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719-59-5

Basic Information
CAS No.: 719-59-5
Name: 2-Amino-5-chlorobenzophenone
Article Data: 107
Molecular Structure:
Molecular Structure of 719-59-5 (2-Amino-5-chlorobenzophenone)
Formula: C13H10ClNO
Molecular Weight: 231.681
Synonyms: (2-amino-5-chlorophenyl)(phenyl)methanone;Aminoketone;Benzophenone, 2-amino-5-chloro- (8CI);5-Chloro-2-aminobenzophenone;Benzophenone, 2-amino-5-chloro-;(2-amino-5-chloro-phenyl)-phenyl-methanone;(2-Amino-5-chlorophenyl)phenylmethanone;Methanone, (2-amino-5-chlorophenyl)phenyl-;2-Benzoyl-4-chloroaniline;2-Amino-5-chlorobenzylphenone;
EINECS: 211-949-7
Density: 1.274 g/cm3
Melting Point: 96-98 °C(lit.)
Boiling Point: 424.3 °C at 760 mmHg
Flash Point: 210.4 °C
Solubility: insoluble
Appearance: yellow powder
Hazard Symbols: HarmfulXn, IrritantXi
Risk Codes: 36/37/38-22-20/21/22
Safety: 26-36
PSA: 43.09000
LogP: 3.73440
Synthetic route
719-64-2

5-chloro-3-phenylanthranil

719-59-5

2-Amino-5-chlorobenzophenone

Conditions
ConditionsYield
With trimethylsilyl iodide; water In acetonitrile at 20℃; for 0.2h;98%
Stage #1: 5-chloro-3-phenylanthranil With iron In ethanol for 0.5h; Reflux;
Stage #2: With sulfuric acid In ethanol for 1h; Reflux;
95.1%
With aluminium trichloride; zinc In tetrahydrofuran for 6h; Ambient temperature;92%
5922-60-1

2-amino-5-chlorobenzonitrile

98-80-6

phenylboronic acid

719-59-5

2-Amino-5-chlorobenzophenone

Conditions
ConditionsYield
With 5,5'-dimethyl-2,2'-bipyridine; methanesulfonic acid; palladium(II) trifluoroacetate; water In 2-methyltetrahydrofuran at 80℃; for 36h; Schlenk technique;96%
With [2,2]bipyridinyl; methanesulfonic acid; palladium(II) trifluoroacetate In tetrahydrofuran; water at 80℃; for 36h;

2-Amino-5-chlorobenzophenone N,N-dimethylhydrazone

719-59-5

2-Amino-5-chlorobenzophenone

Conditions
ConditionsYield
With triethylene diamine nickel thiosulfate; water In chloroform at 20℃; for 0.166667h; Hydrolysis;92%
5922-60-1

2-amino-5-chlorobenzonitrile

873-55-2

sodium benzenesulfonate

719-59-5

2-Amino-5-chlorobenzophenone

Conditions
ConditionsYield
With p-nitrobenzenesulfonic acid; palladium diacetate In tetrahydrofuran; water at 80℃; for 48h; Inert atmosphere; Schlenk technique;92%
55-21-0

benzamide

106-47-8

4-chloro-aniline

719-59-5

2-Amino-5-chlorobenzophenone

Conditions
ConditionsYield
Stage #1: benzamide; 4-chloro-aniline With tin(ll) chloride at 123 - 250℃; for 4h;
Stage #2: With potassium chloride at 95 - 130℃; for 4h;
Stage #3: With phosphoric acid for 23h; Concentration; Temperature; Reflux;
91%
105448-12-2

7-Chlor-2-methylthio-5-phenyl-3H-1,3,4-benzotriazepin

A

74-93-1

methylthiol

B

719-59-5

2-Amino-5-chlorobenzophenone

Conditions
ConditionsYield
With hydrogenchloride for 10h;A n/a
B 83.4%
106-47-8

4-chloro-aniline

100-47-0

benzonitrile

719-59-5

2-Amino-5-chlorobenzophenone

Conditions
ConditionsYield
With gallium(III) trichloride; boron trichloride In chlorobenzene at 100℃; for 20h;81%
With gallium(III) trichloride; boron trichloride 1.) CH2Cl2, 1,1,2,2-tetrachloroethane, 0 deg C, 2.) 1,1,2,2-tetrachloroethane, 100 deg C, 5 h; Yield given. Multistep reaction;
719-64-2

