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Basic Information
CAS No.: 7098-80-8
Name: (2,2-dimethyl-1,3-dioxolan-4-yl)methyl methacrylate
Article Data: 9
Molecular Structure:
Molecular Structure of 7098-80-8 ((2,2-dimethyl-1,3-dioxolan-4-yl)methyl methacrylate)
Formula: C10H16O4
Molecular Weight: 200.235
Synonyms: 96614-23-2;
EINECS: 230-408-6
Density: 1.028
Boiling Point: 275℃
Flash Point: 116℃
PSA: 44.76000
LogP: 1.25720
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Conditions
ConditionsYield
With titanium(IV) isopropylate; 1,4-phenylenediamine In cyclohexane for 15h; Heating;67%
With methanol; sodium methylate; 1,1'-bi-2-naphthol
With titanium(IV) isopropylate transesterification;
Industry scale;
With dibutyltin dilaurate; hydroquinone at 110℃; for 8h;
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2-methyl-acrylic acid 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

Conditions
ConditionsYield
With triethylamine In tetrahydrofuran at 20℃; for 48h;64%
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(R,S)-2,2-dimethyl-1,3-dioxolane-4-methanol

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2-methyl-acrylic acid 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

Conditions
ConditionsYield
With sodium carbonate64%
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2-methyl-acrylic acid 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

Conditions
ConditionsYield
With phosphoric acid at 60℃; Product distribution; Further Variations:; Catalysts; Cyclization;
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Conditions
ConditionsYield
With acetic acid; 4-methoxy-phenol at 80℃; for 0.166667h;80%
Hydrolysis; Acid hydrolysis;
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2-bromo-2-methyl propionic acid 2-(3,5-dioxo-10-oxa-4-azatricyclo[5.2.1.02,6]dec-8-en-4-yl)ethyl ester

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2-methyl-acrylic acid 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

polymer, Mn=34500, Mw/Mn=1.15; monomer(s): glycerol-1-(methacrylate)-2,3-acetonide; 2-bromo-2-methylpropionic acid 2-(3,5-dioxo-10-oxa-4-azatricyclo[5.2.1.02,6]dec-8-en-4-yl)ethyl ester

polymer, Mn=34500, Mw/Mn=1.15; monomer(s): glycerol-1-(methacrylate)-2,3-acetonide; 2-bromo-2-methylpropionic acid 2-(3,5-dioxo-10-oxa-4-azatricyclo[5.2.1.02,6]dec-8-en-4-yl)ethyl ester

Conditions
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With N-propyl 2-pyridylmethanimine; copper(I) bromide In toluene at 40℃;

2-bromo-2-methyl propionic acid 2-(3,5-dioxo-10-oxa-4-azatricyclo[5.2.1.02,6]dec-8-en-4-yl)ethyl ester

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2-methyl-acrylic acid 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

polymer, Mn=6600, Mw/Mn=1.28; monomer(s): glycerol-1-(methacrylate)-2,3-acetonide; 2-bromo-2-methylpropionic acid 2-(3,5-dioxo-10-oxa-4-azatricyclo[5.2.1.02,6]dec-8-en-4-yl)ethyl ester

polymer, Mn=6600, Mw/Mn=1.28; monomer(s): glycerol-1-(methacrylate)-2,3-acetonide; 2-bromo-2-methylpropionic acid 2-(3,5-dioxo-10-oxa-4-azatricyclo[5.2.1.02,6]dec-8-en-4-yl)ethyl ester

Conditions
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With N-propyl 2-pyridylmethanimine; copper(I) bromide In toluene at 40℃;
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2-methyl-acrylic acid 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

polymer, Mn = 11.5 kDa, PDi = 1.15

polymer, Mn = 11.5 kDa, PDi = 1.15

Conditions
ConditionsYield
Stage #1: hostasol methacrylate; 2-bromo-2-methyl-propionic acid 2-(3,5-dioxo-10-oxa-4-azatricyclo[5.2.1.02,6]dec-8-en-4-yl)-ethyl ester; 2-methyl-acrylic acid 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester With N-propyl 2-pyridylmethanimine; copper(I) bromide In methoxybenzene at 20℃;
Stage #2: 2-methyl-acrylic acid 3-trimethylsilanyl-propyn-2-ynyl ester With N-propyl 2-pyridylmethanimine; copper(I) bromide In methoxybenzene at 20℃; Further stages.;
...Expand
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2-methyl-acrylic acid 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

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Conditions
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With N-propyl 2-pyridylmethanimine; copper(I) bromide In methoxybenzene at 20℃;
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