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Basic Information
| CAS No.: | 7795-91-7 |
|---|---|
| Name: | Ethylene glycol mono-sec-butyl ether |
| Molecular Structure: | |
|
|
|
| Formula: | C6H14O2 |
| Molecular Weight: | 118.176 |
| Synonyms: | 2-butan-2-yloxyethanol;2-sec-Butoxyethanol;2-(1-Methylpropoxy)ethanol;Ethanol, 2-sec-butoxy-;Ethanol, 2-sec-butoxy- (6CI,7CI,8CI);2-(1-Methylpropoxy)ethanol;2-sec-Butoxyethanol;Ethylene glycol mono-sec-butyl ether; |
| Density: | 0.896g/cm3 |
| Melting Point: | -69.47°C (estimate) |
| Boiling Point: | 157.8°Cat760mmHg |
| Flash Point: | 50.2°C |
| Safety: | Moderately toxic by ingestion. When heated to decomposition it emits acrid smoke and irritating fumes. See also GLYCOL ETHERS. |
| PSA: | 29.46000 |
| LogP: | 0.79380 |
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Synthetic route
Conditions
| Conditions | Yield |
|---|---|
| With hydro silicate at 99 - 104℃; |
Conditions
| Conditions | Yield |
|---|---|
| With diisobutylaluminium hydride; benzene Behandeln einer Loesung des erhaltenen Diisobutylaluminium-<2-sec-butoxy-aethylats> in Aether mit wss.Schwefelsaeure; | |
| With lithium aluminium tetrahydride; zirconium(IV) chloride In diethyl ether at 30℃; for 12h; | 86 % Spectr. |
Conditions
| Conditions | Yield |
|---|---|
| With sulfuric acid at 95℃; |
Conditions
| Conditions | Yield |
|---|---|
| In benzene |
Conditions
| Conditions | Yield |
|---|---|
| (i) EtMgBr, (ii) /BRN= 102520/; Multistep reaction; |
Conditions
| Conditions | Yield |
|---|---|
| In benzene at 80℃; |
- 497-26-7
2-methyl-1,3-dioxolane
- 97-93-8
triethylaluminum
A
- 110-80-5
2-ethoxy-ethanol
B
- 7795-91-7
2-(1-Methylpropoxy)ethanol
Conditions
| Conditions | Yield |
|---|---|
| With diethylaluminium hydride In hexane; kerosene for 50h; Heating; | A 0.01 mol B 0.03 mol |
...Expand
- 126-39-6
2-ethyl-2-methyl-1,3-dioxolane
- 97-93-8
triethylaluminum
A
- 7795-91-7
2-(1-Methylpropoxy)ethanol
B
- 7795-93-9
2-(1-ethyl-1-methyl-propoxy)-ethanol
Conditions
| Conditions | Yield |
|---|---|
| With diethylaluminium hydride In hexane; kerosene for 40h; Heating; | A 0.01 mol B 0.03 mol |
...Expand
- 126-39-6
2-ethyl-2-methyl-1,3-dioxolane
A
- 7795-91-7
2-(1-Methylpropoxy)ethanol
B
- 7795-93-9
2-(1-ethyl-1-methyl-propoxy)-ethanol
Conditions
| Conditions | Yield |
|---|---|
| With triethylaluminum; diethylaluminium hydride In hexane; kerosene for 20h; Heating; | A 0.015 mol B 0.015 mol |
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Ethylene glycol mono-sec-butyl ether
Toxicity Data With Reference
| 1. | orl-rat LD50:790 mg/kg | SCCUR* Shell Chemical Company. Unpublished Report. (2401 Crow Canyon Rd., San Romon, CA 94583) | ||
| 2. | orl-mus LD50:1660 mg/kg | SCCUR* Shell Chemical Company. Unpublished Report. (2401 Crow Canyon Rd., San Romon, CA 94583) |
Consensus Reports
Glycol ether compounds are on the Community Right-To-Know List.
Safety Profile
Moderately toxic by ingestion. When heated to decomposition it emits acrid smoke and irritating fumes. See also GLYCOL ETHERS.