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83-38-5

Basic Information
CAS No.: 83-38-5
Name: 2,6-Dichlorobenzaldehyde
Article Data: 111
Molecular Structure:
Molecular Structure of 83-38-5 (2,6-Dichlorobenzaldehyde)
Formula: C7H4Cl2O
Molecular Weight: 175.014
Synonyms: 2,6-Dichlorobenzaldehyde
EINECS: 201-472-2
Density: 1.4 g/cm3
Melting Point: 69-71 °C(lit.)
Boiling Point: 239.2 °C at 760 mmHg
Flash Point: 97.4 °C
Solubility: <0.1 g/100 mL at 23 °C in water
Appearance: white to light yellow powder
Hazard Symbols: CorrosiveC, IrritantXi
Risk Codes: 34-36/37/38
Safety: 26-27-28-36/37/39-45-37/39
Transport Information: UN 3261 8/PG 2
PSA: 17.07000
LogP: 2.80590
Synthetic route
15258-73-8

2,6-dichlorobenzyl alcohol

83-38-5

2,6-dichlorobenzaldehyde

Conditions
ConditionsYield
With dmap; tetrakis(actonitrile)copper(I) hexafluorophosphate; N,N'-di-tert-butylethylenediamine; oxygen In dichloromethane at 20℃; under 760.051 Torr; for 3h; Schlenk technique; Molecular sieve; Sealed tube;99%
With tert.-butylnitrite; oxygen; acetic acid In toluene at 50℃; for 8.5h;99%
With 2,2'-azobis(isobutyronitrile); oxygen; sodium bromide In 1,4-dioxane at 70℃;94%
2828-47-9

2,6-Dichlorobenzaldehyde N,N-dimethylhydrazone

83-38-5

2,6-dichlorobenzaldehyde

Conditions
ConditionsYield
With 3-benzyl-5-(2-hydroxyethyl)-4-methyl-1,3-thiazol-3-ium chloride In chloroform at 20℃; for 1h; oxidative cleavage;98%
With chloro-trimethyl-silane; sodium iodide In water; acetonitrile for 0.0333333h; deprotection;94%
With triethylene diamine nickel thiosulfate; water In chloroform at 20℃; for 0.166667h; Hydrolysis;94%
With iron(II) sulfate In chloroform at 20℃; for 0.75h; Hydrolysis;88%
25185-95-9

2,6-dichlorobenzaldoxime

83-38-5

2,6-dichlorobenzaldehyde

Conditions
ConditionsYield
With Cr-MCM-41 zeolite on silica gel for 0.1h; microwave irradiation;98%
With 2,6-dicarboxypyridinium fluorochromate for 0.5h;96%
With potassium permanganate; 1-n-butyl-3-methylimidazolim bromide at 20℃; for 0.383333h; Ionic liquid; chemoselective reaction;91%
89-98-5

2-chloro-benzaldehyde

83-38-5

2,6-dichlorobenzaldehyde

Conditions
ConditionsYield
With N-chloro-succinimide; palladium diacetate; silver trifluoroacetate; anthranilic acid; trifluoroacetic acid In 1,2-dichloro-ethane at 60℃; for 24h; Sealed tube;95%
With N-chloro-succinimide; 2-hydroxyl-5-nitro-3-(trifluoromethyl)pyridine; 4-trifluoromethylphenylamine; palladium diacetate; trifluoroacetic acid In 1,2-dichloro-ethane at 80℃; for 24h; Sealed tube;92%
2014-83-7

1,3-Dichloro-2-chloromethyl-benzene

83-38-5

2,6-dichlorobenzaldehyde

Conditions
ConditionsYield
With dihydrogen peroxide; trimethylamine In water for 2h; Reflux;94%

2-(2,6-dichlorophenyl)-1,3-dithiane

83-38-5

2,6-dichlorobenzaldehyde

Conditions
ConditionsYield
With 1,3,5-trichloro-2,4,6-triazine; dimethyl sulfoxide In dichloromethane at 20℃; for 2.15h;91%
51379-82-9

