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728039-63-2

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Basic Information
CAS No.: 728039-63-2
Name: Bisbiphenyl-4-yl-(4'-broMo-biphenyl-4-yl)-aMine
Article Data: 37
Molecular Structure:
Molecular Structure of 728039-63-2 (Bisbiphenyl-4-yl-(4'-broMo-biphenyl-4-yl)-aMine)
Formula: C36H26BrN
Molecular Weight: 552.513
Synonyms: N-[1.1'-biphenyl]-4-yl-N-(4'-bromo-[1.1'-biphenyl-4yl)-[1.1'-biphenyl]-4-anine
Density: 1.277±0.06 g/cm3 (20 oC 760 Torr)
Melting Point: 225.0 to 229.0 °C
Boiling Point: 703.3±60.0 °C(Predicted)
PSA: 3.24000
LogP: 10.91990
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Synthetic route
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4-bromo-4'-iodobiphenyl

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bis(biphenyl-4-yl)amine

728039-63-2

N-[1,1'-biphenyl]-4-yl-N-(4'-bromo[1,1'-biphenyl]-4-yl)-[1,1'-biphenyl]-4-amine

Conditions
ConditionsYield
With tri-tert-butyl phosphine; palladium diacetate; sodium t-butanolate In toluene for 2h; Reflux;90%
With palladium diacetate; triphenylphosphine; sodium t-butanolate In toluene at 80℃; for 8h; Inert atmosphere;83%
With copper(l) iodide; 1,10-Phenanthroline; potassium tert-butylate In toluene at 100℃; for 48h; Inert atmosphere;82%
92-86-4

4-(4-bromophenyl)bromobenzene

102113-98-4

bis(biphenyl-4-yl)amine

728039-63-2

N-[1,1'-biphenyl]-4-yl-N-(4'-bromo[1,1'-biphenyl]-4-yl)-[1,1'-biphenyl]-4-amine

Conditions
ConditionsYield
With palladium diacetate; triphenylphosphine; sodium t-butanolate In toluene Inert atmosphere; Reflux;78%
With tri-tert-butyl phosphine; palladium diacetate; sodium t-butanolate In toluene for 2h; Reflux;75%
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium t-butanolate In toluene at 80℃; for 25h; Inert atmosphere;74%
462631-32-9

N,N-di-(4-biphenyl)benzylamine

palladium-active carbon

palladium-active carbon

7440-05-3

palladium

A

728039-63-2

N-[1,1'-biphenyl]-4-yl-N-(4'-bromo[1,1'-biphenyl]-4-yl)-[1,1'-biphenyl]-4-amine

B

102113-98-4

bis(biphenyl-4-yl)amine

Conditions
ConditionsYield
With hydrogen In ethanol; dichloromethane; chloroform; toluene
...Expand

bis(triphenylphosphine)palladium(II) dichloride

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4-(4-bromophenyl)bromobenzene

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bis(biphenyl-4-yl)amine

728039-63-2

N-[1,1'-biphenyl]-4-yl-N-(4'-bromo[1,1'-biphenyl]-4-yl)-[1,1'-biphenyl]-4-amine

Conditions
ConditionsYield
In 5,5-dimethyl-1,3-cyclohexadiene; water; toluene
In 5,5-dimethyl-1,3-cyclohexadiene; water
In 5,5-dimethyl-1,3-cyclohexadiene; water; toluene
...Expand

