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Basic Information
CAS No.: 7538-44-5
Name: BIS(2-HYDROXYETHYL)-3-AMINOPROPYLTRIETHOXYSILANE
Article Data: 2
Molecular Structure:
Molecular Structure of 7538-44-5 (BIS(2-HYDROXYETHYL)-3-AMINOPROPYLTRIETHOXYSILANE)
Formula: C13H31NO5Si
Molecular Weight: 309.478
Synonyms: Ethanol,2,2'-[[3-(triethoxysilyl)propyl]imino]di- (7CI,8CI);3-[N,N-Bis(2-hydroxyethyl)amino]propyltriethoxysilane;A 111;A 1111;Bis(2-hydroxyethyl)-3-(aminopropyl)triethoxysilane;JH-A111;N,N-Bis(2-hydroxyethyl)-3-aminopropyltriethoxysilane;N,N-Bis(b-hydroxyethyl)-g-(aminopropyl)triethoxysilane;N,N-Di-b-(hydroxyethyl)-g-aminopropyltriethoxysilane;N-Bis(b-hydroxyethyl) g-aminopropyltriethoxysilane;SIB1140.0;SIT 1140.0;Y 2967;[3-[Bis-(2-hydroxyethyl)amino]propyl]triethoxysilane;[g-[N,N-Bis(b-hydroxyethyl)amino]propyl]triethoxysilane;Ethanol,2,2'-[[3-(triethoxysilyl)propyl]imino]bis-;
EINECS: 231-408-9
Density: 1.03 g/cm3
Boiling Point: 380.2 °C at 760 mmHg
Flash Point: 183.7 °C
Hazard Symbols: IrritantXi
Risk Codes: 10-36/37/38
Safety: 26
Transport Information: UN 1170 3
PSA: 71.39000
LogP: 0.71150
Synthetic route
5089-70-3

(3-chloropropyl)triethoxysilane

111-42-2

2,2'-iminobis[ethanol]

7538-44-5

3-[bis(2-hydroxyethyl)amino]propyltriethoxysilane

Conditions
ConditionsYield
With potassium iodide In dimethyl sulfoxide at 120℃; Inert atmosphere;
7538-44-5

3-[bis(2-hydroxyethyl)amino]propyltriethoxysilane

64-17-5

ethanol

75-24-1

trimethylaluminum

C15H34AlNO6Si

Conditions
ConditionsYield
In toluene at 0℃; for 4h; Inert atmosphere; Schlenk technique;95%
7538-44-5

3-[bis(2-hydroxyethyl)amino]propyltriethoxysilane

64-17-5

ethanol

1191-47-5

dibutylmagnesium

C14H33MgNO6Si

Conditions
ConditionsYield
In n-heptan1ol at 0 - 20℃; for 4h; Inert atmosphere; Schlenk technique;91%
7538-44-5

3-[bis(2-hydroxyethyl)amino]propyltriethoxysilane

64-17-5

ethanol

555-31-7

aluminum isopropoxide

C15H34AlNO6Si

Conditions
ConditionsYield
In toluene at 0℃; for 4h; Inert atmosphere; Schlenk technique;88%
546-68-9

titanium(IV) isopropylate

7538-44-5

3-[bis(2-hydroxyethyl)amino]propyltriethoxysilane

C19H43NO7SiTi

Conditions
ConditionsYield
In ethanol; dichloromethane at 20℃; for 4h; Inert atmosphere; Schlenk technique;
7538-44-5

3-[bis(2-hydroxyethyl)amino]propyltriethoxysilane

C23H43N5O9Si

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: 35 h / 80 °C / Inert atmosphere
1.2: 0.75 h / 150 °C / Inert atmosphere
2.1: water / 2 h / 85 °C
View Scheme
7538-44-5

3-[bis(2-hydroxyethyl)amino]propyltriethoxysilane

C35H65N5O9Si2

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: 35 h / 80 °C / Inert atmosphere
1.2: 0.75 h / 150 °C / Inert atmosphere
2.1: water / 2 h / 85 °C
3.1: ethanol / 3 h / 40 °C
View Scheme

1,6-dicyanatohexane

7538-44-5

3-[bis(2-hydroxyethyl)amino]propyltriethoxysilane

C29H55N5O9Si

Conditions
ConditionsYield
Stage #1: 1,6-dicyanatohexane; 3-[bis(2-hydroxyethyl)amino]propyltriethoxysilane at 80℃; for 35h; Inert atmosphere;
Stage #2: With tin(IV) chloride at 150℃; for 0.75h; Inert atmosphere;
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    Package:50 mL in glass bottle Application:3-[Bis(2-hydroxyethyl)amino]propyl-triethoxysilane solution was used to functionalize nanoporous silica (SBA-15).

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    BIS(2-HYDROXYETHYL)-5-AMINOPROPYLTRIETHOXYSILANE

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Chemistry

The Molecular Structure of Bis(2-hydroxyethyl)aminopropyltriethoxysilane (CAS NO.7538-44-5):

Empirical Formula: C13H31NO5Si
Molecular Weight: 309.4744 
IUPAC Name: 2-[2-hydroxyethyl(3-triethoxysilylpropyl)amino]ethanol 
Nominal Mass: 309 Da
Average Mass: 309.4744 Da
Monoisotopic Mass: 309.197149 Da 
Index of Refraction: 1.465
Molar Refractivity: 83.02 cm3
Molar Volume: 300.2 cm3
Surface Tension: 34.3 dyne/cm
Density: 1.03 g/cm3
Flash Point: 183.7 °C
Enthalpy of Vaporization: 72.68 kJ/mol
Boiling Point: 380.2 °C at 760 mmHg
Vapour Pressure: 2.42E-07 mmHg at 25°C 
InChI
InChI=1/C13H31NO5Si/c1-4-17-20(18-5-2,19-6-3)13-7-8-14(9-11-15)10-12-16/h15-16H,4-13H2,1-3H3
Smiles
[Si](OCC)(OCC)(OCC)CCCN(CCO)CCO
EINECS: 231-408-9 

Safety Profile

Hazard Codes :IrritantXi
Risk Statements :
  R10-36/37/38 (Flammable;Irritating to eyes, respiratory system and skin)
Safety Statements :
  S26 (In case of contact with eyes, rinse immediately with plenty of WATER and seek medical advice )
RIDADR : UN 1170 3/PG 3

Specification

 Bis(2-hydroxyethyl)aminopropyltriethoxysilane (CAS NO.7538-44-5) is also called as (Bis(2-hydroxyethyl)aminopropyl)triethoxysilane ; 2,2'-((3-(Triethoxysilyl)propyl)imino)bisethanol ; Ethanol, 2,2'-((3-(triethoxysilyl)propyl)imino)bis- and so on.