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CAS No.: | 72320-38-8 |
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Name: | 1-Propanol, 3-azido- |
Article Data: | 130 |
Molecular Structure: | |
Formula: | C3H7N3O |
Molecular Weight: | 101.108 |
Synonyms: | 3-azido-1-propanol;1-azidopropan-3-ol;3-azidopropanol;1-Propanol,3-azido;3-azido-propan-1-ol;1,3-azidopropanol; |
Density: | 1.095 g/mL at 25 °C |
Boiling Point: | 64 °C(Press: 2 Torr) |
Flash Point: | 87℃ |
PSA: | 69.98000 |
LogP: | 0.13186 |
1-bromo-3-propanol
3-azidopropan-1-ol
Conditions | Yield |
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With sodium azide In water at 60℃; | 99% |
With sodium azide In water at 80℃; for 72h; Inert atmosphere; Schlenk technique; | 98% |
With sodium azide In N,N-dimethyl-formamide at 90℃; | 97% |
1-chloro-3-hydroxypropane
3-azidopropan-1-ol
Conditions | Yield |
---|---|
With sodium azide In N,N-dimethyl-formamide at 60℃; for 24h; Substitution; | 99% |
With sodium azide In water for 16h; Reflux; | 99% |
With sodium azide In water at 80℃; for 15h; | 99% |
3-hydroxypropyl methanesulfonate
3-azidopropan-1-ol
Conditions | Yield |
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With sodium azide In N,N-dimethyl-formamide at 80℃; for 8h; | 70% |
acrolein
3-azidopropan-1-ol
Conditions | Yield |
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With sodium tetrahydroborate; sodium azide 1.) H2O, AcOH, 5 deg C, 1 h, 2.) Et2O, H2O, 20 deg C, 45 min; Yield given. Multistep reaction; |
2-(3-azidopropoxy)tetrahydro-2H-pyran
3-azidopropan-1-ol
Conditions | Yield |
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With Amberlyst H-15 In methanol at 45℃; for 3h; Hydrolysis; |
Conditions | Yield |
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In water; N,N-dimethyl-formamide | 8.7 g (71.4%) |
3-azidopropan-1-ol
Conditions | Yield |
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With tetrabutyl ammonium fluoride In tetrahydrofuran |
Conditions | Yield |
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With sodium hydroxide; sodium iodide | 98.6 g (92%) |
3-azidopropanal
3-azidopropan-1-ol
Conditions | Yield |
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With sodium tetrahydroborate In water at 20℃; for 0.75h; |
2-chloro-ethanol
3-azidopropan-1-ol
Conditions | Yield |
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With sodium azide In water for 22h; Reflux; |