CAS No.660-68-4,Diethylamine hydrochloride Suppliers

Products Categories

Pharmaceutical (75)
Organic Chemicals (42)
Others (41)
Reagent (9)
Materials (7)
Basic Inorganic Chemicals (1)
Synthetic Flavours & Fragrances (1)

Basic Information

Molecular Structure:
CAS No.:	660-68-4
Name:	Diethylamine hydrochloride
Article Data:	96

Formula:	C₄H₁₁N^.HCl
Molecular Weight:	109.599
Synonyms:	Diethyl ammonium chloride;Di-Ethyl Amine Hydrochloride;Diethylammonium chloride;Ethanamine, N-ethyl-, hydrochloride;diethyl amine hydrochloride;N-Ethylethanamine hydrochloride;diethylazanium chloride;N-ethylethanamine;
EINECS:	211-541-9
Density:	1.0 g/mL at 20 °C
Melting Point:	227-230 °C(lit.)
Boiling Point:	57.3 °C at 760 mmHg
Flash Point:	320-330°C
Solubility:	soluble in water
Appearance:	white to off-white crystals or crystalline powder
Hazard Symbols:	Xn,Xi
Risk Codes:	10-36/37/38
Safety:	26-39-7-24/25-36
Transport Information:	UN 1993 3/PG 3
PSA:	12.03000
LogP:	1.80870

Synthetic route

: 109-89-7
diethylamine

: 660-68-4
diethyl amine hydrochloride

Conditions

Conditions	Yield
With hydroxylamine hydrochloride In ethanol for 2h; Reflux;	100%
With methanol; acetyl chloride In diethyl ether at 0℃; for 1h; Inert atmosphere;	93%

: 36288-37-6
N-hydroxy-4-methylbenzenecarboximidoyl chloride

: 109-89-7
diethylamine

A: 660-68-4
diethyl amine hydrochloride

B: 188118-36-7
N,N-Diethyl-N'-hydroxy-4-methyl-benzamidine

Conditions

Conditions	Yield
In diethyl ether for 48h; Ambient temperature;	A n/a B 99%

...Expand

: 109-89-7
diethylamine

: 1011-84-3
4-nitrobenzohydroximoyl chloride

A: 660-68-4
diethyl amine hydrochloride

B: 188118-39-0
N,N-Diethyl-N'-hydroxy-4-nitro-benzamidine

Conditions

Conditions	Yield
In diethyl ether for 48h; Ambient temperature;	A n/a B 99%

...Expand

: 2-(diethylamino)-1-(4-hydroxyphenyl)ethanone hydrochloride

A: 156-38-7
4-hydroxyphenylacetate

B: 660-68-4
diethyl amine hydrochloride

Conditions

Conditions	Yield
In aq. buffer pH=4 - 7.4; pH-value; Irradiation;	A 99% B 99%

: bis(diethylamino)-(-)-menthylphosphine(pentacarbonyl)molybdenum(0)

A: chlorodiethylamino-(-)-menthylphosphine(pentacarbonyl)molybdenum(0)

B: 660-68-4
diethyl amine hydrochloride

Conditions

Conditions	Yield
With hydrogenchloride In pentane Under stirring a strong stream of hydrogenhalogenide is bubbled for 20 min through the soln. of phosphine complex at room temp.(inert atmosphere).; Solvent is evapd. at room temp. in vac., residue is digested with pentane, dialkylamminhydrohalogenide is filtered off, filtrate is dried to dryness in vac., chromy., elem. anal.;	A 98% B n/a

: bis(diethylamino)-(-)-menthylphosphine(pentacarbonyl)tungsten(0)

A: chlorodiethylamino-(-)-menthylphosphine(pentacarbonyl)tungsten(0)

B: 660-68-4
diethyl amine hydrochloride

Conditions

Conditions	Yield
With hydrogenchloride In pentane Under stirring a strong stream of hydrogenhalogenide is bubbled for 3-10 min through the cooled (-50-0°C) soln. of phosphine complex (inert atmosphere).; Solvent is evapd. at room temp. in vac., residue is digested with pentane, dialkylamminhydrohalogenide is filtered off, filtrate is dried to dryness in vac., recrystn. from pentane (-78°C), not purely isolated.;	A 96% B n/a

Yield

With hydrogenchloride In pentane Under stirring a strong stream of hydrogenhalogenide is bubbled for 3-10 min through the cooled (-50-0°C) soln. of phosphine complex (inert atmosphere).; Solvent is evapd. at room temp. in vac., residue is digested with pentane, dialkylamminhydrohalogenide is filtered off, filtrate is dried to dryness in vac., recrystn. from pentane (-78°C), not purely isolated.;

A 96%
B n/a

: 84534-89-4
bis(diethylamino)phenylphosphine(pentacarbonyl)molybdenum(0)

A: 126289-60-9
chlorodiethylaminophenylphosphine(pentacarbonyl)molybdenum(0)

B: 660-68-4
diethyl amine hydrochloride

Conditions

Conditions	Yield
With hydrogenchloride In benzene Under stirring a strong stream of hydrogenhalogenide is bubbled for 10 min through the cooled (0°C) soln. of phosphine complex (inert atmosphere).; Solvent is evapd. at room temp. in vac., residue is digested with pentane, dialkylamminhydrohalogenide is filtered off, filtrate is dried to dryness in vac., recrystn. from pentane (-78°C), elem. anal.;	A 95% B n/a

