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830346-48-0

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Basic Information
CAS No.: 830346-48-0
Name: 5-Bromo-1-(2-fluoro-6-trifluoromethyl-benzyl)-6-methyl-1H-pyrimidine-2,4-dione
Article Data: 11
Molecular Structure:
Molecular Structure of 830346-48-0 (5-Bromo-1-(2-fluoro-6-trifluoromethyl-benzyl)-6-methyl-1H-pyrimidine-2,4-dione)
Formula: C13H9BrF4N2O2
Molecular Weight: 381.124
Synonyms: 5-bromo-1-(2-fluoro-6-(trifluoromethyl)benzyl)-6-methylpyrimidine-2,4(1H,3H)-dione;5-bromo-1-[[2-fluoro-6-(trifluoromethyl)phenyl]methyl]-6-methylpyrimidine-2,4-dione;
Density: 1.684±0.06 g/cm3(Predicted)
Melting Point: >230°C (dec.)
PSA: 55.12000
LogP: 3.22600
Related products
Synthetic route
830346-47-9

1-(2-fluoro-6-(trifluoromethyl)benzyl)-6-methylpyrimidine-2,4(1H,3H)-dione

830346-48-0

5-bromo-1-[2-fluoro-6-(trifluoromethyl)benzyl]-6-methylpyrimidine-2,4-(1H,3H)-dione

Conditions
ConditionsYield
With bromine In acetic acid at 20℃;97.5%
With bromine; acetic acid for 14h;96%
With bromine; acetic acid at 20℃; for 3h;87%
15018-56-1

5-bromo-6-methyluracil

239087-08-2

1-(bromomethyl)-2-fluoro-6-(trifluoromethyl)benzene

830346-48-0

5-bromo-1-[2-fluoro-6-(trifluoromethyl)benzyl]-6-methylpyrimidine-2,4-(1H,3H)-dione

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 75 - 85℃;81%
830346-46-8

N-{[2-fluoro-6-(trifluoromethyl)phenyl]methyl}urea

830346-48-0

5-bromo-1-[2-fluoro-6-(trifluoromethyl)benzyl]-6-methylpyrimidine-2,4-(1H,3H)-dione

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium iodide / acetonitrile / 20 h / 0 - 20 °C
2: bromine; acetic acid / 2 h
View Scheme
Multi-step reaction with 2 steps
1: sodium iodide; chloro-trimethyl-silane / acetonitrile / 16 h / 0 - 25 °C / Inert atmosphere
2: acetic acid; bromine / 14 h
View Scheme
133116-83-3

2-fluoro-6-(trifluoromethyl)benzonitrile

830346-48-0

5-bromo-1-[2-fluoro-6-(trifluoromethyl)benzyl]-6-methylpyrimidine-2,4-(1H,3H)-dione

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: borane-THF / tetrahydrofuran / 60 °C / Heating / reflux
1.2: 20 °C
2.1: hydrogenchloride; water / 6 h / Heating / reflux
3.1: sodium iodide / acetonitrile / 20 h / 0 - 20 °C
4.1: bromine; acetic acid / 2 h
View Scheme
239087-06-0

(2-fluoro-6-(trifluoromethyl) phenyl)methanamine

830346-48-0

5-bromo-1-[2-fluoro-6-(trifluoromethyl)benzyl]-6-methylpyrimidine-2,4-(1H,3H)-dione

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: hydrogenchloride; water / 6 h / Heating / reflux
2: sodium iodide / acetonitrile / 20 h / 0 - 20 °C
3: bromine; acetic acid / 2 h
View Scheme
Multi-step reaction with 3 steps
1: hydrogenchloride / water / 12 h / 100 °C
2: sodium iodide; chloro-trimethyl-silane / acetonitrile / 16 h / 0 - 25 °C / Inert atmosphere
3: acetic acid; bromine / 14 h
View Scheme
830346-46-8

N-{[2-fluoro-6-(trifluoromethyl)phenyl]methyl}urea

84911-18-2, 609-13-2

ethyl 2-bromoacetoacetate

830346-48-0

5-bromo-1-[2-fluoro-6-(trifluoromethyl)benzyl]-6-methylpyrimidine-2,4-(1H,3H)-dione

Conditions
ConditionsYield
With trimethylsilyl bromide In N,N-dimethyl acetamide at 0 - 80℃; for 16h; Inert atmosphere;32.7 g
830346-48-0

