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868539-96-2

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Basic Information
CAS No.: 868539-96-2
Name: Boc-HPh-Leu-Phe-OMe
Article Data: 6
Molecular Structure:
Molecular Structure of 868539-96-2 (Boc-HPh-Leu-Phe-OMe)
Formula: C31H43N3O6
Molecular Weight: 553.699
Synonyms: Boc-HPh-Leu-Phe-OMe;L-Phenylalanine, (αS)-α-[[(1,1-dimethylethoxy)carbonyl]amino]benzenebutanoyl-L-leucyl-, methyl ester;N-[(S)-2-(tert-Butoxycarbonylamino)-4-phenylbutanoyl]-L-leucyl-L-phenylalanine methyl ester
EINECS: -0
Density: 1.123±0.06 g/cm3(Predicted)
Boiling Point: 753.4±60.0 °C(Predicted)
PSA: 122.83000
LogP: 5.11660
Related products
Synthetic route
82732-07-8, 108524-68-1, 142926-43-0, 100564-78-1

Boc-L-homophenylalanine

Leu-Phe-OMe trifluoroacetate

868539-96-2

(S)-methyl 2-((S)-2-tert.butoxycarbonyIamino-4-phenylbutanamido-4-methylpentanamido)-3-phenylpropanoate

Conditions
ConditionsYield
With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine In DMF (N,N-dimethyl-formamide) at 0 - 20℃;
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In dichloromethane at 0 - 20℃; for 12h;
13734-34-4

N-tert-butoxycarbonyl-L-phenylalanine

38155-18-9

L-leucyl-L-phenylalanine methyl ester

868539-96-2

(S)-methyl 2-((S)-2-tert.butoxycarbonyIamino-4-phenylbutanamido-4-methylpentanamido)-3-phenylpropanoate

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 20℃;
13139-15-6

N-tert-butoxycarbonyl-L-leucine

868539-96-2

(S)-methyl 2-((S)-2-tert.butoxycarbonyIamino-4-phenylbutanamido-4-methylpentanamido)-3-phenylpropanoate

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 20 °C
2: trifluoroacetic acid / dichloromethane / 3 h
3: N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 20 °C
View Scheme
Multi-step reaction with 2 steps
1.1: benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate / N,N-dimethyl-formamide / 0 °C / Inert atmosphere
2.1: trifluoroacetic acid / dichloromethane / 2 h / 0 - 20 °C
2.2: 0 - 20 °C / Inert atmosphere
View Scheme
Multi-step reaction with 3 steps
1: benzotriazol-1-ol; 4-methyl-morpholine; dicyclohexyl-carbodiimide / dichloromethane / 2 h / 0 - 30 °C / Inert atmosphere
2: hydrogenchloride / isopropyl alcohol / 2 h / 25 - 30 °C
3: benzotriazol-1-ol; 4-methyl-morpholine; dicyclohexyl-carbodiimide / dichloromethane / 2 h / 0 - 30 °C / Inert atmosphere
View Scheme
Multi-step reaction with 2 steps
1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C
2: trifluoroacetic acid / dichloromethane
View Scheme
7524-50-7

methyl (2S)-2-amino-3-phenylpropanoate hydrochloride

868539-96-2

(S)-methyl 2-((S)-2-tert.butoxycarbonyIamino-4-phenylbutanamido-4-methylpentanamido)-3-phenylpropanoate

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 20 °C
2: trifluoroacetic acid / dichloromethane / 3 h
3: N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 20 °C
View Scheme
Multi-step reaction with 3 steps
1: benzotriazol-1-ol; 4-methyl-morpholine; dicyclohexyl-carbodiimide / dichloromethane / 2 h / 0 - 30 °C / Inert atmosphere
2: hydrogenchloride / isopropyl alcohol / 2 h / 25 - 30 °C
3: benzotriazol-1-ol; 4-methyl-morpholine; dicyclohexyl-carbodiimide / dichloromethane / 2 h / 0 - 30 °C / Inert atmosphere
View Scheme
15136-32-0, 87976-66-7, 120342-25-8, 5874-73-7

