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73344-75-9

Basic Information
CAS No.: 73344-75-9
Name: C-(3,4-DIMETHOXY-BICYCLO[4.2.0]OCTA-1(6),2,4-TRIEN-7-YL)-METHYLAMINE
Article Data: 2
Molecular Structure:
Molecular Structure of 73344-75-9 (C-(3,4-DIMETHOXY-BICYCLO[4.2.0]OCTA-1(6),2,4-TRIEN-7-YL)-METHYLAMINE)
Formula: C11H15 N O2
Molecular Weight: 193.246
Synonyms: 4,5-Dimethoxy-1-(aminomethyl)benzocyclobutane
Density: 1.113
Boiling Point: 309oC
Flash Point: 153oC
PSA: 44.48000
LogP: 2.00250
Synthetic route
35202-54-1

3,4-dimethoxy-bicyclo[4.2.0]octa-1,3,5-triene-7-carbonitrile

73344-75-9

(±)-(3,4-dimethoxybicyclo[4.2.0]octa-1,3,5-trien-7-yl)methylamine

Conditions
ConditionsYield
With ammonia; hydrogen; nickel In methanol at 60℃; under 22502.3 Torr; Industry scale;100%
With ammonia; hydrogen In methanol at 20℃; under 2327.23 Torr; for 12h; Solvent; Reagent/catalyst;98%
64-18-6

formic acid

73344-75-9

(±)-(3,4-dimethoxybicyclo[4.2.0]octa-1,3,5-trien-7-yl)methylamine

C12H15NO3

Conditions
ConditionsYield
Stage #1: formic acid With 1,1'-carbonyldiimidazole In tetrahydrofuran at 20℃; for 0.25h;
Stage #2: (±)-(3,4-dimethoxybicyclo[4.2.0]octa-1,3,5-trien-7-yl)methylamine In tetrahydrofuran at 20℃; for 12h; Reagent/catalyst; Temperature; Solvent;
90%
1188-37-0

N-acetyl-(S)-glutamic acid

73344-75-9

(±)-(3,4-dimethoxybicyclo[4.2.0]octa-1,3,5-trien-7-yl)methylamine

869856-08-6

(1S)-4,5-dimethoxy-1-(aminomethyl)-benzocyclobutane N-acetyl-L-glutamate

Conditions
ConditionsYield
In ethanol; water at 20℃; Heating / reflux; Industry scale;40%
73344-75-9

(±)-(3,4-dimethoxybicyclo[4.2.0]octa-1,3,5-trien-7-yl)methylamine

51146-56-6

(S)-ibuprofen

C11H15NO2*2C13H18O2

Conditions
ConditionsYield
In acetonitrile at 20℃; for 24h; Solvent;40%
73344-75-9

(±)-(3,4-dimethoxybicyclo[4.2.0]octa-1,3,5-trien-7-yl)methylamine

51146-56-6

(S)-ibuprofen

A

C11H15NO2*2C13H18O2

B

C11H15NO2*2C13H18O2

Conditions
ConditionsYield
In acetonitrile at 20 - 42℃; for 20h; Temperature; Time; Solvent;A 38%
B n/a
15022-08-9

diallylcarbonate

73344-75-9

(±)-(3,4-dimethoxybicyclo[4.2.0]octa-1,3,5-trien-7-yl)methylamine

A

869856-07-5

(1S)-4,5-dimethoxy-1-(ammoniummethyl)benzocyclobutane

B

1422007-49-5

(R)-(3,4-dimethoxybicyclo[4.2.0]octa-1,3,5-trien-7-yl)methylamine

C

allyl {[(7S)-3,4-dimethoxybicyclo[4.2.0]octa-1,3,5-trien-7-yl]methyl}carbamate

D

allyl {[(7R)-3,4-dimethoxybicyclo[4.2.0]octa-1,3,5-trien-7-yl]methyl}carbamate

Conditions
ConditionsYield
With Pseudomonas cepacia lipase II In 2-methyltetrahydrofuran at 30℃; for 42h;A n/a
B n/a
C 35%
D n/a
With lipase from Pseudomonas fluorescens In tert-butyl methyl ether at 30℃; for 24h; Catalytic behavior; Reagent/catalyst; Resolution of racemate; Inert atmosphere; Enzymatic reaction; enantioselective reaction;A n/a
B n/a
C n/a
D n/a
73344-75-9