5-bromo-1-[2-fluoro-6-(trifluoromethyl)benzyl]-6-methylpyrimidine-2,4-(1H,3H)-dione

67341-01-9, 117049-14-6, 138457-46-2, 102089-74-7

(R)-N-(tert-butoxycarbonyl)phenylglycinol

830346-49-1

{(R)-2-[5-bromo-3-(2-fluoro-6-trifluoromethyl-benzyl)-4-methyl-2,6-dioxo-3,6-dihydro-2H-pyrimidin-1-yl]-1-phenyl-ethyl}-carbamic acid tert-butyl ester

Conditions
ConditionsYield
With di-tert-butyl-diazodicarboxylate; triphenylphosphine In tetrahydrofuran at 20℃; for 16h;100%
With triphenylphosphine; diethylazodicarboxylate In tetrahydrofuran for 14h;99%
With di-tert-butyl-diazodicarboxylate; triphenylphosphine In toluene at 5 - 20℃;70%
832711-65-6

N-(benzyloxycarbonyl)-1(R)-hydroxymethyl-1,2,3,4-tetrahydroisoquinoline

830346-48-0

5-bromo-1-[2-fluoro-6-(trifluoromethyl)benzyl]-6-methylpyrimidine-2,4-(1H,3H)-dione

832711-58-7

5-bromo-1-[2-fluoro-6-(trifluoromethyl)benzyl]-6-methyl-3-[N-(benzyloxycarbonyl)-1(R)-1,2,3,4-tetrahydroisoquinoline]methylpyrimidine-2,4(1H,3H)-dione

Conditions
ConditionsYield
With di-tert-butyl-diazodicarboxylate; triphenylphosphine In tetrahydrofuran at 20℃; for 16h;100%
830346-48-0

5-bromo-1-[2-fluoro-6-(trifluoromethyl)benzyl]-6-methylpyrimidine-2,4-(1H,3H)-dione

C7H6FIOZn

1150560-59-0

5-(2-fluoro-3-methoxyphenyl)-1-{[2-fluoro-6-(trifluoromethyl)phenyl]methyl}-6-methylpyrimidine-2,4(1H,3H)-dione

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); tris-(o-tolyl)phosphine In dimethyl sulfoxide at 60 - 70℃; for 6h; Inert atmosphere;83%
830346-48-0

5-bromo-1-[2-fluoro-6-(trifluoromethyl)benzyl]-6-methylpyrimidine-2,4-(1H,3H)-dione

352303-67-4

(2-fluoro-3-methoxyphenyl)boronic acid

1150560-59-0

5-(2-fluoro-3-methoxyphenyl)-1-{[2-fluoro-6-(trifluoromethyl)phenyl]methyl}-6-methylpyrimidine-2,4(1H,3H)-dione

Conditions
ConditionsYield
Stage #1: (2-fluoro-3-methoxyphenyl)boronic acid With potassium iodide; potassium hydroxide In water; acetone at 25 - 30℃; for 0.166667h; Inert atmosphere;
Stage #2: 5-bromo-1-[2-fluoro-6-(trifluoromethyl)benzyl]-6-methylpyrimidine-2,4-(1H,3H)-dione With tri tert-butylphosphoniumtetrafluoroborate In water; acetone at 25 - 45℃; for 0.583333h; Inert atmosphere; Further stages;		79.2%
Stage #1: 5-bromo-1-[2-fluoro-6-(trifluoromethyl)benzyl]-6-methylpyrimidine-2,4-(1H,3H)-dione; (2-fluoro-3-methoxyphenyl)boronic acid With potassium hydroxide In water; acetone for 0.5h;
Stage #2: With palladium diacetate; tri tert-butylphosphoniumtetrafluoroborate In water; acetone at 70℃; for 10h;		76%
Stage #1: 5-bromo-1-[2-fluoro-6-(trifluoromethyl)benzyl]-6-methylpyrimidine-2,4-(1H,3H)-dione; (2-fluoro-3-methoxyphenyl)boronic acid With potassium hydroxide In water; acetone at 30℃; for 0.166667h;
Stage #2: With palladium diacetate; ruphos In water; acetone at 30 - 52℃; for 6h;
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    China (Mainland)  |  Contact Details

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    China (Mainland)  |  Contact Details

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     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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     China (Mainland)  |  Contact Details

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    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

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  • 830346-48-0

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    830346-48-0

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    China (Mainland)  |  Contact Details

    Business Type:Trading Company

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