(N-(tert-butoxycarbonyl)-L-leucinyl)-L-phenylalanine methyl ester

868539-96-2

(S)-methyl 2-((S)-2-tert.butoxycarbonyIamino-4-phenylbutanamido-4-methylpentanamido)-3-phenylpropanoate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: trifluoroacetic acid / dichloromethane / 3 h
2: N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / N,N-dimethyl-formamide / 20 °C
View Scheme
Multi-step reaction with 2 steps
1: hydrogenchloride / isopropyl alcohol / 2 h / 25 - 30 °C
2: benzotriazol-1-ol; 4-methyl-morpholine; dicyclohexyl-carbodiimide / dichloromethane / 2 h / 0 - 30 °C / Inert atmosphere
View Scheme
Multi-step reaction with 2 steps
1: dichloromethane / 3 h / 0 - 20 °C
2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 0 - 20 °C
View Scheme
15136-32-0, 87976-66-7, 120342-25-8, 5874-73-7

(N-(tert-butoxycarbonyl)-L-leucinyl)-L-phenylalanine methyl ester

82732-07-8, 108524-68-1, 142926-43-0, 100564-78-1

Boc-L-homophenylalanine

868539-96-2

(S)-methyl 2-((S)-2-tert.butoxycarbonyIamino-4-phenylbutanamido-4-methylpentanamido)-3-phenylpropanoate

Conditions
ConditionsYield
Stage #1: (N-(tert-butoxycarbonyl)-L-leucinyl)-L-phenylalanine methyl ester With trifluoroacetic acid In dichloromethane at 0 - 20℃; for 2h;
Stage #2: Boc-L-homophenylalanine With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine In dichloromethane; N,N-dimethyl-formamide at 0 - 20℃; Inert atmosphere;		21.59 g
Stage #1: (N-(tert-butoxycarbonyl)-L-leucinyl)-L-phenylalanine methyl ester With trifluoroacetic acid In dichloromethane
Stage #2: Boc-L-homophenylalanine With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In dichloromethane		246 mg
2577-90-4

methyl (2S)-2-amino-3-phenylpropanoate

868539-96-2

(S)-methyl 2-((S)-2-tert.butoxycarbonyIamino-4-phenylbutanamido-4-methylpentanamido)-3-phenylpropanoate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate / N,N-dimethyl-formamide / 0 °C / Inert atmosphere
2.1: trifluoroacetic acid / dichloromethane / 2 h / 0 - 20 °C
2.2: 0 - 20 °C / Inert atmosphere
View Scheme
Multi-step reaction with 3 steps
1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 0 - 20 °C
2: dichloromethane / 3 h / 0 - 20 °C
3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 12 h / 0 - 20 °C
View Scheme
82732-07-8, 108524-68-1, 142926-43-0, 100564-78-1

Boc-L-homophenylalanine

6461-07-0

(S)-methyl 2-((S)-2-amino-4-methylpentanamido)-3-phenylpropanoate hydrochloride

868539-96-2

(S)-methyl 2-((S)-2-tert.butoxycarbonyIamino-4-phenylbutanamido-4-methylpentanamido)-3-phenylpropanoate

Conditions
ConditionsYield
With 4-methyl-morpholine; benzotriazol-1-ol; dicyclohexyl-carbodiimide In dichloromethane at 0 - 30℃; for 2h; Inert atmosphere;121.0 g
61-90-5

L-leucine

868539-96-2

(S)-methyl 2-((S)-2-tert.butoxycarbonyIamino-4-phenylbutanamido-4-methylpentanamido)-3-phenylpropanoate

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: sodium hydroxide / water / 20 h / 25 - 30 °C
2: benzotriazol-1-ol; 4-methyl-morpholine; dicyclohexyl-carbodiimide / dichloromethane / 2 h / 0 - 30 °C / Inert atmosphere
3: hydrogenchloride / isopropyl alcohol / 2 h / 25 - 30 °C
4: benzotriazol-1-ol; 4-methyl-morpholine; dicyclohexyl-carbodiimide / dichloromethane / 2 h / 0 - 30 °C / Inert atmosphere
View Scheme
63-91-2

L-phenylalanine

868539-96-2

(S)-methyl 2-((S)-2-tert.butoxycarbonyIamino-4-phenylbutanamido-4-methylpentanamido)-3-phenylpropanoate

