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66176-39-4

Basic Information
CAS No.: 66176-39-4
Name: alpha-Bromo-p-toluenesulphonyl chloride
Article Data: 18
Molecular Structure:
Molecular Structure of 66176-39-4 (alpha-Bromo-p-toluenesulphonyl chloride)
Formula: C7H6BrClO2S
Molecular Weight: 269.546
Synonyms: p-Toluenesulfonylchloride, a-bromo- (6CI,7CI);4-(Bromomethyl)benzene-1-sulfonyl chloride;4-(Bromomethyl)benzenesulfonylchloride;4-(Bromomethyl)phenylsulfonyl chloride;a-Bromo-p-toluenesulfonyl chloride;
EINECS: -0
Density: 1.732 g/cm3
Melting Point: 69-76 oC
Boiling Point: 329.7 °C at 760 mmHg
Flash Point: 153.2 °C
Appearance: off-white to light yellow crystalline powder
Hazard Symbols: CorrosiveC
Risk Codes: 34
Safety: 26-36/37/39-45
Transport Information: UN 3261
PSA: 42.52000
LogP: 3.58980
Synthetic route
63516-03-0

α-bromo-p-toluidine

66176-39-4

4-(bromomethyl)benzene-1-sulfonyl chloride

Conditions
ConditionsYield
Stage #1: α-bromo-p-toluidine With hydrogenchloride; sodium nitrite In water at -5 - 0℃;
Stage #2: With thionyl chloride; copper(l) chloride In water at -5 - 0℃;
75.9%
34241-39-9

azobisisobutyronitrile

98-59-9

p-toluenesulfonyl chloride

A

66176-39-4

4-(bromomethyl)benzene-1-sulfonyl chloride

B

25426-48-6

4-(1-bromo-ethyl)-benzenesulfonyl chloride

Conditions
ConditionsYield
With N-Bromosuccinimide In 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran; benzeneA n/a
B 66%
34241-39-9

azobisisobutyronitrile

98-59-9

p-toluenesulfonyl chloride

66176-39-4

4-(bromomethyl)benzene-1-sulfonyl chloride

Conditions
ConditionsYield
With N-Bromosuccinimide In 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran; benzene66%
With N-Bromosuccinimide In 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran; benzene66%
98-59-9

p-toluenesulfonyl chloride

66176-39-4

4-(bromomethyl)benzene-1-sulfonyl chloride

Conditions
ConditionsYield
With N-Bromosuccinimide; dibenzoyl peroxide In tetrachloromethane at 80℃; for 10h; Inert atmosphere;65%
With N-Bromosuccinimide; trityl tetrafluoroborate In dichloromethane at 20℃; Irradiation; Inert atmosphere; chemoselective reaction;55%
With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) In benzene for 23h; Reflux;36%
1122-91-4

4-bromo-benzaldehyde

100-53-8

phenylmethanethiol

A

66176-39-4

4-(bromomethyl)benzene-1-sulfonyl chloride

B

78832-95-8

4-(benzylmercapto)benzaldehyde

66176-39-4

4-(bromomethyl)benzene-1-sulfonyl chloride

100-46-9

benzylamine

4-bromomethyl-benzenesulfonic acid benzylamide

Conditions
ConditionsYield
With triethylamine In diethyl ether at 20℃; for 3h; Substitution;100%
With triethylamine In tetrahydrofuran at 0 - 20℃; Inert atmosphere;
110-89-4

piperidine

66176-39-4

4-(bromomethyl)benzene-1-sulfonyl chloride

1-((4-(bromomethyl)phenyl)sulfonyl)piperidine

Conditions
ConditionsYield
With triethylamine In diethyl ether at 20℃; for 3h; Substitution;100%
With triethylamine In dichloromethane at 0℃; for 1.25h; Inert atmosphere;
With sodium carbonate In water at 20℃; pH=9-10;
496-15-1

1-indoline

66176-39-4

4-(bromomethyl)benzene-1-sulfonyl chloride

1-(4-bromomethyl-benzenesulfonyl)-2,3-dihydro-1H-indole

Conditions
ConditionsYield
With triethylamine In diethyl ether at 20℃; for 3h; Substitution;100%
95-14-7

1,2,3-Benzotriazole

66176-39-4

4-(bromomethyl)benzene-1-sulfonyl chloride

1-(4-bromomethyl-benzenesulfonyl)-1H-benzotriazole

Conditions
ConditionsYield
With triethylamine In diethyl ether at 20℃; for 3h; Substitution;100%
66176-39-4

4-(bromomethyl)benzene-1-sulfonyl chloride

109-89-7

diethylamine

15148-73-9

4-(bromomethyl)-N,N-diethylbenzenesulfonamide

Conditions
ConditionsYield
With triethylamine In diethyl ether at 20℃; for 3h; Substitution;100%
With N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; for 2h;
With triethylamine In dichloromethane at 0℃; for 1.25h; Inert atmosphere;
With triethylamine In dichloromethane at 0 - 20℃; for 1h;0.10 g
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  • 66176-39-4 	alpha-Bromo-p-toluenesulphonyl chloride

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