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72320-38-8

Basic Information
CAS No.: 72320-38-8
Name: 1-Propanol, 3-azido-
Article Data: 130
Molecular Structure:
Molecular Structure of 72320-38-8 (1-Propanol, 3-azido-)
Formula: C3H7N3O
Molecular Weight: 101.108
Synonyms: 3-azido-1-propanol;1-azidopropan-3-ol;3-azidopropanol;1-Propanol,3-azido;3-azido-propan-1-ol;1,3-azidopropanol;
Density: 1.095 g/mL at 25 °C
Boiling Point: 64 °C(Press: 2 Torr)
Flash Point: 87℃
PSA: 69.98000
LogP: 0.13186
Synthetic route
627-18-9

1-bromo-3-propanol

72320-38-8

3-azidopropan-1-ol

Conditions
ConditionsYield
With sodium azide In water at 60℃;99%
With sodium azide In water at 80℃; for 72h; Inert atmosphere; Schlenk technique;98%
With sodium azide In N,N-dimethyl-formamide at 90℃;97%
627-30-5

1-chloro-3-hydroxypropane

72320-38-8

3-azidopropan-1-ol

Conditions
ConditionsYield
With sodium azide In N,N-dimethyl-formamide at 60℃; for 24h; Substitution;99%
With sodium azide In water for 16h; Reflux;99%
With sodium azide In water at 80℃; for 15h;99%
24590-50-9

3-hydroxypropyl methanesulfonate

72320-38-8

3-azidopropan-1-ol

Conditions
ConditionsYield
With sodium azide In N,N-dimethyl-formamide at 80℃; for 8h;70%
107-02-8

acrolein

72320-38-8

3-azidopropan-1-ol

Conditions
ConditionsYield
With sodium tetrahydroborate; sodium azide 1.) H2O, AcOH, 5 deg C, 1 h, 2.) Et2O, H2O, 20 deg C, 45 min; Yield given. Multistep reaction;
1056188-13-6

2-(3-azidopropoxy)tetrahydro-2H-pyran

72320-38-8

3-azidopropan-1-ol

Conditions
ConditionsYield
With Amberlyst H-15 In methanol at 45℃; for 3h; Hydrolysis;
60-29-7

diethyl ether

627-30-5

1-chloro-3-hydroxypropane

72320-38-8

3-azidopropan-1-ol

Conditions
ConditionsYield
In water; N,N-dimethyl-formamide8.7 g (71.4%)

1-azido-3-t-butylsiloxypropane

72320-38-8

3-azidopropan-1-ol

Conditions
ConditionsYield
With tetrabutyl ammonium fluoride In tetrahydrofuran
H2 O-EtOH

H2 O-EtOH

627-30-5

1-chloro-3-hydroxypropane

72320-38-8

3-azidopropan-1-ol

Conditions
ConditionsYield
With sodium hydroxide; sodium iodide98.6 g (92%)
58503-60-9

3-azidopropanal

72320-38-8

3-azidopropan-1-ol

Conditions
ConditionsYield
With sodium tetrahydroborate In water at 20℃; for 0.75h;
107-07-3

2-chloro-ethanol

72320-38-8

3-azidopropan-1-ol

Conditions
ConditionsYield
With sodium azide In water for 22h; Reflux;
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