728039-63-2

N-[1,1'-biphenyl]-4-yl-N-(4'-bromo[1,1'-biphenyl]-4-yl)-[1,1'-biphenyl]-4-amine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: sodium t-butanolate; palladium diacetate; tri-tert-butyl phosphine / toluene / 7 h / 20 - 120 °C / Inert atmosphere
1.2: 12 h / Inert atmosphere
2.1: palladium 10% on activated carbon; hydrogen / chloroform; ethanol / 0.5 h / 20 °C
3.1: sodium t-butanolate; bis-triphenylphosphine-palladium(II) chloride / 5,5-dimethyl-1,3-cyclohexadiene / 24 h / 130 °C / Inert atmosphere
View Scheme
Multi-step reaction with 2 steps
1: tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate / 3 h / 90 °C
2: tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate / toluene / 3 h / 90 °C
View Scheme
Multi-step reaction with 2 steps
1: sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0); 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / toluene / 24 h / 100 °C
2: 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; palladium diacetate; sodium t-butanolate / toluene / 24 h / 100 °C
View Scheme
3001-15-8

4,4'-diiodobiphenyl

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bis(biphenyl-4-yl)amine

728039-63-2

N-[1,1'-biphenyl]-4-yl-N-(4'-bromo[1,1'-biphenyl]-4-yl)-[1,1'-biphenyl]-4-amine

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; sodium t-butanolate In 5,5-dimethyl-1,3-cyclohexadiene at 130℃; for 24h; Inert atmosphere;9.1 g
462631-32-9

N,N-di-(4-biphenyl)benzylamine

728039-63-2

N-[1,1'-biphenyl]-4-yl-N-(4'-bromo[1,1'-biphenyl]-4-yl)-[1,1'-biphenyl]-4-amine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: palladium 10% on activated carbon; hydrogen / chloroform; ethanol / 0.5 h / 20 °C
2: sodium t-butanolate; bis-triphenylphosphine-palladium(II) chloride / 5,5-dimethyl-1,3-cyclohexadiene / 24 h / 130 °C / Inert atmosphere
View Scheme
92-67-1

4-Aminobiphenyl

728039-63-2

N-[1,1'-biphenyl]-4-yl-N-(4'-bromo[1,1'-biphenyl]-4-yl)-[1,1'-biphenyl]-4-amine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate / 3 h / 90 °C
2: tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate / toluene / 3 h / 90 °C
View Scheme
Multi-step reaction with 2 steps
1: sodium t-butanolate; tris-(dibenzylideneacetone)dipalladium(0); 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / toluene / 24 h / 100 °C
2: 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene; palladium diacetate; sodium t-butanolate / toluene / 24 h / 100 °C
View Scheme
728039-63-2

N-[1,1'-biphenyl]-4-yl-N-(4'-bromo[1,1'-biphenyl]-4-yl)-[1,1'-biphenyl]-4-amine

C60H42N2O2

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene at 100℃; for 46h;100%
728039-63-2

N-[1,1'-biphenyl]-4-yl-N-(4'-bromo[1,1'-biphenyl]-4-yl)-[1,1'-biphenyl]-4-amine

73183-34-3

bis(pinacol)diborane

1421701-43-0

N,N-bis({[1,1'-biphenyl]-4-yl})-4'-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-[1,1'-biphenyl]-4-amine

Conditions
ConditionsYield
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; potassium acetate In 1,4-dioxane at 100℃; for 12h; Inert atmosphere;98%
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate In toluene Reflux;84%
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate In toluene Reflux;84%
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate In toluene Reflux;84%
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate In 1,4-dioxane at 80℃; Inert atmosphere;77%
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  • Bisbiphenyl-4-yl-(4'-broMo-biphenyl-4-yl)-aMine-CAS NO.: 728039-63-2

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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    TAIHO Unique Advantages:1.We're factory2.Free samples available3.Commodity inspection can be done4.ISO9001,Kosher certifications5.10 years experiences Storage:Store in cool &dry place Package:aluminium foil bag/fiber can/plastic drum Application:comp

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     China (Mainland)  |  Contact Details

    Business Type:Manufacturers

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    Address:No. 49 taifeng Road,Qianjiang City,Hubei,China

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  • Casno:

    728039-63-2

    N-[4-(4-bromophenyl)phenyl]-4-phenyl-N-(4-phenylphenyl)aniline

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     China (Mainland)  |  Contact Details

    Business Type:Trading Company

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