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77472-71-0

Basic Information
CAS No.: 77472-71-0
Name: 2-Oxo-4-phenylpyrrolidine-1-acetic acid hydrazide
Article Data: 2
Cas Database
Molecular Structure:
Molecular Structure of 77472-71-0 (2-Oxo-4-phenylpyrrolidine-1-acetic acid hydrazide)
Formula: C12H15N3O2
Molecular Weight: 233.27
Synonyms: 2-Oxo-4-phenylpyrrolidine-1-acetic acid hydrazide
EINECS: 204-259-2
Density: 1.243±0.06 g/cm3(Predicted)
Melting Point: 154-155 °C
Boiling Point: 529.4±50.0 °C(Predicted)
PSA: 75.43000
LogP: 1.02150
Synthetic route
70291-40-6

2-oxo-4-phenyl-1-pyrrolidineacetic acid, ethyl ester

77472-71-0

2-Oxo-4-phenylpyrrolidine-1-acetic acid hydrazide

Conditions
ConditionsYield
With hydrazine hydrate at 0 - 20℃; for 20h;78%
With hydrazine hydrate In ethanol for 8h; Heating;67%
1198-97-6

4-phenylpyrrolidin-2-one

77472-71-0

2-Oxo-4-phenylpyrrolidine-1-acetic acid hydrazide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 1.) NaH / 1.) dioxane, 90 deg C, 1 h, 2.) 125 deg C, 5 h
2: 67 percent / hydrazine hydrate / ethanol / 8 h / Heating
View Scheme
77519-55-2

2-oxo-4-phenylpyrrolidine-3-carboxylic acid

77472-71-0

2-Oxo-4-phenylpyrrolidine-1-acetic acid hydrazide

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 58 percent / 0.5 h / 190 °C
2: 1.) NaH / 1.) dioxane, 90 deg C, 1 h, 2.) 125 deg C, 5 h
3: 67 percent / hydrazine hydrate / ethanol / 8 h / Heating
View Scheme
55790-17-5

3-methoxycarbonyl-4-phenyl-2-pyrrolidone

77472-71-0

2-Oxo-4-phenylpyrrolidine-1-acetic acid hydrazide

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 89.6 percent / 10percent aq. KOH / 5 h / Heating
2: 58 percent / 0.5 h / 190 °C
3: 1.) NaH / 1.) dioxane, 90 deg C, 1 h, 2.) 125 deg C, 5 h
4: 67 percent / hydrazine hydrate / ethanol / 8 h / Heating
View Scheme
104-88-1

4-chlorobenzaldehyde

77472-71-0

2-Oxo-4-phenylpyrrolidine-1-acetic acid hydrazide

N'-[(E)-(4-chlorophenyl)methylidene]-2-(4-phenyl-2-oxopyrrolidin-1-yl)acetohydrazide

Conditions
ConditionsYield
In ethanol Reflux;89%
77472-71-0

2-Oxo-4-phenylpyrrolidine-1-acetic acid hydrazide

67-64-1

acetone

2-(4-phenyl-2-oxopyrrolidin-1-yl)-N'-isopropylideneacetohydrazide

Conditions
ConditionsYield
for 1h; Reflux;85%
100-52-7

benzaldehyde

77472-71-0

2-Oxo-4-phenylpyrrolidine-1-acetic acid hydrazide

2-(4-phenyl-2-oxopyrrolidin-1-yl)-N'-[(E)-phenyl methylidene]acetohydrazide

Conditions
ConditionsYield
In ethanol Reflux;81%
123-11-5

4-methoxy-benzaldehyde

77472-71-0

2-Oxo-4-phenylpyrrolidine-1-acetic acid hydrazide

N'-[(E)-(4-methoxyphenyl)methylidene]-2-(4-phenyl-2-oxopyrrolidin-1-yl)acetohydrazide

Conditions
ConditionsYield
In ethanol Reflux;71%
77472-71-0

2-Oxo-4-phenylpyrrolidine-1-acetic acid hydrazide

98-86-2

acetophenone

2-(4-phenyl-2-oxopyrrolidin-1-yl)-N'-[(1E)-1-phenyl ethylidene]acetohydrazide

Conditions
ConditionsYield
In ethanol for 3h; Reflux;69%
500-22-1

3-pyridinecarboxaldehyde

77472-71-0

2-Oxo-4-phenylpyrrolidine-1-acetic acid hydrazide

2-(4-phenyl-2-oxopyrrolidin-1-yl)-N'-[(E)-(pyridin-3-yl)methylidene]acetohydrazide

Conditions
ConditionsYield
In ethanol Reflux;62%
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  • CAS:77472-71-0 Phenylpiracetam hydrazide

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    CAS:77472-71-0 Phenylpiracetam hydrazide

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