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66204-44-2

Basic Information
CAS No.: 66204-44-2
Name: 3,3'-methylenebis[5-methyloxazolidine]
Article Data: 9
Molecular Structure:
Molecular Structure of 66204-44-2 (3,3'-methylenebis[5-methyloxazolidine])
Formula: C9H18N2O2
Molecular Weight: 186.254
Synonyms: N,N'-methylene-bis(5-methyloxazolidine);5,5'-dimethyl-3,3'-methanediyl-bis-oxazolidine;3,3'-Methylenebis(5-methyloxazolidine);3,3'-methylenebis-[5-methyloxazoldiine];EINECS 266-235-8;5,5'-dimethyl-di-(1,3-oxazolidin-3-yl) methane;Grotan OX;bis[5-methyl-1,3-oxazolidin-3-yl]methane;
Density: 1.062g/cm3
Boiling Point: 247.6°Cat760mmHg
Flash Point: 70.1°C
PSA: 24.94000
LogP: 0.17610
Synthetic route
50-00-0

formaldehyd

78-96-6, 1674-56-2

3-amino-2-propanol

A

66204-44-2

3,3'-methylenebis-[5-methyloxazoldiine]

B

6,9-dimethyl-3,8-dioxa-1,6-diazabicyclo[4.4.1]undecane

Conditions
ConditionsYield
In tetrahydrofuran at -78℃; for 4h;A 72%
B n/a
In benzene for 6h; Dean-Stark; Reflux; Overall yield = 53 %; Overall yield = 4.9 g;
6168-72-5

2-Amino-1-propanol

paraformaldehyde

paraformaldehyde

66204-44-2

3,3'-methylenebis-[5-methyloxazoldiine]

Conditions
ConditionsYield
Stage #1: 2-Amino-1-propanol; paraformaldehyde Cooling with water-bath; 1/3 part of formaldehyde was added;
Stage #2: paraformaldehyde at 65℃; Second 1/3 part of formaldehyde was added;
Stage #3: paraformaldehyde at 140℃; third part of formaldehyde was added at 65 °ree;C; Heating up to 95 °ree;C until disoslution of formaldehyde; Heating / reflux;
50-00-0

formaldehyd

78-96-6, 1674-56-2

3-amino-2-propanol

66204-44-2

3,3'-methylenebis-[5-methyloxazoldiine]

Conditions
ConditionsYield
In toluene Dean-Stark; Reflux;
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