2,6-Dichlorbenzaldehyd-2,4-dinitrophenylhydrazon

83-38-5

2,6-dichlorobenzaldehyde

Conditions
ConditionsYield
With potassium permanganate at 40℃; for 2.8h; Ionic liquid; chemoselective reaction;81%

2,6-dichlorobenzaldehyde dimethyl acetal

83-38-5

2,6-dichlorobenzaldehyde

Conditions
ConditionsYield
With β‐cyclodextrin In methanol; water at 50℃; for 10h;80%
33486-90-7

1,3-dichloro-2-methoxymethylbenzene

83-38-5

2,6-dichlorobenzaldehyde

Conditions
ConditionsYield
With N-Bromosuccinimide In tetrachloromethane for 1h; Irradiation; Reflux;77%
82073-58-3

2-(2,6-dichlorophenyl)-1,3-dioxolane

6399-81-1

triphenylphosphine hydrobromide

A

83-38-5

2,6-dichlorobenzaldehyde

B

7237-34-5

2-(hydroxyethyl)triphenylphosphonium bromide

Conditions
ConditionsYield
In dichloromethane at 50℃; for 0.0833333h; Microwave irradiation; Sealed tube;A 76%
B n/a
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    Product Name: 2,6-Dichlorobenzaldehyde CAS: 83-38-5 MF: C7H4Cl2O MW: 175.01 EINECS: 201-472-2 Mol File: 83-38-5.mol 2,6-Dichlorobenzaldehyde Structure 2,6-Dichlorobenzaldehyde Chemical Properties Melting point 69-71 °C (li

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Chemistry

The Molecular Structure of 2,6-Dichlorobenzaldehyde (CAS NO.83-38-5):
 

Empirical Formula: C7H4Cl2O
Molecular Weight: 175.0121 
IUPAC Name: 2,6-dichlorobenzaldehyde 
Appearance: white to light yellow powder
Nominal Mass: 174 Da
Average Mass: 175.0121 Da
Monoisotopic Mass: 173.96392 Da 
Index of Refraction: 1.6
Molar Refractivity: 42.79 cm3
Molar Volume: 125 cm3
Surface Tension: 45.1 dyne/cm
Density: 1.4 g/cm3
Flash Point: 97.4 °C
Enthalpy of Vaporization: 47.61 kJ/mol
Boiling Point: 239.2 °C at 760 mmHg
Vapour Pressure: 0.0406 mmHg at 25°C 
Water Solubility: <0.1 g/100 mL at 23 ºC
Sensitive: Air Sensitive
Stability: Stable. Incompatible with strong oxidizing agents, strong bases. Air, light and moisture sensitive
InChI
InChI=1/C7H4Cl2O/c8-6-2-1-3-7(9)5(6)4-10/h1-4H
Smiles
c1(c(cccc1Cl)Cl)C=O 
Product Categories: Benzaldehyde;Dicloxacillin;Aldehydes;C7;Carbonyl Compounds
Synonyms: CCRIS 6014 ; EINECS 201-472-2 ; Benzaldehyde, 2,6-dichloro-   

Uses

 2,6-Dichlorobenzaldehyde (CAS NO.83-38-5) can be used for the synthesis of dyes, intermediates of pesticide and pharmaceuticalare, also used as fungicides and herbicides and used in the manufacture of 2,6 - dichlorobenzonitrile .

Safety Profile

Hazard Codes: IrritantXiCorrosiveC
Risk Statements: 34-36/37/38 
R34: Causes burns
R36/37/38: Irritating to eyes, respiratory system and skin
Safety Statements: 26-27-28-36/37/39-45-37/39 
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice
S27: Take off immediately all contaminated clothing
S28: After contact with skin, wash immediately with plenty of soap-suds
S36/37/39: Wear suitable protective clothing, gloves and eye/face protection
S45: In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible)
S37/39: Wear suitable gloves and eye/face protection
RIDADR: UN 3261 8/PG 2
WGK Germany: 2
Hazard Note: Corrosive
HazardClass: 8
PackingGroup: III
HS Code: 29130000