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: thionyl chloride / 8 h / 25 - 30 °C
2: benzotriazol-1-ol; 4-methyl-morpholine; dicyclohexyl-carbodiimide / dichloromethane / 2 h / 0 - 30 °C / Inert atmosphere
3: hydrogenchloride / isopropyl alcohol / 2 h / 25 - 30 °C
4: benzotriazol-1-ol; 4-methyl-morpholine; dicyclohexyl-carbodiimide / dichloromethane / 2 h / 0 - 30 °C / Inert atmosphere
View Scheme
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    Produce in South China, less pressure in environment protection, more stable production.Honored as "National Hi-tech Enterprise" & "Shenzhen Hi-tech Enterprise";4000+m2 R&D center & 47,000m2 plant, 20 R&D technicians, tens of reactors from 100L to 50

    ShenZhen InnoSyn Biotech Co.,Ltd is an expert manufacturer of derivatives of amino acids and other important intermediates for use in laboratory drug research and peptide applicat

  • ShenZhen InnoSyn Biotech Co.,Ltd

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86-755-28351685

    Address:Floor 5 & 6, Building A1, HAIKEXING Strategic Innovative Industrial Park, 16 BaoShan Road, PingShan District

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  • Boc-HPh-Leu-Phe-Ome

  • Casno:

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    Boc-HPh-Leu-Phe-Ome

    Min.Order: 0

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    Known for its best quality and competitve price, this chemicals we offered is widely appreciated by our customers.Appearance:yellow to white solid Storage:keep sealed and keep from direct light Package:According client's requirements Application:Phar

    Jinan YSPharma Biotechnology Co., Ltd is a large group specializing in contract manufacturing to the pharmaceutical, agrochemical and Fine chemicals with top quality products and s

  • coolpharm Ltd

    China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:86-531-8233381 86-18678657237

    Address:Room 302,Building 1,Union Fortune Square, No. 2117,Tianchen Road,High-tech Zone,Jinan,Shandong,China

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  • Casno:

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    Boc-HPh-Leu-Phe-OMe

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    In stock ,If you need HNMR\HPLC,please contact us!excellent quality and reasonable price and absolutely worthy. Storage:in stock Application:Pharmaceutical Intermediate Transportation:By air or By sea or By express

    Cjioo, Kajie (Shanghai) biotechnology co., LTD., is an expert in China's independent inhibitors, Cjioo Chemicals is one of the world's leading supplier of high performance life sci

  • Cjioo(Shanghai) biotechnology co., LTD

    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-021-31664350

    Address:Pudong New Area Shanghai Miaojing Road 600-17

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  • Carfilzomib Impurity 70

  • Casno:

    868539-96-2

    Carfilzomib Impurity 70

    Min.Order: 0

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    1. Our staff are all biomedical related majors with rich experience in the pharmaceutical industry, and can provide you with more professional services.2. Our supplier has a good quality management system, and the quality of products is reliable and

  • Shenzhen Sumshine Biotech Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:15914108025

    Address:229A, No.15, Xinbeli Industrial Zone, Xinshi Community, Dalang Street, Longhua District

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  • 868539-96-2

  • Casno:

    868539-96-2

    868539-96-2

    Min.Order: 0

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    R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates

    Alchemist-pharm chemical Technology Co. Ltd. is a high-tech company which specificalized in R&D and production of fine chemicals, pharmaceutical raw materials and intermediates. L

  • Alchemist-pharm chemical Technology Co. Ltd.

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:0086-371-67991738

    Address:Address:No. 35 Dongqing Street High-tech District 450001, Zhengzhou China

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  • Boc-HPh-Leu-Phe-OMe

  • Casno:

    868539-96-2

    Boc-HPh-Leu-Phe-OMe

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    high purity Application:Drug intermediates Materials intermediates and active molecules

    Novachemistry offers a broad range of specialty chemicals and customized synthesis services to a range of pharmaceutical, agrochemical and biochemical industries. Novachemistry has

  • NovaChemistry

    United Kingdom  |  Contact Details

    Business Type:Trading Company

    Tel:+44 (0)208 191 7890

    Address:Unit11, Ark Business Centre, Gorden Road, Loughborough, United Kingdom

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