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73-66-5

Basic Information
CAS No.: 73-66-5
Name: 5-ethoxymethyl-2-methylpyrimidin-4-ylamine
Article Data: 15
Molecular Structure:
Molecular Structure of 73-66-5 (5-ethoxymethyl-2-methylpyrimidin-4-ylamine)
Formula: C8H13 N3 O
Molecular Weight: 167.211
Synonyms: Pyrimidine,4-amino-5-(ethoxymethyl)-2-methyl- (6CI,7CI,8CI);2-Methyl-4-amino-5-(ethoxymethyl)pyrimidine; 2-Methyl-5-(ethoxymethyl)-6-aminopyrimidine;4-Amino-2-methyl-5-(ethoxymethyl)pyrimidine;4-Amino-5-(ethoxymethyl)-2-methylpyrimidine; NSC 41790
Density: 1.113g/cm3
Boiling Point: 276.4°C at 760 mmHg
Flash Point: 121°C
Safety: A poison by ingestion. Experimental reproductive effects. When heated to decomposition it emits toxic vapors of NOx.
PSA: 61.03000
LogP: 1.48490
Synthetic route
749835-80-1

2-methyl-5-ethoxymethyl-6-chloropyrimidine

73-66-5

5-ethoxymethyl-2-methyl-pyrimidin-4-ylamine

Conditions
ConditionsYield
With ammonia In methanol at 140℃; for 4.5h; Autoclave;82%
With ethanol; ammonia at 140℃;
109-95-5

ethyl nitrite

874-43-1, 1195-07-9, 25449-06-3

5-(aminomethyl)-2-methylpyrimidin-4-amine dihydrochloride

73-66-5

5-ethoxymethyl-2-methyl-pyrimidin-4-ylamine

Conditions
ConditionsYield
With ethanol at 90 - 100℃;
64-17-5

ethanol

3699-10-3

2-ethoxymethyl-3c-methoxy-acrylonitrile

124-42-5

acetamidine hydrochloride

141-52-6

sodium ethanolate

73-66-5

5-ethoxymethyl-2-methyl-pyrimidin-4-ylamine

3699-10-3

2-ethoxymethyl-3c-methoxy-acrylonitrile

143-37-3

acetamidine

73-66-5

5-ethoxymethyl-2-methyl-pyrimidin-4-ylamine

Conditions
ConditionsYield
With ethanol
3699-12-5

3c-ethoxy-2-ethoxymethyl-acrylonitrile

143-37-3

acetamidine

73-66-5

5-ethoxymethyl-2-methyl-pyrimidin-4-ylamine

Conditions
ConditionsYield
With ethanol

3-acetoxy-2-ethoxymethyl-acrylonitrile

143-37-3

acetamidine

73-66-5

5-ethoxymethyl-2-methyl-pyrimidin-4-ylamine

Conditions
ConditionsYield
With ethanol; benzene
64-17-5

ethanol

3-acetoxy-2-ethoxymethyl-acrylonitrile

143-37-3

acetamidine

71-43-2

benzene

73-66-5

5-ethoxymethyl-2-methyl-pyrimidin-4-ylamine

Conditions
ConditionsYield
Erwaermen des Reaktionsprodukts mit 10prozentig.KOH;
Erwaermen des Reaktionsprodukts mit 10prozentig.KOH;Geschwindigkeit;
99764-73-5

3-t-butoxypropanenitrile

124-42-5

acetamidine hydrochloride

109-94-4

formic acid ethyl ester

A

73-66-5

5-ethoxymethyl-2-methyl-pyrimidin-4-ylamine

B

127556-60-9

2-methyl-4-amino-5-tert-butoxymethylpyrimidine

Conditions
ConditionsYield
Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
2141-62-0

3-(ethoxy)propionitrile

73-66-5

5-ethoxymethyl-2-methyl-pyrimidin-4-ylamine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: ethyl formate; benzene / beim Erwaermen des Reaktionsgemisches mit Dimethylsulfat
2: ethanol
View Scheme
Multi-step reaction with 2 steps
1: ethyl formate; benzene / beim Erwaermen des Reaktionsgemisches mit Diaethylsulfat
2: ethanol
View Scheme
5423-97-2

5-ethoxymethyl-2-methyl-3H-pyrimidin-4-one

73-66-5

5-ethoxymethyl-2-methyl-pyrimidin-4-ylamine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: POCl3
2: ethanol; NH3 / 140 °C
View Scheme
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Toxicity Data With Reference

1.   

orl-rat LD50:1450 mg/kg

    85GMAT    Toxicometric Parameters of Industrial Toxic Chemicals Under Single Exposure Izmerov, N.F., et al.,Moscow, USSR.: Centre of International Projects, GKNT,1982,81.
2.   

orl-mus LD50:239 mg/kg

    85GMAT    Toxicometric Parameters of Industrial Toxic Chemicals Under Single Exposure Izmerov, N.F., et al.,Moscow, USSR.: Centre of International Projects, GKNT,1982,81.

Safety Profile

A poison by ingestion. Experimental reproductive effects. When heated to decomposition it emits toxic vapors of NOx.