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CAS No.: | 63470-85-9 |
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Name: | 2-methoxy-N-[2-nitro-5-(phenylthio)phenyl]acetamide |
Article Data: | 4 |
Molecular Structure: | |
Formula: | C15H14 N2 O4 S |
Molecular Weight: | 318.353 |
Synonyms: | 2-methoxy-N-[2-nitro-5-(phenylthio)phenyl]acetamide |
Density: | 1.35g/cm3 |
Boiling Point: | 551.7°C at 760 mmHg |
Flash Point: | 287.5°C |
PSA: | 112.94000 |
LogP: | 4.50360 |
methyl methoxyacetate
2-nitro-5-phenylthioaniline
2-methoxy-N-(2-nitro-5-(phenylsulfanyl)phenyl)acetamide
Conditions | Yield |
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at 120 - 130℃; Temperature; | 95.5% |
2-nitro-5-phenylthioaniline
2-methoxyacetic acid
2-methoxy-N-(2-nitro-5-(phenylsulfanyl)phenyl)acetamide
Conditions | Yield |
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With pyridine; thionyl chloride In toluene at 75 - 110℃; for 10.5h; Reagent/catalyst; Solvent; Temperature; | 94.8% |
bromobenzene
2-methoxy-N-(2-nitro-5-(phenylsulfanyl)phenyl)acetamide
Conditions | Yield |
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Multi-step reaction with 2 steps 1: potassium carbonate / 150 - 160 °C / Inert atmosphere 2: 120 - 130 °C View Scheme |
2-methoxy-N-(2-nitro-5-(phenylsulfanyl)phenyl)acetamide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: potassium carbonate / 130 - 135 °C / Inert atmosphere 2: 120 - 130 °C View Scheme |
chlorobenzene
2-methoxy-N-(2-nitro-5-(phenylsulfanyl)phenyl)acetamide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: potassium carbonate / 130 - 135 °C / Inert atmosphere 2: 120 - 130 °C View Scheme |
2-methoxy-N-(2-nitro-5-(phenylsulfanyl)phenyl)acetamide
2-amino-5-phenylthio-(2-methoxy)acetanilide
Conditions | Yield |
---|---|
With hydrogen In methanol at 25 - 35℃; under 750.075 - 3750.38 Torr; for 12h; Temperature; Solvent; Autoclave; | 94.2% |
With hydrogen; nickel In chlorobenzene at 35 - 55℃; under 22065.2 - 36775.4 Torr; | |
With hydrogen; nickel In 1,2-dichloro-benzene at 40 - 50℃; under 22065.2 - 36775.4 Torr; |
2-methoxy-N-(2-nitro-5-(phenylsulfanyl)phenyl)acetamide
Conditions | Yield |
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With hydrogen; nickel In tetrahydrofuran at 30 - 40℃; under 36775.4 Torr; |