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| CAS No.: | 768398-03-4 |
|---|---|
| Name: | (6-METHYL-2-P-TOLYL-IMIDAZO[1,2-A]PYRIDIN-3-YL)-ACETONITRILE |
| Article Data: | 10 |
| Molecular Structure: | |
|
|
|
| Formula: | C17H15 N3 |
| Molecular Weight: | 261.326 |
| Synonyms: | Zolpidem IV |
| Density: | 1.12g/cm3 |
| PSA: | 41.09000 |
| LogP: | 3.68418 |
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- 97730-31-9(S)-4'-(2-Methylbutyl)Biphenyl-4-Carbonitrile
- 88965-00-8
6-methyl-2-(4-methyl-phenyl)-imidazo[1,2-a]pyridine
- 590-17-0
cyanomethyl bromide
- 768398-03-4
6-methyl-3-cyanomethyl-2-(4-methylphenyl)imidazo[1,2-a]pyridine
| Conditions | Yield |
|---|---|
| With fac-tris(2-phenylpyridinato-N,C2')iridium(III); sodium hydrogencarbonate In dimethyl sulfoxide at 20℃; for 12h; Schlenk technique; Inert atmosphere; Irradiation; regioselective reaction; | 85% |
- 59463-54-6
S-cyanomethyl O-ethyl carbonodithioate
- 88965-00-8
6-methyl-2-(4-methyl-phenyl)-imidazo[1,2-a]pyridine
- 768398-03-4
6-methyl-3-cyanomethyl-2-(4-methylphenyl)imidazo[1,2-a]pyridine
| Conditions | Yield |
|---|---|
| With tris[2-phenylpyridinato-C2,N]iridium(III); N,N-dimethyl-formamide at 24℃; Minisci Aromatic Substitution; Inert atmosphere; UV-irradiation; regioselective reaction; | 61% |
| With dilauryl peroxide In 1,2-dichloro-ethane at 85℃; Microwave irradiation; regioselective reaction; | 51% |
- 13138-21-1
diazoacetonitrile
- 88965-00-8
6-methyl-2-(4-methyl-phenyl)-imidazo[1,2-a]pyridine
- 768398-03-4
6-methyl-3-cyanomethyl-2-(4-methylphenyl)imidazo[1,2-a]pyridine
| Conditions | Yield |
|---|---|
| With iron(III) chloride In acetonitrile at 60℃; for 6h; Sealed tube; Green chemistry; | 50% |
- 88965-00-8
6-methyl-2-(4-methyl-phenyl)-imidazo[1,2-a]pyridine
- 75-05-8
acetonitrile
- 768398-03-4
6-methyl-3-cyanomethyl-2-(4-methylphenyl)imidazo[1,2-a]pyridine
| Conditions | Yield |
|---|---|
| With ferrocene; bis(1-methyl-1-phenylethyl)peroxide at 20 - 100℃; for 20h; Inert atmosphere; Sealed tube; | 48% |
- 143-33-9
sodium cyanide
- 106961-34-6
Trimethyl-(6-methyl-2-p-tolyl-imidazo[1,2-a]pyridin-3-ylmethyl)-ammonium; iodide
- 768398-03-4
6-methyl-3-cyanomethyl-2-(4-methylphenyl)imidazo[1,2-a]pyridine
| Conditions | Yield |
|---|---|
| Yield given; | |
| In water at 82 - 84℃; for 12h; |
- 151-50-8
potassium cyanide
- 106961-33-5
dimethyl-(6-methyl-2-p-tolylimidazo[1,2-a]pyridin-3-ylmethyl)-amine
A
- 768398-03-4
6-methyl-3-cyanomethyl-2-(4-methylphenyl)imidazo[1,2-a]pyridine
B
- 365213-58-7
2-(4-methylphenyl)-6-methylimidazo[1,2-α]pyridine-3-acetamide
| Conditions | Yield |
|---|---|
| Stage #1: dimethyl-(6-methyl-2-p-tolylimidazo[1,2-a]pyridin-3-ylmethyl)-amine With methyl iodide In ethanol at 20℃; for 24h; Stage #2: potassium cyanide In ethanol; water for 4h; Heating; |
- 88965-00-8
6-methyl-2-(4-methyl-phenyl)-imidazo[1,2-a]pyridine
- 768398-03-4
6-methyl-3-cyanomethyl-2-(4-methylphenyl)imidazo[1,2-a]pyridine
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1.1: 78 percent / acetic acid / H2O / 4 h / 50 - 55 °C 2.1: MeI / ethanol / 24 h / 20 °C 2.2: H2O; ethanol / 4 h / Heating View Scheme | |
| Multi-step reaction with 3 steps 1: 79 percent / AcOH View Scheme |
- 106961-33-5
dimethyl-(6-methyl-2-p-tolylimidazo[1,2-a]pyridin-3-ylmethyl)-amine
- 768398-03-4
6-methyl-3-cyanomethyl-2-(4-methylphenyl)imidazo[1,2-a]pyridine
- 1101863-48-2
C20H24N3O2(1+)*Cl(1-)
- 143-33-9
sodium cyanide
- 768398-03-4
6-methyl-3-cyanomethyl-2-(4-methylphenyl)imidazo[1,2-a]pyridine
| Conditions | Yield |
|---|---|
| Stage #1: C20H24N3O2(1+)*Cl(1-) With sodium hydroxide; water pH=7.5 - 8; Stage #2: sodium cyanide In water at 50 - 55℃; for 3h; Product distribution / selectivity; |
- 1603-41-4
(5-methyl-pyridin-2-yl)amine
- 768398-03-4
6-methyl-3-cyanomethyl-2-(4-methylphenyl)imidazo[1,2-a]pyridine
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: sodium hydrogencarbonate / ethanol / 6 h / 20 °C / Inert atmosphere 2: ferrocene; bis(1-methyl-1-phenylethyl)peroxide / 20 h / 20 - 100 °C / Inert atmosphere; Sealed tube View Scheme |
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