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6372-42-5

Basic Information
CAS No.: 6372-42-5
Name: Cyclohexyldiphenylphosphine
Article Data: 30
Molecular Structure:
Molecular Structure of 6372-42-5 (Cyclohexyldiphenylphosphine)
Formula: C18H21 P
Molecular Weight: 268.338
Synonyms: Cyclohexyldiphenylphosphine;Diphenylcyclohexylphosphine
EINECS: 228-904-2
Melting Point: 58-62 ºC
Boiling Point: 374 °C at 760 mmHg
Flash Point: 189.4 °C
Solubility: Insoluble in water
Appearance: white to light yellow crystal powder
Risk Codes: 36/37/38
Safety: S24/25
PSA: 13.59000
LogP: 4.45200
Synthetic route
1079-66-9

chloro-diphenylphosphine

1,3-dioxoisoindolin-2-yl cyclohexanecarboxylate

6372-42-5

cyclohexyldiphenylphosphine

Conditions
ConditionsYield
With N,N,N',N'',N'''-pentamethyldiethylenetriamine; zinc In N,N-dimethyl-formamide at 20℃; for 12h; Reagent/catalyst; Time;95%
13689-20-8

(cyclohexyl)diphenylphosphane oxide

6372-42-5

cyclohexyldiphenylphosphine

Conditions
ConditionsYield
With copper(II) trifluoromethanesulfonate; 1,1,3,3-Tetramethyldisiloxane In toluene at 100℃; Inert atmosphere;86%
With oxalyl dichloride; hydrogen In chloroform-d1 at 130℃; under 60006 Torr; for 18h; Reagent/catalyst;85%
With copper(II) bis(trifluoromethanesulfonate); 1,1,3,3-tetramethyldisilazane In toluene at 80℃;82%
542-18-7

cyclohexyl chloride

4376-01-6

sodium diphenylphosphide

6372-42-5

cyclohexyldiphenylphosphine

Conditions
ConditionsYield
In tetrahydrofuran at 25℃; for 2h; Inert atmosphere;73%
626-62-0

1-iodocyclohexane

829-85-6

diphenylphosphane

6372-42-5

cyclohexyldiphenylphosphine

Conditions
ConditionsYield
With 1,3-dicyano-5-fluoro-2,4,6-tris(diphenylamino)benzene; N-ethyl-N,N-diisopropylamine In acetonitrile for 24h; Inert atmosphere; Glovebox; Sealed tube; Irradiation;73%
108-85-0

1-bromocyclohexane

603-35-0

triphenylphosphine

6372-42-5

cyclohexyldiphenylphosphine

Conditions
ConditionsYield
Stage #1: triphenylphosphine In tetrahydrofuran at 20℃; Inert atmosphere;
Stage #2: 1-bromocyclohexane In tetrahydrofuran for 0.166667h; Inert atmosphere;
70%
With ammonia; sodium 2.) irradiation, 30 min; Multistep reaction;
1336-21-6

ammonium hydroxide

931-51-1

cyclohexylmagnesiumchloride

644-97-3

Dichlorophenylphosphine

100-58-3

phenylmagnesium bromide

6372-42-5

cyclohexyldiphenylphosphine

Conditions
ConditionsYield
With hydrogenchloride In water70%
542-18-7

cyclohexyl chloride

603-35-0

triphenylphosphine

6372-42-5

cyclohexyldiphenylphosphine

Conditions
ConditionsYield
With ammonia; sodium 2.) irradiation, 180 min; Multistep reaction;
603-35-0

triphenylphosphine

A

6476-37-5

dicyclohexylphenylphosphine

B

6372-42-5

cyclohexyldiphenylphosphine

C

2622-14-2

tricyclohexylphosphine

Conditions
ConditionsYield
With n-butyllithium; hydrogen; bis(2,6-diisopropylphenoxy) trichloroniobium(V) In hexane; benzene at 60℃; under 62057.8 Torr; Kinetics; var. of catalyst;
With n-butyllithium; hydrogen; In hexane; benzene at 60℃; under 62057.8 Torr;
15658-08-9

dicyclohexylzinc(II)

1079-66-9

chloro-diphenylphosphine

6372-42-5

cyclohexyldiphenylphosphine

Conditions
ConditionsYield
In tetrahydrofuran at 0℃; for 1h;
108-85-0

1-bromocyclohexane

1079-66-9

chloro-diphenylphosphine

6372-42-5

cyclohexyldiphenylphosphine

Conditions
ConditionsYield
With pyridine; tris-(trimethylsilyl)silane; 1,1'-azobis(1-cyanocyclohexanenitrile) In benzene for 20h; Heating;
Stage #1: 1-bromocyclohexane; chloro-diphenylphosphine With manganese; CpCr[(XylNCMe)2CH]; lead(II) bromide In tetrahydrofuran at 25℃; for 28h;
Stage #2:
92 %Spectr.
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Chemistry

Molecular Structure of Cyclohexyldiphenylphosphine (CAS NO.6372-42-5):

IUPAC Name: Cyclohexyl(diphenyl)phosphane 
Molecular Formula: C18H21P
Molecular Weight: 268.34
EINECS: 228-904-2 
XLogP3-AA: 4.9
H-Bond Donor: 0
H-Bond Acceptor: 0
Melting Point: 58-62 °C(lit.)
Flash Point: 189.4 °C
Enthalpy of Vaporization: 59.7 kJ/mol
Boiling Point: 374 °C at 760 mmHg
Vapour Pressure: 1.85E-05 mmHg at 25 °C
Water Solubility: insoluble
Sensitive: Air Sensitive
Appearance: white to light yellow crystal powder
Canonical SMILES: C1CCC(CC1)P(C2=CC=CC=C2)C3=CC=CC=C3
InChI: InChI=1S/C18H21P/c1-4-10-16(11-5-1)19(17-12-6-2-7-13-17)18-14-8-3-9-15-18/h1-2,4-7,10-13,18H,3,8-9,14-15H2
InChIKey: ZXKWUYWWVSKKQZ-UHFFFAOYSA-N
Product Categories: Ligand; Phosphine Ligands; Synthetic Organic Chemistry; Basic Phosphine LigandsCatalysis and Inorganic Chemistry; Catalysis and Inorganic Chemistry; Cross-Coupling; Phosphine Ligands; Phosphorus Compounds

Safety Profile

Safety Information of Cyclohexyldiphenylphosphine (CAS NO.6372-42-5):
Safety Statements: 24/25 
S24/25:Avoid contact with skin and eyes.
WGK Germany: 3
RTECS: SY8387500

Specification

 Cyclohexyldiphenylphosphine (CAS NO.6372-42-5), its Synonyms are Diphenylcyclohexylphosphine ; Phosphine, cyclohexyldiphenyl- ; Cyclohexyldiphenyl-phosphin ; Cyclohexyl diphenyl phosphine .