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CAS No.: | 7128-82-7 |
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Name: | 1,5-PENTANEETHONIUM DIBROMIDE |
Article Data: | 9 |
Molecular Structure: | |
Formula: | C17H40 N2 . 2 Br |
Molecular Weight: | 432.326 |
Synonyms: | 1,5-Pentanediaminium,N,N,N,N',N',N'-hexaethyl-, dibromide (9CI); Ammonium, pentamethylenebis[triethyl-,dibromide (8CI); Pentamethylenebis[triethylammonium bromide] (7CI);1,5-Bis(triethylammonium)pentane dibromide; DB 2 |
Melting Point: | 276-278 °C (decomp) |
PSA: | 0.00000 |
LogP: | 0.91370 |
1,5-dibromo-pentane
triethylamine
N1,N1,N1,N5,N5,N5-hexaethylpentane-1,5-diamonium dibromide
Conditions | Yield |
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In acetone for 24h; Reflux; | 90% |
In neat (no solvent) at 110℃; for 24h; Autoclave; | 64% |
With ethanol | |
In methanol at 65℃; for 72h; |
(5-bromopentyl)triethylammonium bromide
triethylamine
N1,N1,N1,N5,N5,N5-hexaethylpentane-1,5-diamonium dibromide
Conditions | Yield |
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In propan-1-ol Heating; | 72% |
Conditions | Yield |
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Multi-step reaction with 2 steps 1: 21 percent / hexane / 10 h / Heating 2: 72 percent / propan-1-ol / Heating View Scheme |
Conditions | Yield |
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Multi-step reaction with 2 steps 1: 21 percent / hexane / 10 h / Heating 2: 72 percent / propan-1-ol / Heating View Scheme |
1,5-dibromo-pentane
ethanol
N1,N1,N1,N5,N5,N5-hexaethylpentane-1,5-diamonium dibromide
Conditions | Yield |
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With triethylamine Heating / reflux; |
Conditions | Yield |
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With silica gel In water colloidal silica and Et3N(CH2)5NEt3Br2 added to aq. soln. of Al(NO3)3*9H2O and NaOH; stirred (room temp., 1 day); heated (160°C, 8 days,autoclave, rotation 60 rpm); filtered off; washed repeatedly (water); dried overnight (room temp.); elem. anal.; thermal anal.; |
N1,N1,N1,N5,N5,N5-hexaethylpentane-1,5-diamonium dibromide
Conditions | Yield |
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With silica gel In water colloidal silica and Et3N(CH2)5NEt3Br2 added to aq. soln. of Al(NO3)3*9H2O and KOH; stirred (room temp., 1 day); heated (160°C, 8 days, autoclave, rotation 60 rpm); filtered off; washed repeatedly (water); dried overnight (room temp.); elem. anal.; thermal anal.; |
N1,N1,N1,N5,N5,N5-hexaethylpentane-1,5-diamonium dibromide
Conditions | Yield |
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With anion exchange resin DIAION |
N1,N1,N1,N5,N5,N5-hexaethylpentane-1,5-diamonium dibromide
Conditions | Yield |
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With ammonium hexafluorophosphate In water for 4h; |