(±)-(3,4-dimethoxybicyclo[4.2.0]octa-1,3,5-trien-7-yl)methylamine

A

869856-07-5

(1S)-4,5-dimethoxy-1-(ammoniummethyl)benzocyclobutane

B

1422007-49-5

(R)-(3,4-dimethoxybicyclo[4.2.0]octa-1,3,5-trien-7-yl)methylamine

C

benzyl {[(7S)-3,4-dimethoxybicyclo[4.2.0]octa-1,3,5-trien-7-yl]methyl}carbamate

Conditions
ConditionsYield
With Pseudomonas cepacia lipase II In 2-methyltetrahydrofuran at 30℃; for 24h;A n/a
B n/a
C 30%
1470-91-3

but-3-enoyl chloride

73344-75-9

(±)-(3,4-dimethoxybicyclo[4.2.0]octa-1,3,5-trien-7-yl)methylamine

73348-43-3

N-<(4,5-dimethoxybenzocyclobutenyl)methyl>-3-butenamide

Conditions
ConditionsYield
With pyridine In dichloromethane29%
73344-75-9

(±)-(3,4-dimethoxybicyclo[4.2.0]octa-1,3,5-trien-7-yl)methylamine

73344-71-5, 73344-77-1

cis-8,9-dimethoxy-1,2,3,4,4a,5,6,10b-octahydrobenzisoquinoline

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 29 percent / pyridine / CH2Cl2
2: 57 percent / various solvent(s) / 18 h / Heating
3: LiAlH4, AlCl3 / diethyl ether / 2.25 h / Ambient temperature
View Scheme
73344-75-9

(±)-(3,4-dimethoxybicyclo[4.2.0]octa-1,3,5-trien-7-yl)methylamine

cis-N-n-propyl-8,9-dimethoxy-1,2,3,4,4a,5,6,10b-octahydrobenzisoquinoline

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 29 percent / pyridine / CH2Cl2
2: 57 percent / various solvent(s) / 18 h / Heating
3: LiAlH4, AlCl3 / diethyl ether / 2.25 h / Ambient temperature
4: NaBH4 / benzene
View Scheme
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    (3,4-Dimethoxybicyclo[4.2.0]octa-1,3,5-trien-7-yl)methanamine

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86 519 82111935

    Address:Chinese Jiangsu Province Changzhou City Jintan District Jincheng Town Miaotou NO4(Pharmaceutical Park)

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  • Casno:

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    Manufacturer Direct Sales Low Price 4,5-dimethoxy-1-(aminomethyl)benzocyclobutane

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    Known for its best quality and competitve price, this chemicals we offered is widely appreciated by our customers.Our advantages:1, High quality with competitive price:1) Standard:BP/USP/EP/Enterprise standard2) All Purity≥99%3) We are manufacturer a

    Shaanxi Mingqi Chemical Co., Ltd is committed to the development of import and export trade in the production, operation and plant extracts of pharmaceutical raw materials and inte

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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    Prime Molecular Co., Ltd. is an advanced chemical intermediates manufacture with ?two R&D centers and two production sites in China, all well-equipped with dedicated and profession

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    China (Mainland)  |  Contact Details

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    Changzhou Pesan Chemical Co., Ltd. is a dynamic and specialized chemical company. Since our establishment, We provide raw materials and key intermediates for pharmaceutical industr

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     China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:+86 021 61559630

    Address:No.7-9,Guanghua St.,Zhonglou District,Changzhou,China

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    As a professional chemical R&D and synthesis supplier, Shanghai Forever Synthesis Co.,Ltd. is specialized R&D and synthesizing APIs and Impurities. Besides, we value more special service, that is, to customize chemical synthesis according to client’s

    As a professional chemical synthesis supplier, Shanghai Forever Synthesis Co.,Ltd. is specialized in trading and developing active pharmaceutical ingredients, intermediates, and AP

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    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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    United Scientific Company Located in Shanghai of China , is a competitive player in the global specialty and fine chemical market. Fenghua has both the expertise and flexibility to produce a wide range of chemicals. Focusing on developing the innovat

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    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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    The system can just identify the products information in first sheet, it is not be permitted to add or edit new sheet by userself.Our products are required in MG to Gram only. · Pharmaceutical Reference Standards· Traceable workin

    SimSon Pharma, a renowned name in pharmaceutical sector, has built high its reputation as a complete solution provider in contract research arena. We are a JAS/ANZ ISO 9001:2015 Ce

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    India  |  Contact Details

    Business Type:Manufacturers

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    Ivabradine Impurity f,73344-75-9

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    instock with good quality and wholesale price Storage:Keep in a cool & dry place Package:Packing material and QTY as your request Application:Pharma;Industry;other application Transportation:Express or as your request Port:Any port of China

    Wuhan MoonZY Biological Technology Co.,Ltd (MoonzyBio)is located in Wuhan city,hubei province,China,we have a group of senior technical backbones, specialized in R & D and sales in

  • Wuhan MoonZY Biological Technology Co.,Ltd

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:13545198479

    Address:203,Building 3, International Enterprise Center, No. 1 Guanshan 2nd Road, East Lake New Technology Development Zone,

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    Bicyclo[4.2.0]octa-1,3,5-triene-7-methanamine,3,4-dimethoxy-

    Min.Order: 0

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    Bicyclo[4.2.0]octa-1,3,5-triene-7-methanamine,3,4-dimethoxy-Appearance:Off white to slight yellow solid Storage:Store in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/Pharmaceutical intermediates T

    Nanjing Raymon Biotech Co., Ltd. is specialized in developing and marketing middle & high level pharmaceutical intermediates. We are supplying different categories of high-quality

  • Nanjing Raymon Biotech Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:86-025-52181296

    Address:Block B, No. 918, Shuanglong Avenue

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