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756525-99-2

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Basic Information
CAS No.: 756525-99-2
Name: alpha-MaleiMidopropionyl-oMega-succiniMidyl-4(ethylene glycol)
Article Data: 4
Molecular Structure:
Molecular Structure of 756525-99-2 (alpha-MaleiMidopropionyl-oMega-succiniMidyl-4(ethylene glycol))
Formula: C22H31N3O11
Molecular Weight: 513.502
Synonyms: AmbotzPEG1575;α-Maleimidopropionyl-ω-succinimidyl-4(ethylene glycol);monodisperse Mal-PEG4-NHS-ester;(2,5-dioxopyrrolidin-1-yl) 3-[2-[2-[2-[2-[3-(2,5-dioxopyrrol-1-yl)propanoylamino]ethoxy]ethoxy]ethoxy]ethoxy]propanoate;
Density: 1.36±0.1 g/cm3(Predicted)
PSA: 170.57000
LogP: -0.80250
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Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: dichloromethane / 20 °C
2: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C
3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride
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Multi-step reaction with 3 steps
1: dichloromethane / 20 °C
2: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C
3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride
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Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C
2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride
View Scheme
Multi-step reaction with 2 steps
1: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C
2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride
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3-[2-[2-[2-[[3-(2,5-dioxo-2,5-dihydro-pyrrol-1-yl)-propionylamino]ethoxy]ethoxy]ethoxy]ethoxy]propionic acid-2,5-dioxo-pyrrolidin-1-yl ester

Conditions
ConditionsYield
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride0.109 g
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride0.109 g
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride0.109g
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 2h;330 mg
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Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: dicyclohexyl-carbodiimide
2: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C
3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride
View Scheme
Multi-step reaction with 3 steps
1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 2 h / 20 °C
2: sodium hydrogencarbonate / water; 1,2-dimethoxyethane / 2 h / 20 °C
3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 2 h / 20 °C
View Scheme
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3-maleimidopropionic acid N-hydroxysuccinimide ester

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Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium hydrogencarbonate / water; 1,2-dimethoxyethane / 2 h / 20 °C
2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 2 h / 20 °C
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3-[2-[2-[2-[[3-(2,5-dioxo-2,5-dihydro-pyrrol-1-yl)-propionylamino]ethoxy]ethoxy]ethoxy]ethoxy]propionic acid-2,5-dioxo-pyrrolidin-1-yl ester

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N-(2-aminoethyl)-valine

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Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In dichloromethane97%
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C24H40N6O5

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Conditions
ConditionsYield
In dichloromethane at 20℃; for 4h;95%
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3-[2-[2-[2-[[3-(2,5-dioxo-2,5-dihydro-pyrrol-1-yl)-propionylamino]ethoxy]ethoxy]ethoxy]ethoxy]propionic acid-2,5-dioxo-pyrrolidin-1-yl ester

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2-(5-methoxyindol-3-yl)ethylamine

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Conditions
ConditionsYield
In N,N-dimethyl-formamide at 20℃; for 0.5h;92%
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3-[2-[2-[2-[[3-(2,5-dioxo-2,5-dihydro-pyrrol-1-yl)-propionylamino]ethoxy]ethoxy]ethoxy]ethoxy]propionic acid-2,5-dioxo-pyrrolidin-1-yl ester

tert-butyl 1-((4-(4-(3-azidopropoxy)benzoyl)phenyl)amino)-3,6,9,12-tetraoxapentadecan-15-oate

tert-butyl 1-((4-(4-((1-(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)-3,19-dioxo-7,10,13,16-tetraoxa-4,20-diazatricosan-23-yl)oxy)benzoyl)phenyl)amino)-3,6,9,12-tetraoxapentadecan-15-oate

Conditions
ConditionsYield
In dichloromethane at 20℃; for 3h;90%
756525-99-2

3-[2-[2-[2-[[3-(2,5-dioxo-2,5-dihydro-pyrrol-1-yl)-propionylamino]ethoxy]ethoxy]ethoxy]ethoxy]propionic acid-2,5-dioxo-pyrrolidin-1-yl ester

L-valyl-N6-(tert-butoxycarbonyl)-L-lysine

N-[19-(2,5-dioxo-2,5-dihydro-1H-pyrrol-1-yl)-17-oxo-4,7,10,13-tetraoxa-16-azanonadecan-1-oyl]-L-valyl-N6-(tert-butoxycarbonyl)-L-lysine

Conditions
ConditionsYield
With 4-methyl-morpholine In N,N-dimethyl-formamide at 20℃;82%
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    Business Type:Trading Company

    Tel:+44 (0)208 191 7890

    Address:Unit11, Ark Business Centre, Gorden Road, Loughborough, United Kingdom

       Inquiry Now

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