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790-41-0

Basic Information
CAS No.: 790-41-0
Name: P-CHLOROBENZOIC ANHYDRIDE
Article Data: 65
Molecular Structure:
Molecular Structure of 790-41-0 (P-CHLOROBENZOIC ANHYDRIDE)
Formula: C14H8 Cl2 O3
Molecular Weight: 295.122
Synonyms: Benzoic acid,4-chloro-, anhydride (9CI); Benzoic acid, p-chloro-, anhydride (6CI,7CI,8CI);4-Chlorobenzoic acid anhydride; 4-Chlorobenzoic anhydride; NSC 404992;p-Chlorobenzoic acid anhydride; p-Chlorobenzoic anhydride
Density: 1.401g/cm3
Boiling Point: 439°C at 760 mmHg
Flash Point: 182.5°C
PSA: 43.37000
LogP: 3.99060
Synthetic route
74-11-3

para-chlorobenzoic acid

790-41-0

4-chlorobenzoic anhydride

Conditions
ConditionsYield
With iodine; triethylamine; triphenylphosphine In dichloromethane at 0 - 20℃;99%
With N,N-bis[2-oxo-3-oxazolidinyl]phosphorodiamidic chloride; tributyl-amine In acetonitrile at 20℃; for 0.5h;97%
With thionyl chloride In dichloromethane at 22 - 25℃; for 1h;96.9%
15163-60-7

p-chlorobenzoic acid potassium salt

122-01-0

4-chloro-benzoyl chloride

790-41-0

4-chlorobenzoic anhydride

Conditions
ConditionsYield
With 1,4-diaza-bicyclo[2.2.2]octane for 0.116667h;98%
With N-benzyl-N,N,N-triethylammonium chloride In chloroform at 20℃; for 2h; Acylation;97%
122-01-0

4-chloro-benzoyl chloride

790-41-0

4-chlorobenzoic anhydride

Conditions
ConditionsYield
With sodium hydrogencarbonate In acetonitrile at 45℃; for 5h; ultrasound;97%
With bis(triphenylphosphine)dichlorocobalt(II); tetrabutylammomium bromide; sodium hydrogencarbonate In acetonitrile at 120℃; for 12h;95%
With N,N-dimethyl-formamide; zinc In pentane at 20℃; for 2h;95%
450408-66-9

4,5-dichloro-2-(4-chloro-benzoyl)-2H-pyridazin-3-one

A

932-22-9

4,5-dichloro-2H-pyridazin-3-one

B

790-41-0

4-chlorobenzoic anhydride

Conditions
ConditionsYield
With zinc(II) chloride In acetonitrile for 7h; Heating;A n/a
B 95%
15163-60-7

p-chlorobenzoic acid potassium salt

74-11-3

para-chlorobenzoic acid

790-41-0

4-chlorobenzoic anhydride

Conditions
ConditionsYield
Stage #1: para-chlorobenzoic acid With trichloroisocyanuric acid; triphenylphosphine In dichloromethane at 0 - 20℃;
Stage #2: p-chlorobenzoic acid potassium salt In dichloromethane at 20℃; for 1.5h;
94%
15966-68-4

1-(4-Aminophenyl)-5-phenyl-1,2,3-triazole

122-01-0

4-chloro-benzoyl chloride

A

89779-05-5

5-phenyl-1-<4-(4-chlorobenzoylamino)phenyl>-1H-1,2,3-triazole

B

790-41-0

4-chlorobenzoic anhydride

Conditions
ConditionsYield
In pyridine at 70℃; for 3h;A 80%
B n/a
84292-45-5

1-(4-Aminophenyl)-5-methyl-1,2,3-triazole

122-01-0

4-chloro-benzoyl chloride

A

89779-17-9

5-methyl-1-<4-(4-chlorobenzoylamino)phenyl>-1H-1,2,3-triazole

B

790-41-0

4-chlorobenzoic anhydride

Conditions
ConditionsYield
In pyridine at 70℃; for 3h;A 55%
B n/a
104-88-1

4-chlorobenzaldehyde

A

790-41-0

4-chlorobenzoic anhydride

B

74-11-3

para-chlorobenzoic acid

Conditions
ConditionsYield
With bromine; oxygen In acetonitrile at 20℃; for 5h; UV-irradiation;A 28%
B 45%
1613-88-3

4-chloro-N-hydroxybenzamide

A

790-41-0

4-chlorobenzoic anhydride

B

74-11-3

para-chlorobenzoic acid

Conditions
ConditionsYield
With dinitrogen tetraoxide In acetonitrile at -20℃; for 2h;A 25%
B 41%
64-17-5

ethanol

74-11-3

para-chlorobenzoic acid

A

7335-27-5

ethyl 4-chlorobenzoate

B

790-41-0

4-chlorobenzoic anhydride

Conditions
ConditionsYield
With magnesium chloride at 40℃; for 24h;A 20%
B n/a
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  • P-Chlorobenzoic Anhydride  CAS NO.790-41-0

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    P-Chlorobenzoic Anhydride CAS NO.790-41-0

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