: 126306-20-5
bis(diethylamino)phenylphosphine(pentacarbonyl)tungsten(0)

A: 126289-63-2
chlorodiethylaminophenylphosphine(pentacarbonyl)tungsten(0)

B: 660-68-4
diethyl amine hydrochloride

Conditions

Conditions	Yield
With hydrogenchloride In pentane Under stirring a strong stream of hydrogenhalogenide is bubbled for 3-10 min through the cooled (-50-0°C) soln. of phosphine complex (inert atmosphere).; Solvent is evapd. at room temp. in vac., residue is digested with pentane, dialkylamminhydrohalogenide is filtered off, filtrate is dried to dryness in vac., recrystn. from pentane (-78°C), not purely isolated.;	A 93% B n/a

Yield

A 93%
B n/a

: 31355-55-2, 39210-30-5
trichlorotris(tetrahydrofuran)molybdenum(III)

: 4648-54-8
trimethylsilylazide

: 76276-42-1
diethylammonium O,O-dimethyl phosphorodithioate

: 82621-45-2
[MoN(S2P(OCH3)2)2]4

B: 660-68-4
diethyl amine hydrochloride

Conditions

Conditions	Yield
In tetrahydrofuran byproducts: (CH3)3SiCl; (N2); mixt. of complex/(CH3)3SiN3/THF warmed at 45-50°C for 1 h,evapd., (C2H5)2NH2(S2P(OCH3)2) and THF added, stirred for 3 h; concd., filtered, filtrate treated with MeOH, concd., MeOH added, ppt. filtered, washed with MeOH, dried, recrystd. (MeOH/THF); elem. anal.;	A 61% B 93%

...Expand

: 771-99-3
4-phenylpiperidine

: 24424-99-5
di-tert-butyl dicarbonate

A: 660-68-4
diethyl amine hydrochloride

B: 123387-49-5
tert-butyl 4-phenylpiperidine-1-carboxylate

Conditions

Conditions	Yield
With diethylamine In 1,2-dichloro-ethane at 20℃;	A n/a B 90.6%

...Expand

Downstream Products

7664-41-7

75-04-7

75-00-3

Total:144 Page 1 of 4 1 2 3 4 Next>>

Post a RFQ

Cas No.:

Product Name:

Quantity:

Email:

Company name:

Valid Period:

Detailed Requirements:

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

What can I do for you?
Get Best Price

Get Best Price for 660-68-4

Chemistry

IUPAC Name:N-ethylethanamine hydrochloride
Molecular Formula:C₄H₁₁N·ClH
Molecular Weight:109.62
EINECS:211-541-9
Melting Point:227-230 °C
Boiling Point:320-330 °C
Solubility:Soluble
Density:1.0 g/mL at 20 °C
Sensitive:Hygroscopic
Appearance:Off-white solid
Diethylammonium Chloride's(660-68-4) Synonyms: Diethyl-ammonium;Ethanamine,N-ethyl-,hydrochloride;n-ethylethanaminehydrochloride;n-ethyl-ethanaminhydrochloride;TETRAMETHYLTHIONINE CHLORIDE;NEISSER'S METHYLENE BLUE;NEISSER'S SOLUTION IA;SWISS BLUE
Diethylammonium Chloride's(660-68-4) Molecular Structure:

Toxicity Data With Reference

1.	orl-rat LD50:9900 mg/kg	GISAAA Gigiena i Sanitariya. 49 (1)(1984),71.
2.	orl-mus LD50:4860 mg/kg	GTPZAB Gigiena Truda i Professionalnye Zabolevaniia. Labor Hygiene and Occupational Diseases. 31 (1)(1987),49.
3.	ipr-mus LD50:960 mg/kg	JJPAAZ Japanese Journal of Pharmacology. 17 (1967),475.
4.	scu-mus LD50:1130 mg/kg	AIPTAK Archives Internationales de Pharmacodynamie et de Therapie. 112 (1957),36.
5.	ivn-mus LD50:320 mg/kg	AIPTAK Archives Internationales de Pharmacodynamie et de Therapie. 112 (1957),36.

Consensus Reports

EPA Genetic Toxicology Program. Reported in EPA TSCA Inventory.

Safety Profile

Poison by intravenous route. Moderately toxic by subcutaneous and intraperitoneal routes. When heated to decomposition it emits toxic fumes of NO_x, NH₃, and HCl.

Safety Information of Diethylammonium Chloride(660-68-4)
Hazard Codes Xn,Xi
Risk Statements 10-36/37/38
10 Flammable
36/37/38 Irritating to eyes, respiratory system and skin
Safety Statements 26-39-7-24/25-36
RIDADR UN 1993 3/PG 3
WGK Germany 3
RTECS SP5740000
F 21
HS Code 29211200

Specification

Stability and Reactivity of Diethylammonium Chloride(660-68-4)
【Disposal Code】3
【Incompatibilities】Oxidizing agents.
【Stability】Stable under normal temperatures and pressures.
【Decomposition】Hydrogen chloride, nitrogen oxides, carbon monoxide, irritating and toxic fumes and gases, carbon dioxide, nitrogen.