Products Categories
| CAS No.: | 68733-20-0 |
|---|---|
| Name: | 1,3,4,6-TETRA-O-ACETYL-2-AZIDO-2-DEOXY-ALPHA-D-MANNOPYRANOSE |
| Article Data: | 14 |
| Molecular Structure: | |
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| Formula: | C14H19 N3 O9 |
| Molecular Weight: | 373.32 |
| Synonyms: | [(2R,3S,4R,5S,6R)-3,4,6-triacetyloxy-5-azidooxan-2-yl]methyl acetate; |
| Melting Point: | 132 °C |
| PSA: | 164.18000 |
| LogP: | -0.16744 |
- 81281-59-67-Benzylideneaminotheophylline
- 82993-81-5D-threo-Ritalinic acid hydrochloride
- 73441-42-6METHYL-5-CHLORO-2,2-DIMETHYLVALERATE
- 852475-26-4MC1568
- 958254-66-51H-Imidazo[4,5-b]pyridine-2-carboxaldehyde, 1-methyl-, hydrochloride
- 99170-93-1N-Methyl-2-oxazolamine
- 717878-06-31-(4-fluorophenyl)-4-nitro-1H-imidazole
- 914458-26-7[5-(2-fluorophenyl)-1-pentyl-1H-pyrrol-3-yl]-1-naphthalenyl-Methanone
- 894852-01-87-BROMO-2,2-DIMETHYL-2H-PYRIDO[3,2-B][1,4]OXAZIN-3(4H)-ONE
- 71825-51-92-methyl-2-(4-nitrophenyl)propanenitrile
- 108-24-7
acetic anhydride
- 115945-97-6
methyl 3-O-acetyl-2-azido-4,6-O-benzylidene-2-deoxy-α-D-mannopyranoside
- 68733-20-0
1,3,4,6-tetra-O-acetyl-2-azido-2-deoxy-α-D-mannopyranoside
| Conditions | Yield |
|---|---|
| With sulfuric acid at 0℃; for 1h; | 92% |
- 108-24-7
acetic anhydride
- 68733-20-0
1,3,4,6-tetra-O-acetyl-2-azido-2-deoxy-α-D-mannopyranoside
| Conditions | Yield |
|---|---|
| With sulfuric acid at 20℃; for 2h; | 82% |
- 108-24-7
acetic anhydride
- 116003-78-2
Methyl 2-azido-2-deoxy-4,6-O-(phenylmethylene)-α-D-mannopyranoside
- 68733-20-0
1,3,4,6-tetra-O-acetyl-2-azido-2-deoxy-α-D-mannopyranoside
| Conditions | Yield |
|---|---|
| With sulfuric acid at 20℃; for 2.5h; | 78% |
| With sulfuric acid at 20℃; for 0.666667h; | 75% |
- 1600-27-7
mercury(II) diacetate
- 2873-29-2
D-glucal triacetate
A
- 56883-33-1
2-azido-2-deoxy-3,4,6-tri-O-acetyl-α-D-glucopyranosyl acetate
B
- 80321-89-7
1,3,4,6-Tetra-O-acetyl-2-azido-2-deoxy-β-D-glucopyranose
D
- 68733-20-0
1,3,4,6-tetra-O-acetyl-2-azido-2-deoxy-α-D-mannopyranoside
| Conditions | Yield |
|---|---|
| With chlorine azide In tetrachloromethane at 0℃; for 1h; Product distribution; Irradiation; other halogen-azide, in other solvents under irradiation or in the dark, various time and temperature; | A 9% B 62% C 8% D 11% |
| With chlorine azide 1.) CCl4, irrad., 0 deg C, 1 h; 2.) glacial acetic acid, room temp.; Yield given. Multistep reaction; | A n/a B 62% C 8% D 11% |
| With chlorine azide 1.) CCl4, irrad., 0 deg C, 1 h; 2.) glacial acetic acid, room temp.; Yield given. Multistep reaction; | A 9% B 62% C 8% D n/a |
