white powder.
CAS: 6306-60-1
Molecular Formula: C8H5Cl2N
Molecular Weight: 186.04
EINECS: 228-621-4
Molecular structure:
Melting point: 58-61 °C(lit.)
Flash point: 176 °C
BRN: 2047688