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790304-84-6

Basic Information
CAS No.: 790304-84-6
Name: Isoquinoline,6-(1-methylethyl)-
Article Data: 4
Cas Database
Molecular Structure:
Molecular Structure of 790304-84-6 (Isoquinoline,6-(1-methylethyl)-)
Formula: C12H13 N
Molecular Weight: 171.242
Synonyms: 6-Isopropylisoquinoline
EINECS: N/A
Density: 1.026±0.06 g/cm3(Predicted)
Melting Point: 44-45 °C
Boiling Point: 284.1±9.0 °C(Predicted)
Flash Point: N/A
Solubility: N/A
Appearance: N/A
Hazard Symbols: N/A
Risk Codes: N/A
Safety:
Transport Information: N/A
PSA: 12.89000
LogP: 3.35820
Synthetic route
34784-05-9

6-bromo-isoquinoline

1068-55-9

isopropylmagnesium chloride

790304-84-6

6-isopropylisoquinoline

Conditions
ConditionsYield
Stage #1: isopropylmagnesium chloride With zinc(II) chloride In tetrahydrofuran at 0℃; for 1.5h; Inert atmosphere;
Stage #2: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride In tetrahydrofuran for 0.25h;
Stage #3: 6-bromo-isoquinoline In tetrahydrofuran for 12h;
75%

N-[(4-isopropylphenyl)methylene]-2,2-dimethoxyethanamine

790304-84-6

6-isopropylisoquinoline

Conditions
ConditionsYield
Stage #1: N-[(4-isopropylphenyl)methylene]-2,2-dimethoxyethanamine With sulfuric acid at 140℃; for 0.333333h;
Stage #2: With sodium hydroxide In water
15%
With sulfuric acid at 100℃; for 0.5h;
790304-84-6

6-isopropylisoquinoline

1609-47-8

diethyl dicarbonate

27491-70-9, 28447-24-7, 25411-73-8

dimethyl diazomethylphosphonate

ethyl (R)-1-(diazo(dimethoxyphosphoryl)methyl)-6-isopropylisoquinoline-2(1H)-carboxylate

Conditions
ConditionsYield
With (R)-6,6’-bis(3',4',5'-trifluoro-2,6-dimethyl[1,1'-biphenyl]-4-yl)-1,1'-spirobiindane-7,7'-diyl phosphate In toluene at -30℃; for 56h; Inert atmosphere; Molecular sieve; enantioselective reaction;97%
790304-84-6

6-isopropylisoquinoline

935542-80-6

6-isopropyl-1,2,3,4-tetrahydroisoquinoline hydrochloride

Conditions
ConditionsYield
Stage #1: 6-isopropylisoquinoline With hydrogen; acetic acid; platinum(IV) oxide for 72h;
Stage #2: With hydrogenchloride In 1,4-dioxane
95%
623-73-4

diazoacetic acid ethyl ester

790304-84-6

6-isopropylisoquinoline

1609-47-8

diethyl dicarbonate

ethyl (R)-1-(1-diazo-2-ethoxy-2-oxoethyl)-6-isopropylisoquinoline-2(1H)-carboxylate

Conditions
ConditionsYield
With (R)-6,6’-bis((4-(tert-butyl)-2-methylphenyl))-1,1'-spirobiindane-7,7'-diyl phosphate In toluene at -20℃; for 88h; Inert atmosphere; Molecular sieve; enantioselective reaction;78%
790304-84-6

6-isopropylisoquinoline

C12H13NO

Conditions
ConditionsYield
With dihydrogen peroxide; acetic acid at 80℃; for 12h;60%
790304-84-6

6-isopropylisoquinoline

13716-46-6

triethylsilyloxydiethyl phosphonic ester

17341-93-4

2,2,2-Trichloroethyl chloroformate

A

C19H25Cl3NO5P

B

C19H25Cl3NO5P

Conditions
ConditionsYield
With 1-((S)-1-(N-benzyl-N-methylcarbamoyl)-2,2-dimethylpropyl)-3-(3,5-bis(trifluoromethyl)phenyl)thiourea In toluene at -50℃; for 72h; Overall yield = 87 %; enantioselective reaction;A n/a
B n/a
790304-84-6

6-isopropylisoquinoline

630422-59-2

1-chloro-6-isopropylisoquinoline

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: acetic acid; dihydrogen peroxide / 12 h / 80 °C
2: trichlorophosphate / 6 h / 50 °C
View Scheme
790304-84-6

6-isopropylisoquinoline

1-(cyclohex-1-en-1-yl)-6-isopropylisoquinoline

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: acetic acid; dihydrogen peroxide / 12 h / 80 °C
2.1: trichlorophosphate / 6 h / 50 °C
3.1: potassium carbonate / tetrahydrofuran / 0.5 h / Inert atmosphere
3.2: 12 h / 80 °C / Inert atmosphere
View Scheme
790304-84-6

6-isopropylisoquinoline

6-isopropyl-1-(3-methylcyclohex-1-en-1-yl)isoquinoline

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: acetic acid; dihydrogen peroxide / 12 h / 80 °C
2.1: trichlorophosphate / 6 h / 50 °C
3.1: potassium carbonate / tetrahydrofuran / 0.5 h / Inert atmosphere
3.2: 12 h / 80 °C / Inert atmosphere
View Scheme
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    Product Name: Isoquinoline, 6-(1-methylethyl)- (9CI) Synonyms: Isoquinoline,6-(1-methylethyl)-;Isoquinoline, 6-(1-methylethyl)- (9CI);6-isopropylisoquinoline;6-propan-2-ylisoquinoline CAS: 790304-84-6 MF: C12H13N MW: 171.23832 EINECS: Product

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    Hangzhou Keying Chem Co., Ltd. Is a comprehensive enterprise, dedicated to the development, production and marketing of chemicals. As a technology innovative and service profession

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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