| With chlorine azide 1.) CCl4, irrad., 0 deg C, 1 h, 2.) glacial acetic acid, room temp.; Yield given. Multistep reaction; | A 9% B n/a C 8% D 11% |
- 113544-40-4
1,3,4,6-tetra-O-acetyl-2-O-trifluoromethanesulfonyl-α-D-glucopyranose
- 68733-20-0
1,3,4,6-tetra-O-acetyl-2-azido-2-deoxy-α-D-mannopyranoside
| Conditions | Yield |
|---|---|
| With sodium azide In N,N-dimethyl-formamide at 60℃; for 0.5h; | 58% |
| With sodium azide In N,N-dimethyl-formamide | 20% |
| With sodium azide In N,N-dimethyl-formamide at 60℃; for 5h; | 10% |
- 127-09-3
sodium acetate
- 668481-16-1
Acetic acid (2R,3S,4R)-4-acetoxy-2-acetoxymethyl-5-azido-6-nitrooxy-tetrahydro-pyran-3-yl ester
A
- 56883-33-1
2-azido-2-deoxy-3,4,6-tri-O-acetyl-α-D-glucopyranosyl acetate
B
- 80321-89-7
1,3,4,6-Tetra-O-acetyl-2-azido-2-deoxy-β-D-glucopyranose
C
- 68733-20-0
1,3,4,6-tetra-O-acetyl-2-azido-2-deoxy-α-D-mannopyranoside
| Conditions | Yield |
|---|---|
| In acetic acid at 100℃; for 1h; | A n/a B n/a C 17% |
- 127-09-3
sodium acetate
- 2873-29-2
D-glucal triacetate
A
- 56883-33-1
2-azido-2-deoxy-3,4,6-tri-O-acetyl-α-D-glucopyranosyl acetate
B
- 68733-20-0
1,3,4,6-tetra-O-acetyl-2-azido-2-deoxy-α-D-mannopyranoside
| Conditions | Yield |
|---|---|
| With sodium azide; ammonium cerium(IV) nitrate 1.) EtOAc, CH3CN, -40 deg C, 6 d; 2.) glacial acetic acid, 100 deg C, 1 h; Yield given. Multistep reaction. Yields of byproduct given; |
- 127-09-3
sodium acetate
- 2873-29-2
D-glucal triacetate
- 68733-20-0
1,3,4,6-tetra-O-acetyl-2-azido-2-deoxy-α-D-mannopyranoside
| Conditions | Yield |
|---|---|
| With sodium azide; ammonium cerium(IV) nitrate 1.) acetonitrile, ethylacetate, -40 deg C; Yield given. Multistep reaction; |
- 4692-12-0
1,3,4,6-tetra-O-acetyl glucopyranose
- 68733-20-0
1,3,4,6-tetra-O-acetyl-2-azido-2-deoxy-α-D-mannopyranoside
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: 97 percent / pyridine / CH2Cl2 / 1 h / -20 °C 2: 58 percent / NaN3 / dimethylformamide / 0.5 h / 60 °C View Scheme | |
| Multi-step reaction with 2 steps 1: 66 percent / pyridine; CH2Cl2 / 1.5 h / 3 °C 2: 10 percent / NaN3 / dimethylformamide / 5 h / 60 °C View Scheme |
- 3162-96-7
methyl 4,6-O-benzylidene-α-D-glucopyranoside
- 68733-20-0
1,3,4,6-tetra-O-acetyl-2-azido-2-deoxy-α-D-mannopyranoside
| Conditions | Yield |
|---|---|
| Multi-step reaction with 3 steps 1: pyridine / dichloromethane / 3 h / -78 - 20 °C 2: sodium azide / N,N-dimethyl-formamide / 2 h / 80 °C 3: sulfuric acid / 2 h / 20 °C View Scheme |
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