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| CAS No.: | 656-66-6 |
|---|---|
| Name: | 3-Fluoro-4-iodoaniline |
| Article Data: | 6 |
| Molecular Structure: | |
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|
| Formula: | C6H5FIN |
| Molecular Weight: | 237.015 |
| Synonyms: | Aniline,3-fluoro-4-iodo- (7CI,8CI); |
| EINECS: | 690-811-1 |
| Density: | 2.009 g/cm3 |
| Melting Point: | 76-77 °C |
| Boiling Point: | 273.722 °C at 760 mmHg |
| Flash Point: | 119.343 °C |
| Solubility: | Slightly soluble in water (228.3 mg/L at 25°C). |
| PSA: | 26.02000 |
| LogP: | 2.59370 |
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| Conditions | Yield |
|---|---|
| With iodine; sodium hydrogencarbonate In water at 20℃; for 0.5h; | A 74% B 6% C 4% |
| Conditions | Yield |
|---|---|
| With iron(III) chloride; N-iodo-succinimide; 1-butyl-3-methylimidazolium trifluoromethanesulfonimide at 20℃; for 2h; Inert atmosphere; | 62% |
| With iodine; sodium hydrogencarbonate In water at 20℃; for 3h; | 62% |
| With sodium periodate; sulfuric acid; iodine In acetic acid at 80℃; for 4h; | 50% |
| With iodine; mercury(II) oxide In ethanol | |
| With iodine; sodium hydrogencarbonate In water at 20℃; |
| Conditions | Yield |
|---|---|
| With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide In triethylamine at 20℃; for 46h; Sonogashira Cross-Coupling; Schlenk technique; Inert atmosphere; | 97% |
| With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine In tetrahydrofuran at 20℃; for 21h; Sonogashira Cross-Coupling; Inert atmosphere; |
| Conditions | Yield |
|---|---|
| With sodium hydroxide In ethylene glycol at 100℃; for 2h; Hiyama Coupling; | 92% |
| Conditions | Yield |
|---|---|
| With sodium tris(acetoxy)borohydride; acetic acid In dichloromethane at 20℃; for 2h; | 70% |
| Conditions | Yield |
|---|---|
| With sodium tris(acetoxy)borohydride; acetic acid In dichloromethane at 20℃; for 2h; | 70% |
| Conditions | Yield |
|---|---|
| With copper(I) oxide In dimethyl sulfoxide at 130℃; for 10h; | 65% |
- 656-66-6
3-fluoro-4-iodoaniline
- 320592-15-2
1,4-anhydro-3,5-di-O-benzyl-2-deoxy-L-erythro-pent-1-enitol
- 320592-21-0
4-(5-((benzyloxy)methyl)-4-(benzyloxy)-2,5-dihydro-β-L-furan-2-yl)-3-fluoroaniline
| Conditions | Yield |
|---|---|
| With triphenyl-arsane; triethylamine; palladium diacetate In acetonitrile at 70℃; for 24h; | 57% |
| Conditions | Yield |
|---|---|
| With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine In acetonitrile at 20 - 60℃; for 1.5h; Sonogashira Cross-Coupling; Inert atmosphere; | 54% |
- 656-66-6
3-fluoro-4-iodoaniline
- 127099-85-8, 780722-26-1
N-Cyanoguanidine
| Conditions | Yield |
|---|---|
| With hydrogenchloride In water at 100℃; for 18h; Inert atmosphere; Sealed tube; | 54% |
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Chemistry
Molecular Structure of 3-Fluoro-4-iodoaniline(656-66-6):
IUPAC Name:3-fluoro-4-iodoaniline
Molecular Formula:C6H5FIN
Molecular Weight:237.013473 g/mol
Density:2.008 g/cm3
Flash Point:119.3 °C
Enthalpy of Vaporization:51.21 kJ/mol
Boiling Point:273.7 °C at 760 mmHg
Vapour Pressure:0.00564 mmHg at 25 °C
Water Solubility:228.3 mg/L at 25 °C
Synonyms of 3-Fluoro-4-iodoaniline(656-66-6):
3-FLUORO-4-IODOANILINE;3-Fluoro-4-iodobenzenamine
Categories of 3-Fluoro-4-iodoaniline(656-66-6):
Aniline;Anilines, Amides & Amines;Fluorine Compounds;Iodine Compounds