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634-47-9

Basic Information
CAS No.: 634-47-9
Name: 2-CHLOROLEPIDINE
Article Data: 21
Molecular Structure:
Molecular Structure of 634-47-9 (2-CHLOROLEPIDINE)
Formula: C10H8ClN
Molecular Weight: 177.633
Synonyms: Lepidine,2-chloro- (6CI,7CI,8CI);2-Chloro-4-methylquinoline;2-Chlorolepidine;NSC96476;
EINECS: 211-209-3
Density: 1.225 g/cm3
Melting Point: 55-58 °C(lit.)
Boiling Point: 296 °C at 760 mmHg
Flash Point: 158.2 °C
Appearance: white to light yellow crystal powder
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-37/39
PSA: 12.89000
LogP: 3.19660
Synthetic route
4053-40-1

4-methylquinoline 1-oxide

634-47-9

2-chloro-4-methylquinoline

Conditions
ConditionsYield
With trichlorophosphate In dichloromethane; N,N-dimethyl-formamide at 0 - 25℃; Inert atmosphere; regioselective reaction;81%

(4-methylquinolin-2-yl)diphenyl(6-(trifluoromethyl)pyridin-3-yl)phosphonium trifluoromethanesulfonate

634-47-9

2-chloro-4-methylquinoline

Conditions
ConditionsYield
With lithium chloride In 1,4-dioxane at 80℃; for 72h; Inert atmosphere; Sealed tube; regioselective reaction;32%
607-66-9

4-methylquinolin-2-ol

634-47-9

2-chloro-4-methylquinoline

Conditions
ConditionsYield
With phosphorus pentachloride; trichlorophosphate for 24h; Chlorination; Heating;96%
With trichlorophosphate for 10h; Heating;82%
With phosphorus pentachloride; trichlorophosphate
10286-18-7

2-Chloro-4-methylquinoline 1-oxide

634-47-9

2-chloro-4-methylquinoline

Conditions
ConditionsYield
With tris(bipyridine)ruthenium(II) dichloride hexahydrate; di-tert-butyl 1,4-dihydro-2,6-dimethyl-3,5-pyridine-dicarboxylate In acetonitrile at 20℃; for 0.0833333h; Inert atmosphere; Irradiation; chemoselective reaction;82%
607-66-9

4-methyl-1,2-dihydroquinolin-2-one

634-47-9

2-chloro-4-methylquinoline

Conditions
ConditionsYield
With phosphorus pentachloride; trichlorophosphate at 135 - 140℃;
With phosphorus pentachloride; benzoyl chloride at 250℃;
With ((1,3,5-triazine-2,4,6-triyl)tris(oxy))tris(triphenylphosphonium) chloride In neat (no solvent) at 140 - 150℃; for 2h;
With trichlorophosphate at 120℃; for 2h;
2-oxy-4-methyl-quinoline

2-oxy-4-methyl-quinoline

634-47-9

2-chloro-4-methylquinoline

Conditions
ConditionsYield
With trichlorophosphate at 80 - 85℃;
676-58-4

methylmagnesium chloride

703-61-7

2,4-dichloroquinoline

634-47-9

2-chloro-4-methylquinoline

Conditions
ConditionsYield
With zinc dibromide In tetrahydrofuran
102-01-2

N-phenylacetoacetamide

634-47-9

2-chloro-4-methylquinoline

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sulfuric acid / 1 h / 100 °C
2: trichlorophosphate / 2 h / 120 °C
View Scheme
Multi-step reaction with 2 steps
1: Polyphosphoric acid / 130 - 140 °C
2: trichlorophosphate; pyridine / 80 - 90 °C
View Scheme
62-53-3

aniline

[(Xantphos)2Pd(3-methyl-1-butenyl]OTf

[(Xantphos)2Pd(3-methyl-1-butenyl]OTf

634-47-9

2-chloro-4-methylquinoline

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: 0.07 h / microwave irradiation
1.2: H2SO4 / 0.08 h / microwave irradiation
2.1: 82 percent / POCl3 / 10 h / Heating
View Scheme
62-53-3

aniline

634-47-9

2-chloro-4-methylquinoline

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 3 h / 185 °C
2: sulfuric acid / 1 h / 100 °C
3: trichlorophosphate / 2 h / 120 °C
View Scheme
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Chemistry

Molecular Structure:

Molecular Formula: C10H8ClN
Molecular Weight: 177.6302
IUPAC Name: 2-Chloro-4-methylquinoline
Synonyms of Quinoline,2-chloro-4-methyl- (CAS NO.634-47-9): 2-Chloro-4-methylquinoline ; 2-Chlorolepidine ; EINECS 211-209-3 ; NSC 96476 ; Lepidine, 2-chloro- (8CI) ; Quinoline, 2-chloro-4-methyl- (9CI)
CAS NO: 634-47-9
Classification Code: Quinoline&Isoquinoline ; Alkylquinolines ; Haloquinolines ; Quinolines
Melting point: 55-58 °C 
Index of Refraction: 1.634
Molar Refractivity: 51.9 cm3
Molar Volume: 144.9 cm3
Surface Tension: 46.5 dyne/cm
Density: 1.225 g/cm3
Flash Point: 158.2 °C
Enthalpy of Vaporization: 51.43 kJ/mol
Boiling Point: 296 °C at 760 mmHg
Vapour Pressure: 0.0026 mmHg at 25°C

Uses

  Quinoline,2-chloro-4-methyl- (CAS NO.634-47-9) is used in organic synthesis.

Safety Profile

Hazard Codes of Quinoline,2-chloro-4-methyl- (CAS NO.634-47-9): IrritantXi
Risk Statements: 36/37/38 
R36/37/38: Irritating to eyes, respiratory system and skin.
Safety Statements: 26-37/39-36 
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. 
S37/39: Wear suitable gloves and eye/face protection. 
S36: Wear suitable protective clothing.
WGK Germany: 3