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CAS No.: | 676-58-4 |
---|---|
Name: | Methylmagnesium chloride |
Article Data: | 10 |
Molecular Structure: | |
Formula: | CH3 Cl Mg |
Molecular Weight: | 74.7928 |
Synonyms: | Methylmagnesiumchloride (6CI);Chloromethylmagnesium; |
EINECS: | 211-629-7 |
Density: | 1.013 g/mL at 25 °C |
Boiling Point: | 66 °C |
Flash Point: | ?1 °F |
Solubility: | reacts with water |
Appearance: | dark brown solution |
Hazard Symbols: | F,C |
Risk Codes: | 11-14/15-34-19-15 |
Safety: | 26-30-36/37/39-43-45-7/8-33-29-16 |
Transport Information: | UN 3399 4.3/PG 2 |
PSA: | 0.00000 |
LogP: | 1.27330 |
Conditions | Yield |
---|---|
With magnesium In tetrahydrofuran | |
With magnesium In solid matrix at -258.2℃; | |
With magnesium; lithium chloride In tetrahydrofuran at 0 - 20℃; Inert atmosphere; |
Conditions | Yield |
---|---|
With diethyl ether |
Conditions | Yield |
---|---|
In diethyl ether at 0 - 20℃; | 100% |
8-bromo-2-tetralone
methylmagnesium chloride
8-bromo-2-hydroxy-2-methyl-1,2,3,4-tetrahydronaphthalene
Conditions | Yield |
---|---|
With titanium tetrachloride In tetrahydrofuran; dichloromethane at 0℃; for 2h; | 100% |
methylmagnesium chloride
methyl 6-<2-(7-acetamidoheptyl)-1,3-dioxolan-2-yl>hexanoate
N-<7-<2-(6-hydroxy-6-methylheptyl)-1,3-dioxolan-2-yl>heptyl>acetamide
Conditions | Yield |
---|---|
In tetrahydrofuran for 12h; | 100% |
methylmagnesium chloride
dimethyl (RS)-6,6'-dibromobiphenyl-2,2'-dicarboxylate
6,6'-dibromobiphenyl-2,2'-di(1-methylethanol)
Conditions | Yield |
---|---|
In tetrahydrofuran for 3h; Heating; | 100% |
methylmagnesium chloride
Conditions | Yield |
---|---|
In tetrahydrofuran | 100% |
methylmagnesium chloride
3-(6',6'-dimethyl-2'-methylenecyclohexyl)propan-1-al
4-(6',6'-dimethyl-2'-methylenecyclohexyl)butan-2-ol
Conditions | Yield |
---|---|
100% |
methylmagnesium chloride
C6H4(CH2CH2C(O)O)
4-(2-hydroxyphenyl)-2-methyl-2-butanol
Conditions | Yield |
---|---|
In tetrahydrofuran at 0 - 20℃; | 100% |
In tetrahydrofuran Ambient temperature; | 6.25 g |
In tetrahydrofuran; (2S)-N-methyl-1-phenylpropan-2-amine hydrate; water | |
Stage #1: methylmagnesium chloride; C6H4(CH2CH2C(O)O) In tetrahydrofuran for 18.6667h; Stage #2: With water In tetrahydrofuran Cooling; |
methylmagnesium chloride
Conditions | Yield |
---|---|
In tetrahydrofuran at -20 - 20℃; | 100% |
at -20℃; for 0.0833333h; pH=13; Grignard reaction; |
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Molecular Structure:
Molecular Formula: CH3ClMg
Molecular Weight: 74.7925
IUPAC Name: Magnesium carbanide chloride
Synonyms of Methylmagnesium chloride (CAS NO.676-58-4): Chloromethylmagnesium ; EINECS 211-629-7 ; HSDB 5740 ; Magnesium, chloromethyl-
CAS NO: 676-58-4
Classification Code: Organometallics ; GRIGNARD REAGENTS ; AlkylChemical Synthesis ; Grignard Reagents ; Organic Bases ; Organometallic Reagents ; Synthetic Reagents
Hazard Codes of Methylmagnesium chloride (CAS NO.676-58-4): F,C
Risk Statements: 11-14/15-34-19
R11: Highly flammable.
R14: Reacts violently with water.
R15: Contact with water liberates extremely flammable gases.
R34: Causes burns.
R19: May form explosive peroxides.
Safety Statements: 26-30-36/37/39-43-45-7/8-33-29-16
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
S30: Never add water to this product.
S36/37/39: Wear suitable protective clothing, gloves and eye/face protection.
S43: In case of fire use ... (there follows the type of fire-fighting equipment to be used.)
S45: In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.)
S7: Keep container tightly closed.
S8: Keep container dry.
S33: Take precautionary measures against static discharges.
S29: Do not empty into drains.
S16: Keep away from sources of ignition.
RIDADR :UN 3399 4.3/PG 2
WGK Germany: 1
F: 1-3-10
HazardClass: 4.3
PackingGroup: I