5-chloro-3-phenylanthranil

98-80-6

phenylboronic acid

A

719-59-5

2-Amino-5-chlorobenzophenone

B

108694-41-3

(5-chloro-2-(phenylamino)phenyl)(phenyl)methanone

Conditions
ConditionsYield
With potassium carbonate; copper dichloride In dimethyl sulfoxide at 100℃; for 6h; Reagent/catalyst; Solvent; Sealed tube;A 17%
B 81%
106-47-8

4-chloro-aniline

98-88-4

benzoyl chloride

719-59-5

2-Amino-5-chlorobenzophenone

Conditions
ConditionsYield
With antimony(III) oxide In dichloromethane at 15℃; for 2h; Temperature;78%
Stage #1: 4-chloro-aniline; benzoyl chloride With antimony(III) trioxide In dichloromethane at 15℃; for 2h; Friedel-Crafts Acylation;
Stage #2: With nitric acid In dichloromethane at 10 - 45℃; for 11.5h; Temperature;
77%
With dysprosium((III) oxide In tetrachloromethane at 15℃; for 2h; Temperature;76%
86230-82-2

7-chloro-9-phenyl-1,2-dihydrooxazolo<2,3-b>-1,3,4-benzotriazepine

719-59-5

2-Amino-5-chlorobenzophenone

Conditions
ConditionsYield
With sulfuric acid In ethanol at 40℃; for 1.16667h;75%
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    Product Name: 2-Amino-5-chlorobenzophenone Alias: (2-amino-5-chlorophenyl)phenyl-methanon;2-Amino-5-chlorbenzophenon;2-Amino-5-chlorbenzophenone;2-Amino-5-chlorodiphenylone;2-Benzoyl-4-chloroaniline;Methanone, (2-amino-5-chlorophenyl)phenyl-;(2-AMIN

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Chemistry

IUPAC Name: (2-amino-5-chlorophenyl)-phenylmethanone 
Empirical Formula: C13H10ClNO
Molecular Weight: 231.6776g/mol
EINECS: 211-949-7 
Structure of 2-Amino-5-chlorobenzophenone (CAS NO.719-59-5):

Index of Refraction: 1.636
Molar Refractivity: 65.17 cm3
Molar Volume: 181.7 cm3
Polarizability: 25.83×10-24cm3
Surface Tension: 52.2 dyne/cm
Density: 1.274 g/cm3
Flash Point: 210.4 °C
Enthalpy of Vaporization: 67.87 kJ/mol 
Melting Point: 96-98 °C(lit.)
Boiling Point: 424.3 °C at 760 mmHg
Vapour Pressure: 2.09E-07 mmHg at 25°C 
Stability: Stable. Incompatible with strong oxidizing agents. 
Product Categories: Benzene derivatives;FINE Chemical & INTERMEDIATES;Aromatic Benzophenones & Derivatives (substituted);ketone;Diazepam 
Canonical SMILES: C1=CC=C(C=C1)C(=O)C2=C(C=CC(=C2)Cl)N
InChI: InChI=1S/C13H10ClNO/c14-10-6-7-12(15)11(8-10)13(16)9-4-2-1-3-5-9/h1-8H,15H2
InChIKey: ZUWXHHBROGLWNH-UHFFFAOYSA-N

Toxicity Data With Reference

1.    

ipr-mus LD50:681 mg/kg

    IJSIDW    Indian Journal of Pharmaceutical Sciences. (Indian Journal of Pharmaceutical Sciences, Kalina, Santa Cruz 44 (1982),1.

Consensus Reports

Reported in EPA TSCA Inventory.

Safety Profile

Moderately toxic by intraperitoneal route. When heated to decomposition it emits toxic vapors of NOx and Cl.
Hazard Codes:  Xi,Xn
The Risk Statements information of  2-AMINO-5-CHLOROBENZOPHENONE :
22:  Harmful if swallowed 
20/21/22:  Harmful by inhalation, in contact with skin and if swallowed
36/37/38:  Irritating to eyes, respiratory system and skin
The Safety Statements information of  2-AMINO-5-CHLOROBENZOPHENONE :
26:  In case of contact with eyes, rinse immediately with plenty of water and seek medical advice 
36:  Wear suitable protective clothing 
WGK Germany: 3
RTECS: PC4933500
HS Code: 29223900

Specification

  2-Amino-5-chlorobenzophenone , its cas register number is 719-59-5. It also can be called (2-Amino-5-chlorophenyl)phenylmethanone ; 2-Benzoyl-4-chloroaniline ; 3-14-00-00214 (Beilstein Handbook Reference) ; 5-Chloro-2-aminobenzophenone . 2-Amino-5-chlorobenzophenone (CAS NO.719-59-5) is a yellow powder.